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Synthesis, Characterizations and Gasoline Antiknock Properties of Transition Metal Complexes

在环保和节能的推动下,必须有更经济高效的无铅化汽油抗爆剂来满足人们对高辛烷值汽油的需求。

Objective: To establish a simple and fast high performance method to determine trace antimony in packaging materials for food.

目的:建立简便、快速、高效的测定食品包装材料中微量锑的方法。

The method was established to analysis the oxine-copper with ion pair of antiphase HPLC and Ultrasonic-assisted solvent extraction methods.

建立了喹啉铜原药的超声波辅助溶剂提取-反相离子对高效液相色谱法的分析方法。

This article mainly established the analysis method to extract the oxine-copper residues in cucumber and soil with ion pair of antiphase HPLC and Ultrasonic-assisted solvent. This method mainly uses XBridge C18 column and UV detector by using waters phase of phosphatic buffered solution/acetonitrile (60:40, by vol) as mobile phase with 0.8 mL/min flow ratio and UV detection at 250 nm. The residue time was 4.71 minute. Accuracy, precision, and sensitivity of the method all satisfy the demands of pesticide residue analysis.

建立了黄瓜和土壤中喹啉铜的超声波辅助溶剂提取-反相离子对高效液相色谱法的残留分析方法,该方法使用XBridge C18色谱柱和可变波长紫外检测器,并以水相磷酸盐缓冲溶液-乙腈(体积比为60:40)作流动相;流速为0.8 mL/min;检测波长为250 nm;保留时间为4.71 min;该方法的准确度、精密度及灵敏度均满足农药残留分析的要求。

The ultrasonic-assisted solvent extraction and quantitative analysis of the oxine-copper residues in soil with ion pair of antiphase HPLC was established. This methods mainly uses XBridge C5 column and UV detector by using waters phase of phosphatic buffered solution/acetonitrile (60:40, by vol) as mobile phase with 0.8 mL/min flow ratio and UV detection at 245 nm. The residue time was 4.72 minute. The linear correlation of this method was 0.9987. The recovery rate was 76.2 to 108.7%. Comparatively standard deviation was 0.6 to 3.37%. The detection limits of method was 0.05 mg/kg.

建立了土壤中喹啉铜的超声波辅助溶剂提取-反相离子对高效液相色谱法的残留分析方法,该方法使用XBridge C18色谱柱和可变波长紫外检测器,并以水相磷酸盐缓冲体系-乙腈(体积比60:40)作流动相;流速为0.8mL/min;检测波长为245nm;保留时间为4.72min;线性相关系数为0.9987,回收率在76.2%~108.7%之间,相对标准偏差在0.6%~3.37%之间,对土壤的最低检出限为0.05mg/kg。

Keywords Caffeine;Antipyrine;Sodium Salicylate;Satongfeng Injection;HPLC;Determination of content

咖啡因;安替比林;水杨酸钠;撒痛风注射液;高效液相色谱法;含量测定

Under laboratory conditions 25 min after ultraviolet ray irradiation, 5% zinc oxide's protection efficiency index are 29.4%,0.1% antiscorbutic acid protection efficiency indices is only 7.4%. 4We select appropriate types and concentrations of pesticides from 4.5% alphacypermethrin EC, 20% Imidaclopr...

4.5%高效氯氰菊酯乳油, 20%虫可溶性液剂, 2%啶虫可溶性液剂作为供试农药,筛选合适的农药种类和浓度与绿僵菌混配,作为绿僵菌的增效剂。

A high level of expression of GST-NOR1 is obtained in JM 105, and its antiserum can be prepared successfully.

成功获得了高效表达NOR1基因的原核表达产物,通过对该融合蛋白的纯化为它的多抗制备奠定了基础。

High titer antiserum against mouse Foxp3 is produced and can be used to identify the Foxp3 expression in normal mouse tissues.

制备了高效价的特异性小鼠Foxp3抗血清,并可用于正常小鼠组织的Foxp3蛋白的表达鉴定,为进一步研究Foxp3奠定了实验基础。

Electronics antiskid control system is to ensure train to operate safely and efficiently.

列车电子防滑控制系统是确保行车安全和高效的重要设备。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

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