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The room temperature modulus and high temperature modulus of cured samples with low content of onium salt initiator have little change before and after the addition of co-initiator.

碘锚盐引发剂含量较低时,加入共引发剂的体系的常温及高温模量与未加体系相比没有明显变化;碘锚盐引发剂含量较高时,加入共引发剂的体系的常温模量比未加体系有所上升,而高温模量则变化不大。

In the field of visible photosensitive resin, the absorption spectrum, excited state, solvent polarity effect, fluorescence spectrum, fluorescence quenching, concentration effect, photo fading, reaction mechanism as well as photopolymerization kinetics of xanthene iodonium salts and cyanine dye-borate were discussed. It is found that under the radiation of visible light, intra-ion-pair electron transfer reactions occur in bis salt of fluorescein and unsymmetrical trimethine cyanines containing quinoline end group triphenyl-butylboron, and the fading rate is very high.

在可见光敏树脂部分,通过对呫吨染料碘鎓盐和菁染料-硼盐体系的吸收光谱性质、激发态性质、溶剂极性效应、荧光光谱、荧光猝灭、浓度效应、光褪色反应、光聚合动力学等的研究,结果发现:荧光黄双二苯基碘鎓盐体系和含喹啉环端基不对称三甲川菁染料-三苯基丁基硼盐体系在可见光作用下均发生离子对内电子转移反应,且光褪色反应速率很高。

The incidence of anaphylactoid reaction is 1.28%.

低渗透压、非离子型碘造影剂目前已完全替代了以往的高渗透压、离子型碘造影剂,副反应明显减少[1,2]。

In a similar way, using N,N\'-dibenzyl tartamide as auxiliary,-(2-methyl)allyl-2-chloro-phenyl-methyl azide, a vital intermediate of Repaglinide, can be prepared via asymmetric allylation of o-chlorobenzaldehyde in

产物经氧化和碘加成内酯化反应得到阿伐他汀中间体(3R,5S)-3-羟基-5-碘甲基戊内酯(10);将N-苄基酒石酸二酰胺用于邻氯苯甲醛的不对称烯丙基化反应以较高光学收率得-甲基烯丙基-2-氯苯基-甲基醇

Although the ion-exchange capacity of membrane quaternized by methyl iodide is higher than that of membrane quaternized by methylene diiodide,mechanical properties of the former are too poor to form membranes.

以一碘甲烷为季铵化试剂制备的离子交换膜其离子交换当量要比以二碘甲烷为季铵化试剂的要高,但机械强度差。在相同条件下,提高反应温度,有利于膜的季铵化反应,而不利于膜的磺化反应。

Urine VMA level is a useful marker to detect extra-adrenal pheochromocytoma and CT scan is the most reliable in localizing the lesions.131-MIBG scintigraphy is of great value for the localiza-tion and quantitative for extrarenal pheochromocytoma with high sensitivity and accuracy.It may be also used as a therapeutic method.

VMA及血、尿儿茶酚胺是定性诊断异位嗜铬细胞瘤的主要依据,CT诊断定位准确、131碘-间位碘代苄胍(131I-MIBG)定位准确、敏感性高,且可作为治疗措施。

The second part, we have developed a convenient and highly-regioselective approach to synthesis of trisubstituted iodofurans.

第二部分,我们发展出一个便利且具有高度位向选择性的方法来制备三取代碘化呋喃,由高炔丙基醇可以顺利的得到2,4,5-三取代碘化呋喃。

The conversion of alcohols to alkyl halides was investigated using acidic ionic liquid X as halogenating agent, acidic catalyst as well as medium. The reactions of primary alcohols gave very satisfactory conversions and selectivities except for the substrates with lower boiling point,such as n-octanol and benzyl alcohol. They obtained the corresponding halides with almost quantitative yields(95%-100%).The secondary alcohols also gave the corresponding halides with excellent conversions, however, the by-products of dehydration were detected.

伯醇除某些低沸点底物外,都以高转化率(最高达100%)和高选择性(最高达100%)转化为相应的氯代烃、溴代烃和碘代烃,例如正辛醇、苯甲醇,在X中进行卤代反应得到令人满意的结果,无论氯代、溴代还是碘代得到卤代产物的收率一般都很好华东师范大学化学系01级博士学位论文(95十100%),极少有重排产物及脱水产物被检测出来。

Reached slightly higher iodine delivery rates with a 300 mg l/ml iopromide solution than with 370 mgI/ml or iopamidol 370 mgl/ml.10The advantage of less concentrated (e.g. 300 mgl/ml) over more concentrated low osmolar contrast media in respect of injection and iodine delivery rates at room temperature and at 37°C was confirmed.11,12 In vivo, a slightly slower intravenous injection of concentrated contrast media may be compensated or even overcompensated because a higher concentration may be maintained after dilution by a given rate of blood flow.

到达递送以这 300 毫克 l│毫升 iopromide 解决评估的些微比较高的碘超过与 370 mgI│毫升或 iopamidol 370 mgl│毫升。10个比较不集中的(举例来说 300 mgl│毫升)结束更集中的低 osmolar 差别媒体的利益在注入和碘递送率方面在室温和 37 °C 被确认了。11,12在活泼地,一个集中差别媒体的些微比较慢静脉内注入可能被偿还或者平坦的 overcompensated 因为较高的集中可能在稀释之后被血流程的给定比率所维护。

After forming the tooth week bag, usually carried on a medicine processing to the tooth week bag, can place to go into various medicine in the tooth week bag, such as iodine glycerin, compound prescribe iodine liquid or anti-virus medicine, make the tooth kept a higher medicine density inside the bag for week, exterminate a tooth various germ of bag attained to disinfect, eliminate inflammation and refrained from rash action for week of function.

形成了牙周袋后,通常对牙周袋进行药物处理,可在牙周袋内置入各种药物,如碘甘油、复方碘液或抗菌药物,使牙周袋内保持较高的药物浓度,消灭牙周袋的各种细菌,达到杀菌、消炎和收敛的作用。

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