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Methods:The target compound was synthesized using 4-hydrazino-N-methyl-benzyl-sulphonamide hydrochloride and 4,4-dimethoxy-N,N-dimethyl butylamine as the starting materials,PPA and sodium dihydrogen phosphate instead as catalysts and isopropyl ether and acetone as solvents for recrylstallization,via 4-step reactions:condensation,rearrangement,cyclization and salt formtion.

以4-肼基-N-甲基-苄基磺酰胺盐酸盐与4,4-二甲氧基-N,N-二甲基-丁胺为起始原料,改用多聚磷酸和磷酸二氢钠作为催化剂,后处理采用异丙醚和丙酮作为重结晶溶剂,经缩合、重排、环合、成盐的4步反应合成琥珀酸舒马曲坦。

A slow, cadenced trot in which the horse alternately raises and returns to the ground first one diagonal pair of feet, then the other.

巴沙基,斜横步:马术中的一种慢而有节奏的步子,令马一对斜对脚与另一对交替着抬起和放下

Then the protected D-mannitol, mixed with lead tetraacetate, hippuric and acetic anhydride, were refluxed in THF for 18 h in a one-pot two step reaction to afford a chiral precursor-2-phenyl-4-[-2,3-O-]-propylidene-5(4H)-oxazolones.

产物与四乙酸铅、马尿酸、乙酐于THF中回流18 h完成一釜二步反应,纯化后得到含有手性碳原子的环丙烷氨基酸前体-2 苯基-4-[-2,3-O-]丙叉?

The synthesis of dimethyl fumarate was studied from maleic anhydride and methanol with phospho molybdic acid as the catalyst and bromate as the isomerization catalyst by one-step in this short paper.

采用固体杂多酸磷钼酸为催化剂,溴酸盐为异构化剂,经顺酐一步合成了富马酸二甲酯,探讨了醇酐比、反应时间、催化剂的量、异构化剂的量以及异构化时间对合成DMF收率的影响,并确立了最佳反应条件。

Qi Ji leaped, not ten steps; Numa drive 10, in'll work.

骐骥一跃,不能十步;驽马十驾,功在不舍。

The antiarrhythmic drug ibutilide fumarate was synthesized from aniline by methylsulfonylation, Friedel Crafts reaction, condensation, reduction and salification with an overall yield of 44%.

以苯胺为起始原料,经甲磺酰化、傅克反应、缩合、还原和成盐反应等 5步合成了抗心律失常药富马酸伊布利特,总收率 4 4 %。

He communicated to his accomplices outside the hall, who then used a computer to relay moves to him, Indian chess federation secretary D.V. Sundar said on Wednesday.

印度国际象棋协会的官员桑达尔表示,夏尔马借助此装置与待在赛场外面的同伙取得联系,后者则通过电脑将下一步的走法传递给他。

After a stop in Tuzla , his air force T – 43A took off for the 45 – minute hop to Dubrovnik on the Dalmatian coast .

然后,他的 T-43A 军用飞机又开始了前往达尔马辛海岸的杜步洛尼的历时45分钟的飞行。

The analysis of weathering crust characteristic of lower Permian Kalagang group in Malang sag, Santanghu basin suggests that the paleo-weathered crust includes weathering clay ground, strong weathering rubble layer, weak, weathering block-stone layer and unweathered rock layer in vertical and was distributed under the unconformity interface and presented in planar manner horizontally.

对三塘湖盆地马朗凹陷下二叠统卡拉岗组风化壳特征的分析,认为古风化壳纵向上分为风化粘土层、强风化碎石层、弱风化块石层以及未风化岩石层等,平面上呈面状分布于不整合界面之下,剖析该区古风化壳成藏地质条件和构造演化,探讨了可能发育油气藏类型及与风化壳的关系,并指出了该区下一步下二叠统卡拉岗组有利的勘探目标是在P2t剥蚀线与P1k剥蚀线之间范围内,其次为卡拉岗组剥蚀线以东地区。

They could also push much harder to help reconcile the two Palestinian groups—and, by the by, insist that Hamas unambiguously disavows violence and, at least de facto, says it accepts Israel.

这些国家也应加大力度敦促巴方两党早日和解,退一步说,使哈马斯果断放弃暴力手段,并起码事务上承认以色列。

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The absorption and distribution of chromium were studied in ryeusing nutrient culture technique and pot experiment.

采用不同浓度K2CrO4(0,0.4,0.8和1.2 mmol/L)的Hoagland营养液处理黑麦幼苗,测定铬在黑麦体内的亚细胞分布、铬化学形态及不同部位的积累。

By analyzing theory foundation of mathematical morphology in the digital image processing, researching morphology arithmetic of the binary Image, discussing two basic forms for the least structure element: dilation and erosion.

通过分析数学形态学在图像中的理论基础,研究二值图像的形态分析算法,探讨最小结构元素的两种基本形态:膨胀和腐蚀;分析了数学形态学复杂算法的基本原理,把数学形态学的部分并行处理理念引入到家实际应用中。

Have a good policy environment, real estate, secondary and tertiary markets can develop more rapidly and improved.

有一个良好的政策环境,房地产,二级和三级市场的发展更加迅速改善。