高压

Then using 3,4,5-trichlorobenzotrifluoride as starting material to prepare 2,6-dichloro-4-trifluoromethylaniline through three routines, The direct ammonolysis method may realize the maximum use of the atom and it meets the modern green chemistry requirement. But the reaction must carry on under the high temperature and high pressure condition, and side reaction had occurred, the conversion was high, but the yield of the product was only 68%.

直接氨解法可以实现原子的最大利用率，符合现代绿色化学原子经济性要求，但是反应需在高温高压条件下进行，且有副反应发生，原料转化率高，但所需产品的收率只有68%。

A novel synthetic approach of 3,3'-azobis(6-amino-1,2,4,5-tetrazine) was firstly devised. Taking 3,6-bis(3,5-dimethylpyrazol-1-yl)-1,2,4,5-tetrazine as a primary material, DAAT was synthesized by high pressure ammonolysis and potassium permanganate oxidation. Compared with the four-step reaction in the literature, this new approach was reduced to two steps with a yield of 58.1%. The intermediate and DAAT were characterized by elemental analysis, IR and NMR spectra.

自行设计了3，3'-偶氮双(6-氨基-1，2，4，5-四嗪)新合成路线、采用3，5-双(3，5-二甲基吡唑-1-基)-1，2，4，5-四嗪为原料，由文献报道的4步反应缩减为2步，经高压氨解、高锰酸钾氧化合成了DAAT，总收率大幅提高，达到58.1%，并采用元素分析、红外光谱、核磁共振光谱等进行了结构表征。

The obtained compound (2) was treated with borane-tetrahydrofuran (B2H6–THF) complex under nitrogen atmosphere in excessive THF for 18 h to give a kind of dark brown oil,followed by ammonolysis with NH3·H2O in autoclave at 100 ℃ for 6 h to produce 2-(5-amino-2- nitrophenyl) ethanol (3) in 84.4% yield.

用硼烷还原5-氟-2-硝基苯乙酸后，接着用氨水在高压釜中加热到100 ℃氨解，得到2-(5-氨基-2-硝基苯)乙醇（84.4%）。

Waste minimization in ammonolysis process of O,O-dimethylphosphorochloridothioate;2. An Investigation on the Micelle-Catalytic Hydrolysis and Ammonolysis of Carboxylic Acid Esters;3. The final product is generated by ammonolysis of the compound under high pressure.

以4-溴-1，8-萘酐为原料，用2，4-二甲基苯胺在醋酸中与之反应得到N-2′，4′-二甲基苯基-4-溴-1，8-萘酰亚胺，然后将NDNA在高压下用氨水进行氨解得到最终产品。

The P-wave velocity-depth profile and electrical conductivity-depth profile can be calculated from the experimental data and the fundamental geothermal parameters in northern margin of the North China craton. The comparison of the calculated results with the elastic and electrical structure of this area reveals that the v of amphibolite is approximately equal to the middle crust, the electrical conductivity of amphibolite intersects the range of the middle and lower crust in this area.

利用实验获得的弹性波纵波速度及其温度系数和压力系数以及电导率与温度的关系，结合现今华北克拉通地热学的基本参数，计算得到斜长角闪岩的弹性波纵波速度－深度剖面和电导率-深度剖面，将二者分别与华北克拉通北缘深部地壳的弹性及电性结构进行对比的结果表明：高温高压下绿泥石化斜长角闪岩的弹性波纵波速度与该地区中地壳速度相当，电导率介于中、下地壳范围内。

This group case of illness all uses scanning of scanner of CT of Lightspecd Plus helix, scanning layer is thick for 5mm, removed 5mm, CT of go ahead of the rest is smooth sweep, injector of reuse high pressure, shed vein of rate classics ancon to inject how to fire force with 3ml/s (320mgI/ml)90ml, the 65s after inject ends scans, scanning parameter 120kv, 230ma, sweep time 0.8s, rebuild with layer thick 2.5mm, removed 1.25mm.

本组病例均使用Lightspecd plus螺旋CT扫描仪扫描，扫描层厚为5mm，间隔5mm，先行CT平扫，再使用高压注射器，以3ml/s流率经肘静脉注射安射力(320mgI/ml)90ml，注射完毕后65s扫描，扫描参数120kv，230ma，扫描时间0.8s，并以层厚2.5mm、间隔1.25mm重建。

Kb, probably in the crust-mantle transition zone. The plagioclase phenocrysts are dominantly andesine with reverse zoning, and those of hornblende are Al-rich (Al2O3 ~15.9 wt%), indicative of high-pressure crystallization.

斜长石斑晶主要为中长石且具反向分带，而富铝的角闪石斑晶（Al2O3 ~15.9 wt%）也反映了高压结晶的特点。

So there need not only no failure but working in a stably good condition in the ignition system, the using condition and adjust of the use factors are the most important thing for the system performance. The paper analyses the characteristics of electronic ignition system, points out that determinant use factors are mainly the voltage of battery, the occupy-emptiness rate of the ignition signal, the clearance of spark plug, the resistance of high-voltage part, and the cam angle of spark advance.

本论文重点分析了电子点火系统故障特征，论证了决定电子点火系统性能的使用因素主要有电瓶电压、点火信号发生器发出电压信号的占空比、火花塞间隙、高压阻抗、点火提前角，这些因素在点火系使用过程中故障率占点火故障比例最大，故障出现的频率最高，而且有时常因维修调整不当导致点火系统性能变差。

The influences on gas flow and dielectric strength recovery properties, which are caused by altering the angle of elevation, the dimension and the profile of arc nozzle of SF6 circuit breaker, were investigated.

SF6高压断路器的喷口对断路器开断过程中吹弧气体的流动特性起着控制作用，从而成为灭弧室的心脏。

It is prepared by reacting anhydrous ammonia and carbon dioxide gas under very high pressure in the presence of a suitable catalyst.

它是在某种催化剂参与下，由无水氨和二氧化碳气体在高压条件下反应生成的。

In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

。但是，在否定句或疑问句里，这种带有"do"的方法表达的效果却没有什么强调的意思。

Go down on one's knees;kneel down

屈膝跪下。。。下跪祈祷