高温测定

Polyimide films capped with nonreactive phthalimide end groups were synthesized with theoretical number average molecular mass of 10000 and 30000 calculated using the Carothers equation. The effect of end-capper on the thermal properties was studied by investigating the change of the glass transition temperature T(subscript g of films after cured at high temperature.

制备了经邻苯二甲酸酐封端的理论数均分子量为10000和30000的聚酰亚胺薄膜，通过差示扫描热分析测定薄膜高温热处理前后玻璃化温度的变化，研究了PA封端对ODPA/ODA聚酰亚胺薄膜热稳定性能的影响。

An environmentally benign method to accelerate the pinacol rearrangement in high temperature liquid water by the addition of CO2 was proposed.

提出了一种通过引入CO2来提高高温液态水中频那醇重排反应速度的方法，测定了不同CO2初始压力和温度等对频那醇重排反应动力学的影响。

For resolving the lack of solubility data terephthalic acid in aqueous acetic acid, a method of determining the solubility at high temperature was developed.

针对对苯二甲酸工业中的溶解度基础数据缺乏的问题，提出了一种测定高温下对苯二甲酸在醋酸水溶液中的溶解度的方法。

Using thermophilic oxidation process to treat kitchen garbage, and determine the effects of temperature, COD, moisture and weight on the reaction process.

采用高温好氧法对厨房垃圾进行了处理，测定温度、COD、含水率、重量对反应过程的影响。

With regard to functional components, final baked Toona Sinensis contained polyphenol and total flavonoids.

在机能性成分测定中，证实添加香椿之土司经过高温烤焙后，仍可保有总酚及总类黄酮含量。

In this study, isolate 23 microbes with lipase activity from Wu-Jie scrap heap at Ilan and Taichung Environmental Protection Section. When the microbes incubator in 50oC, there are isolates B61 and M63 that lipase activity are better than others. Brevibacillus borstelensis SH168 isolated from NTU resterant food waste compost is used as control check. Isolates B61, M63 and Brevibacillus borstelensis SH168 determine the lipase activity by the LB with tributyrin. The lipase activity of isolates B61 and M63 are 2~3 fold higher than Brevibacillus borstelensis SH168. So isolates B61 and M63 are more useful in producing lipase. Isolate B61 can grow at pH 5~9, and at temperature 20oC ~ 60oC; isolate M63 can grow at pH 6~10, and at temperature 30oC ~ 50oC. Isolates B61 and M63 were identified by 16S rRNA. Isolate B61 is Bacillus circulans, and isolate M63 is Bacillus species.

本研究，於宜兰五结垃圾场和台中市环保局厨余堆肥样品中共分离出 23 株具脂肪酶活性菌株， 23 株菌株中经过三油酸甘油酯的洋菜培养基於 50℃培养 5 天后，发现有 2 株菌的脂肪酶活性较强，分别为分离株 B61 和 M63；以本实验室先前自台大女九餐厅蔬果厨余堆肥中所筛选出的耐高温脂解菌 Brevibacillus borstelensis SH168作为本实验对照菌株，将分离株 B61、M63 及 Brevibacillus borstelensis SH168 3 株菌株於含有三酪酸甘油酯液态培养基培养并测定其脂肪酶活性，发现分离菌株之活性皆比 Brevibacillus borstelensis SH168 高出 2~3 倍，认为分离株 B61、M63 适於产生脂肪酶的菌株，分离株 B61 在 pH 5~9 皆可生长，生长温度介於 20 oC ~ 60oC；分离株 M63 在 pH 6~10 可生长，生长温度介於 30 oC ~ 50oC； 2 株分离菌株以 16S rRNA定序结果分离株 B61 为 Bacillus circulans，分离株 M63 为 Bacillus 属。

High-temperature cellulolytic microbes were isolated from cow dung unartificial compost and were determined the enzyme activity of C1, CMCaae and Fpaae.

方法］从牛粪自然堆肥中分离出高温纤维素分解纤维素菌，并测定其外切纤维素酶活（C1酶）、羧甲基纤维素酶活、FPA酶活。

Methods Soil was air-dried, grinded, and screened through 100 mesh sieve. Appropriate sample was put in porcelain crucible with 0.5 g Aldrin reagents, and another 2 g Aldrin was used to cover the sample. Then the mixture was burned, cooled off, lixiviated by water, and determined by arsenic-cerium redox spectrophotometry.

土壤经自然风干，粉碎过100目筛，取适量试样于盛有0.5g艾氏试剂的瓷钳埚中，再取2g艾氏试剂覆盖试样，置高温炉中灼烧，冷却，水浸提，砷铈氧化还原分光光度法测定碘含量。

Relevant conditions were optimized to ensure that most of trace elements evaporated steadily during laser ablation in layer-by-layer. So the impurity elements of low boiling point were determined successfully.

对分析条件进行了全面系统的优化，使高温合金中大多数痕量元素通过层层剥蚀的激光剥蚀过程被稳定地蒸发，从而顺利对低沸点杂质元素进行了测定。

The results showed that Kaidimycin was chemically neutral, macrocylic polylactones, stable and liable to dissolve into water and pyridine, slight to dissolve into methanol, ethanol and N-butanol, difficult to dissolve into ethyl acetate, acetone, benzene and chloroform. Chemical reaction of functional group of Kaidimycin showed that it had glycoside, amino acid and aldehyde, no reducing sugar, polypeptide and phenol.

凯地菌素属中等极性的、中性抗生素，极性纸层析结果与多烯类抗生素的纸层析结果相似：易溶于水、吡啶，微溶于甲醇、乙醇、正丁醇，不溶于乙酸乙酯、丙酮、苯、三氯化碳；对高温、光照和紫外处理有很好的稳定性；官能团反应试验结果发现，凯地菌素可能含有糖苷键、氨基酸伯氨基和醛基，不含有还原糖、多肽和酚基，高锰酸钾、浓硫酸反应与多烯大环内酯类抗生素的特性相似；并且依据纯品，采用生物法和分光光度法对摇床发酵液进行了效价的测定。

And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

47：5 法老对约瑟说，你父亲和你弟兄们到你这里来了。

Additionally, the approximate flattening of surface strip using lines linking midpoints on perpendicular lines between geodesic curves and the unconditional extreme value method are discussed.

提出了用测地线方程、曲面上两点间短程线来计算膜结构曲面测地线的方法，同时，采用测地线间垂线的中点连线和用无约束极值法进行空间条状曲面近似展开的分析。