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By using ceric ammonium nitrate as the initiator, a superabsorbent polymer was prepared from graft copolymer of corn starch and acrylonitrile.

用硝酸铈铵作引发剂,通过水溶液聚合法制得了玉米淀粉接枝丙烯腈高吸水性树脂。

Using ceric ammonium nitrate as the initiator, a superabsorbent polymer was prepared from graft copolymer of corn starch and acrylamide.

用硝酸铈铵作引发剂,通过水溶液聚合法制得了玉米淀粉接枝丙烯酰胺高吸水性树脂。

The Carboxymethyl Cellulose grafted polyacrylamide was synthesized with the cerous ammonium nitrate as the initiator and the absorbent resin with excellent water absorbing abilities was produced through hydrolyzing the CMC-g-PAM.

以羧甲基纤维素为基质,以硝酸铈铵为引发剂,成功的制备了羧甲基纤维素接枝聚丙烯酰胺,进一步水解获得了具有优异吸水性能的高吸水树脂。

Preparation of the cathode includes:shaping under the press of 40Mpa, sintering at 550℃for 1 hour and at 900℃for 8 hours and threading with molybdenum bar; Considering the literatures we choose CaCl2 as salt for preparation titanium. Pretreatment of salt is for 1 hour at 100℃and for 2 hours at 300℃. Partial pressure of oxygen which need lower than 5.11×10-7Pa to reduct titanium oxides and hygroscopic property of salt need a sealed equipment to electrolyse. And finally successfully designed a satisfied one and the results show that the equipment can be satisfied the requirment of the experiment. Flow of the inert gas is 1.5L/min, the voltage is 2.8 V, temperature is 850℃and time is 2 hours during pre-electrolysis. Flow of the inert gas is 0.2L/min, the voltage is 3.1 V, temperature is 900℃and time changes with the mass of TiO2 during electrolysis, namely the greater need the longer time; To eliminate influence of salt and other impurities, the products need to wash with distilled water and dilute chlorhydric acid , then wash with dilute hydrochloric acid under supersonic wave assistant. Finally, electrometical properties of the electrolysis of TiO2 is researched by cyclic voltammetry and chronoamperometry, and results show that there are two main reodox steps, namely from TiO2 to TiO and from TiO to Ti.

阴极制备主要包括40MPa压力下模压成型、两段式烧结(1小时内升至550℃保温1小时,再1小时升温至900℃保温8小时)及烧结后TiO2块打孔用钼棒串接三个主要环节;实验中选用CaCl2作为电解熔盐,并对其进行预处理(100℃,保温1小时; 300℃,保温2小时);经热力学计算,还原钛氧化物的氧分压至少要低于5.11×10-7Pa,结合电解过程中所用熔盐CaCl2有极强的吸水性的特点,电解装置应有较高的密封性,自行设计了一套密封性可靠的电解装置,便于实验过程中熔盐预处理和氧分压的控制;通过干燥处理预电解过程中Ar流量大约为1.5L/min、电压为2.8 V、温度为850℃、时间为2小时,电解过程中Ar流量大约为0.2L/min、电压为3.1V、温度为900℃,实验结果表明电解时间与TiO2质量密切相关,质量越大需要电解的时间越长;通过自来水冲洗—稀盐酸浸泡、洗涤—在超声波辅助作用下稀盐酸洗涤,可减少熔盐及其它杂质对电解产物检测结果的影响;最后,通过循环伏安法、计时电流法对电解机理的研究,确定电解还原TiO2制备金属钛主要经历了TiO2-TiO-Ti的过程。

The common stainless steel chromic quantity is not lower than 12% generally, high even achieves 18%.

一般的不锈钢活接含铬量一般不低于12%,高的甚至达到18%。

The strain gradient, the fiber Bragg grating's reflection and the short wavelength loss decide the two stopbands. Because of having no extra loss result from coupler and no high cost result from circuitor, the band pass filter formed by single chirped fiber grating have many good characters such as little insert loss its insert loss is the fiber splice loss, small volume, low cost and excellent property, moreover there is no report about fabricating filter by using this method, thus we will apply national invent paten about the method of fabrication fiber band pass filter using single chirped fiber grating. According to the parameters linearly chirped fiber gratings of Canada BRAGG Photonics Inc.

由于没有耦合器带来的3dB的额外损耗,也没有环行器带来的高的制作成本,用单支chirped光纤光栅形成可调光纤带通滤波器具有插入损耗极小(插入损耗为光纤与光纤之间的融接损耗)、体积小、制作成本低廉并且性能优良等特点,而且国内外还未见类似制作方法的报道,我们对用单支chirped光纤光栅形成可调光纤带通滤波器这一制作方法正在申请国家发明专利。

Then, the Elman neural network was used to process quantitative and classifiable recognization.

实验结果表明,该特征提取和神经网络分类算法对于粘接质量定量识别的准确度很高。

In this thesis, it is studied that the Li2O-Al2O3-SiO2 system glass ceramics of high expansion which can be a match for the iron nickel alloy (485 alloy ) with 102×10-7/℃expansion coefficient, and influence of the change of every group compos...

本课题研究了能和膨胀系数为102×10-7/℃的铁镍合金(485合金)匹配封接的高膨胀Li2O—AL2O3—SiO2系统微晶玻璃,研究了各组份变化对微晶玻璃性能的影响。

The Multi-Point Effect in frequency domain is studied, and the analytical procedure is simplified to some extent, that is, the responding data is accurate enough only with the input according to the first four degressively arranged eigenvalue of earthquake power spectrum matrix.

对于240米高的超大型土石坝,相关程度越小,坝顶竖向永久位移和易破坏单元的损伤值越大,当竖向与水平向地震动强度接近时,这一规律更明显。时域和频域内这一规律是一致的。

The UV and IR spectroscopic studies of the monomer films showed that the photoreaction ratio of monomer (about 50%) was higher than the corresponding photosensitive polymer (about 10%, PVCi). The polarized IR spectra proved that obvious anisotropic absorption was displayed in the irradiated photosensitive film. With polarizing microscopy method, we found that these kinds of photoalignment films exhibited good alignment ability, and the stability of the photoalignment film could reach about 100℃. 2 A photosensitive self-assembled monolayer was fabricated that contained photo-cycloadditable groups, such as, coumarin and cinnamate. The reaction process were detected by contact angle method because the IR absorption of monolayer was very weak. The photosensitive self-assembled monolayer promote uniform alignment of nematic liquid crystals by LPUV, and it thermal stability could reach about 130℃. 3 A cationic bolaform amphiphiles was synthesized that had two photosensitive double bonds, and can be polymerized by ultraviolet. A layer-by-layer self-assembled deposition film was prepared in aqueous solution by using this material and poly (sodium 4-styrenesulfonate). The UV-Vis. spectra proved that the multilayers film was uniform and layer-by-layer. When LPUV irradiated the film, the photopolymerizable double bond underwent [2+2] cycloaddition, and the production of the reaction distributed along the polarized direction of incident LPUV. Polarized UV-Vis. spectra indicated that the irradiated self-assembled multiplayer film was anisotropic, and the dichromic ration is about 0.09, it is higher than the spin-coating method of photosensitive polymer or monomer. We used this anisotropic film as alignment layer of nematic liquid crystals, and obtained a uniform and stability alignment result, the static contrast ratio is about 100, which is very close to application of liquid crystal device. This thesis is an instance that the photochemical material was used in the physics region of liquid crystals, the route that was from photosensitive monomer, self-assembled monolayer film to self-assembled multiplayer film was undergone, by this logical research method photoailgnment of liquid crystal was extended and consummated.

围绕上述思路开展了如下工作:1合成了三种可进行光二聚反应的光敏小分子单体,LPUV 辐照制作了光控取向膜;用紫外-可见光谱法和红外光谱法分析了薄膜中的光化学反应,发现小分子的光反应程度可达到50%以上,至少比光敏高分子高出5倍;薄膜的偏振红外光谱证实,经过LPUV 辐照后薄膜出现了明显的各向异性;将小分子光控取向膜制成液晶器件,在偏光显微镜下观察看到均匀一致的液晶取向;并且热稳定性达到100℃左右,接近实用化要求。2制备了含肉桂酸、香豆素基团的自组装单层膜;采用接触角的方法监测自组装反应的动力学过程;紫外-可见光谱证实了自组装单层膜在石英基板表面形成;自组装单层膜经LPUV 辐照后能诱导液晶均匀取向,而且热稳定性可达130℃,热稳定性进一步提高。3合成了含有光敏双键的双季铵盐,在水溶液状态下将它和聚乙烯基苯磺酸钠沉积生成layer-by-layer 自组装多层膜,紫外-可见光谱证实这是一个逐层均匀的沉积;在LPUV 照射下,自组装膜中的光敏双键按照偏振方向发生[2+2]环加成反应,形成取向膜,用二向色性值评价的分子取向度高于高分子及小分子光控取向膜的水平;实验证明用自组装多层膜制成的液晶器件亮暗态均匀,静态对比度约为100,达到实用化器件的水平。

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Lugalbanda was a god and shepherd king of Uruk where he was worshipped for over a thousand years.

Lugalbanda 是神和被崇拜了一千年多 Uruk古埃及喜克索王朝国王。

I am coming just now,' and went on perfuming himself with Hunut, then he came and sat.

我来只是现在,'歼灭战perfuming自己与胡努特,那麼,他来到和SAT 。

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三叶草是爱尔兰和圣特里克节的标志同时它的寓意是带来幸运。3片心形叶子围绕着一根断茎,深绿色。