黄原酸

Objective To determine the contents of chlorogenic acid and baicalin in the Yinhuang Buccal Tablet.

目的：测定银黄含片中绿原酸和黄芩苷的含量。

The main results were as follows. The main nutrition bioactive components in Opuntia Milpa Alta were analyzed using chemical and instrumental analytical methods. The results showed that the content of crude protein and fat was 0.65%～0.68% and 0.30%～0.31% respectively. The total content of the amino acids was 6.81%～7.38%, and Glu was 1.08%～1.52%.The contents of pectin and cellulose was 1.47%～1.68%, 0.87%～1.22% respectively. They were oxalate free and rich in Ca 5.6%, Fe 8.06mg/100g, Zn 3.30mg/100g, VB6 5.62mg/100g, low in tannin 0.02%～0.04%.The bioactive matter content such as polysaccharide, polyphenol, and flavone were high, about 1.27%, 63.14mg/100g, 36.21mg/100g respectively.

主要研究内容如下：采用化学和仪器分析方法，对米邦塔仙人掌中的主要营养和生理活性成分进行分析，结果表明，粗蛋白含量为0.65%～0.68%，脂肪含量为0.30%～0.31%；氨基酸总量为6.81%～7.38%，其中谷氨酸含量达1.08%～1.52%；果胶、膳食纤维分别为1.47%～1.68%和0.87%～1.22%；干样钙含量5.6%，铁8.06mg/100g，锌3.30mg/100g；B族维生素丰富，其中干样VB6含量5.62mg/100g；单宁0.02%～0.04%；不含草酸；生理活性物质如粗多糖、多酚、黄酮类物质分别约为1.27%、63.14mg/100g、36.21mg/100g，半乳糖约占多糖中单糖总量的80%；HPLC检测出8种酚类物质，绿原酸含量最多达42.40μg/g，其次是芦丁和槲皮素，其含量分别为25.02μg/g和10.91μg/g。

There is significant positive correlation between the total flavonoids content and total chlorogenic acid content in the leaves of S.chinensis with three different altitudes.

对不同生境夏蜡梅营养器官的总黄酮和总绿原酸含量进行测定，并分析了与环境因子之间的相关性。

To further study the chemical constitutes of lipophilic active parts, we prepared Alc95% and Alc50% according to original literature. 20 compounds were isolated by using macroporous resin, silica gel, polyamide, Sephadex LH-20, Rp-18, preparative TLC and preparative HPLC chromato-graphy. The structures of them were elucidated by means of physical and chemical properties, modern spectroscopic analysis techniques—UV、IR、 EI/MS、ESI/MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC. They are nine anthraquinones: chrysophanol (95-1), physcion (95-2), emodin (95-5), aloemodin (95-7), rhein (50-1), sennoside A or B (50-6),ω-hydroxylemodin (95-10), chrysophanol-8-0-β-D-glucoside (95-12), aloemodin-ω-0-β-D-glucoside (95-13); three phenanthaquinones: tanshinone ⅡA (95-3), cryptotanshinone (95-6), tanshinone Ⅰ(95-4); one isoflavone: 7, 3'-dihydroxyl-5' methoxyisoflavone (95-14) and protocaechuic aldehyde (95-9), protocaechuic acid (95-11), astragaloside Ⅳ(50-4), amygdalin (50-5), 2, 3, 5, 4'-tetrahydroxylstilbene-2-0-β-D-glucoside (50-3),-catechin (50-2), cinnamic acid (95-8). Among them, 3'-dihydroxyl-5' methoxyisoflavone (95-14) is a new compound.

经过溶剂萃取、大孔吸附树脂富集、Sephadex LH-20精制、制备TLC及Semi-pre HPLC等手段从中分离了20个化合物，利用理化性质和波谱技术(UV、IR、EI／MS、ESI／MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC)相结合鉴定了它们的结构，分别为9种蒽醌类化合物：大黄酚，大黄素甲醚，大黄素，芦荟大黄素，大黄酸，番泻苷A或B，ω-羟基大黄素(ω-hydroxylemodin)，大黄酚-8-0-β-D-葡萄糖苷(chrysophanol-8-0-β-D-glucoside)，芦荟大黄素-ω-0-β-D-葡萄糖苷(aloemodin-ω-0-β-D-glucoside)；3种菲醌类化合物：丹参酮ⅡA(tanshinoneⅡA)，隐丹参酮，丹参酮Ⅰ(tanshinone Ⅰ)；1种异黄酮：7，3'-二羟基-5'-甲氧基异黄酮（7，3'-dihydroxy-5' methoxyisofla-vone）以及原儿茶醛，原儿茶酸，黄芪甲苷(astragaloside Ⅳ)，苦杏仁苷，2，3，5，4'-四羟基二苯乙烯-2-0-β-D-葡萄糖苷（2，3，5，4'-tetrahydroxylstilbene-2-O-β-D-g1ucoside），Z—儿茶素，桂皮酸。

Purified water, octyl palmitate, castor oil phosphate, triethoxycaprylylsilane, glyceryl stearate, peg-100 stearate, isopropyl palmitate, cetearyl alcohol, vegetable glycerin, phenoxyethanol, benzyl alcohol, potassium sorbate, tocopherol, stearic acid, certified organic aloe barbadensis extract, certified organic lavandula angustifolia extract, avena sativa kernal flour, certified organic helianthus annuus seed oil, panthenol (vitamin B5), certified organic simmondsia chinensis seed oil, polysorbate 60, allantoin, certified organic chamomilla recutita flower extract, potassium cetyl phosphate, and xanthan gum.

纯水、辛基棕榈酸酯、蓖麻油磷酸盐、triethoxycaprylylsilane、硬脂酸锌，异丙酯、peg-100棕榈酸、cetearyl酒精、蔬菜甘油、萃取物、苯甲醇、山梨酸钾、生育酚、硬脂酸、有机认证索芦荟精华、有机认证此提取物、淡紫色沙枣阿韦纳处理(燕麦粉、有机认证的核心annuus的向日葵籽油、维他命原B5、泛醇经认证的有机simmondsia羊(霍霍巴籽油、polysorbate 60、尿囊素、有机认证chamomilla recutita洋甘菊三叶草萃取物、钾cetyl磷酸盐、黄原胶。

The separation and purification techniques of chlorogenic acid and flavonoids in Chinese medicine Eucommia ulmoide oliver were tested.

试验研究了杜仲绿原酸、总黄酮的分离纯化工艺。

The Wuling Mountain where Our company location is rich in traditional Chinese medicine resources,we have research in zhenzhulan tea ,honeysuckle,Ginkgo biloba,Chinese goldthread,corktree,Wsojutsu var ,Wild Buckwheat Rhizome,Artemisia annua,red clover,Eucommia Bark,Fiveleaf Gynostemma Herb,we can provide special products as tea polyphenols,Honeysuckle P.E,Fagopyrum P.E,Red Clover P.E,Gynostemma P.E.

我们公司以武陵山区丰富的中药资源作为依托，对区域内优势资源珍珠兰茶、金银花、银杏、黄连、黄柏、白术、金荞麦、黄花蒿、红车轴草、杜仲、绞股蓝等进行了开发，基于以上资源资源，我们可以为合作伙伴提供茶多酚、绿原酸、金荞麦提取物、红车轴草提取物、绞股蓝提取物等特色产品。

Thetotal amount of 13 kinds of acid methanol soluble phenolic substances in female plant leaves ofAcer negundo L.was also significantly higher than that in male plant leaves.

因为原儿茶酸、丁香酸、苯甲酸、肉桂酸、杨梅黄酮等组分的含量较高，复叶槭雌株叶片中13种酸性醇溶性酚类物质的总量普遍高于雄株(p＜0.01)。

Results: Up to date, most of the found chemical compostition of Flos Lonicerae conclude essential oil, flavonoid, organic acid, triterpenoid and microelement; The pharmacal researches show that it can antagonize pathogenic microorganism, anticatarrhals,...

结果 ：至目前为止，已发现的化学成分主要有挥发油、黄酮类、有机酸、三萜类、无机元素等；药理研究表明金银花具有抗病原微生物、抗炎、解热、保肝、抗生育、止血、免疫调节、降血脂、中枢兴奋等作用；临床上主要用于多种感染、各种炎症、高热症、高脂血症、肿瘤放疗、化疗口干症等；金银花质量标准主要以其主要成分绿原酸为指标，检测方法多采用薄层色谱法和高效液相色谱法。

Results: The hairy root was successfully induced and the hairy root culture system was set up; The opines assay was positive for mannopine and agropine; The result of determination showed that there were a lot of anthroquinone constituents in the rhubarb hairy root and the contents of rhein, aloe-emodin, emodin or 8-O-methylchrysophanol were respectively higher than those in wild plant root.

结果：诱导出了天山大黄发根，并建立了发根离体培养系；从发根中检测到甘露碱、农杆碱的存在；定量分析发现，天山大黄发根中含有多种蒽醌类成分，其中大黄酸、芦荟大黄素、大黄素、大黄酚-8-甲醚的含量分别高于原植物根中的含量。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。