高温测定

We present a simple approach to determine the content of casein in crosslinked polyacylamide, i. e., protein molecules are complexed with copper ions by biuret reaction. The polymer containing proteins is cinerated at high temperature and then the residue is dissolved into nitric acid. Protein content is measured by determining concentration of copper ion in nitric acid solution using atomic absorption spectrum.

本文提出了一种在交联聚丙烯酰胺中测定酪蛋白的简便方法，即：利用双缩脲反应使蛋白质与铜离子络合，含蛋白质的聚合物在高温下灰化，残留物溶于硝酸，通过用原子吸收光谱测定硝酸溶液中的铜离子浓度来测量蛋白质的含量。

Rapid determination methods for BOD are reviewed, high temperature method、corelation coefficient method and biosensor method included.

综述BOD快速测定方法，快速测定方法包括高温法、相关系数法和生物传感器法。

The research results will be of significance for coal utilization ,fluoridation pollution appreciation and control and can provide prescription for studying new fluorine determination process .

文献[1]中介绍了煤中微量元素氟的各种间接和直接的测定方法的研究进展，并对各种方法的适用性、存在的问题及测定精度进行比较分析和评价，结果表明：高温燃烧水解——氟离子选择电极法测量煤中氟具有操作简单、快

By systemic researching and simulating experiment, the text gains such results as follows,1. On the base of sufficiency research on the oil-gas hydrocarbon systemic chemistry composing and the physical chemistry characters, we traverse the mechanism of the paraffin's deposition. Then we consider that paraffin deposition is a complex process ofphysical chemistry, which includes more than one single mechanism.2. Traversing and comparing the literature in detail on different factors that has effect on paraffin deposition, the available experimental methods on paraffin deposition, prevention of paraffin deposition, and removing of the deposited paraffin on the spot.3. Ameliorated the laser equipment of solid particle inspecting system and the corresponding test methods. Determine WCT of dead oil and live oil from KS101 well under different pressure with this system. The result implies that dead oil has opposite regulation on paraffin deposition temperature to live oil.4. A vapor-liquid-solid envelop is drawn by superposition regular vapor-liquid envelop and WCT curve thereby explained that the departure and quick raising of the curve in the low temperature zone is caused by the appearance of paraffin in solid phase.5. Estimation is made to determine the depth of paraffin deposition in the well.

通过系统的研究和实验模拟，本文取得了以下研究成果：(1)在充分调研油气烃类体系的化学组成及其物理化学特征的基础上，详细研究了石蜡沉降的机理，认为石蜡沉积是一个复杂的物理化学过程，是多种机理共同作用的结果；(2)深入调研并综合阐述了影响石蜡固相沉积的各种主要因素，对目前国内外常用的有机固相沉积实验研究方法和现场清防蜡措施也做出详尽的描述，并加以对比评价；(3)改进了油气藏开发重点实验室自行研制组装的高温高压下测定固相沉积的激光装置和测试方法，并用该套设备测定出柯深101井的井口脱气油样和凝析气平衡油样不同压力下的析蜡点，实验结果表明，脱气油和平衡油析蜡规律相反；(4)将常规气-液两相相图和析蜡曲线叠加得到了气—液—固三相相图，从而解释了气-液两相等液量线在低温区域偏离正常并快速上翘是由于体系有石蜡固相出现；(5)利用实验测试的析蜡温度预测析蜡位置，表明只有在距井口465m油管以上会有蜡析出。

Adding fused MnO2-CaF2 Mineralizer into fine silicon powder can change its cryst al structure and improve the amount of tridymite,thus can improve the kiln furni ture's high temperature properties and prolong its lifetime.

MnO2-CaF2混合矿化剂能改善硅微粉析晶结构，增加磷石英的含量，从而改善窑具的高温性能，延长使用寿命；采用XRD法测定析晶结构，并测定窑具的抗折强度、抗折强度保持率、气孔率、吸水率等各项性能指标，综合分析得出MnO2-CaF2混合矿化剂的最佳加入量为2%。

The glass and crystalline glass-solders of Li2O-ZnO-SiO2 system were prepared by conventional melt technology. The various factors effecting on glass ceramics and glass were investigated,which include glass chemical composition and heat-treatment and so on. And then by means of XRD, DTA, IR and SEM, the structure and properties of the glass and glass-ceramic were studied. The coefficient of linear expansion , transform temperature and soft temperature wer measured. And then the factors that effect the mechanical strength of glass-ceramic were discussed and the fluxion property was determined and the crystallization course and mechanism were discussed, which can provide certain therial reference value for practice producing and glass seals to glass, ceramics and metal.

用高温熔融法制备了Li_2O-ZnO-SiO_2系统玻璃及其结晶型玻璃焊料，探讨了各种因素(包括玻璃组成、热处理制度等)对微晶玻璃的结构和性能的影响；利用X射线衍射分析、DTA、红外光谱分析以及扫描电镜等现代测试手段，对玻璃的结构与性能进行研究，测定了玻璃及微晶玻璃的线膨胀系数、转变温度和软化温度，同时对影响微晶玻璃的强度的因素进行了探讨，并对该体系玻璃的流散性进行了测定，对它的析晶过程和析晶机理进行探讨，为实际生产和与玻璃、陶瓷及金属封接提供了一定的理论参考价值。

The C-curves of the cyanided case of 18CrMnTi and 18CrMnMo steels austeni-tized at 860℃ were determined by metallographic methods.

用金相法测定了18CrMnTi与18CrMnMo钢高温氰化层经860℃奥氏体化后的恒温C-曲线与马氏体开始转变温度M_H，同时也测定了A_1温度。

The subject function values used nine indexes in tomato of high temperature stress including the rate of fruit setting, the relative output, the index of rolling leaves, the stabilization of membrane, the relative geminating of pollens, the contents of dissociating proline and the content of soluble sugar.

通过对高温下番茄的坐果率、相对产量、卷叶指数、相对生长量、膜稳定性、相对花粉萌发率、热害指数，以及游离脯氨酸和可溶性糖含量等9项指标的测定，采用隶属函数数值法，综合比较鉴定了耐高温能力不同的6个番茄品系。

In this thesis, the phase diagram of Zn-Al binary system on 10~69.5 w% was reinvestigated by using differential scanning calorimeter, X-ray diffraction and pushrod dilatometer. The process of isothermal transformation during the aging of high-Aluminum-Zinc-based alloy was studied by using differential scanning calorimetry, and the aging behavior of the alloy was analyzed at the aspect of thermal analysis kinetics. The change of microstructure which the alloy was being heated was observed on high-temperature metallurgical microscope. The microstructure and wear-friction properties were compared among the alloys treated with several different heat treatment processes, and a model for heat treatment processes was proposed based on artificial neural network,so as to predict the relationship between friction coefficient and parameters of aging treatment such as aging temperature and time.

本文采用高温X射线衍射、示差扫描量热分析、热膨胀等方法重新测定含锌量范围为10％～69.5％的Zn-Al系二元相图，利用示差扫描量热分析法，研究高铝锌基合金时效等温转变过程，并从热分析动力学的角度分析高铝锌基合金合金时效行为；使用高温金相显微镜观察合金加热时的组织变化；比较几种不同热处理工艺对高铝锌基合金显微组织与耐磨性能的影响并利用人工神经网络建立高铝锌基合金热处理工艺模型，预测合金摩擦系数随时效温度及时间变化规律。

Before the marked self-reduction of the pellets at 1 000 ℃,the high temperature strength depends on organic binder; and after that,on reduced metallic iron.

采用自制的高温抗压强度测定装置，研究了使用有机黏结剂的含碳球团在不同温度、气氛条件下高温强度随时间的变化。

And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

47：5 法老对约瑟说，你父亲和你弟兄们到你这里来了。

Additionally, the approximate flattening of surface strip using lines linking midpoints on perpendicular lines between geodesic curves and the unconditional extreme value method are discussed.

提出了用测地线方程、曲面上两点间短程线来计算膜结构曲面测地线的方法，同时，采用测地线间垂线的中点连线和用无约束极值法进行空间条状曲面近似展开的分析。