香草醛

MethodsVanillin was used as colour developing reagent in the presence of perchloric acid.

方法利用在高氯酸的条件下香草醛-冰醋酸与三萜酸的反应测定总三萜酸。

objective:to make a comparative analysis of the total saponins content in polygalaceae phloem and xylem parts to guide clinical treatment.methods:we determined the polygalaceae total saponins content at the 575 nm with oleanolic acid as a reference substance and vanillin-perchoric acid as a developer by using uv-visible spectrophotometry.results:the total saponins content of xylem parts was 3.33%,and that of polygalaceae phloem was 0.69%.conclusion:the total saponins content in polygalaceae xylem parts is much more than that of phloem parts,the total saponins in polygalaceae mainly exists in xylem parts.

目的：对远志原药材木部及皮部中总皂苷含量进行比较分析，用以指导临床用药。方法：以齐墩果酸为对照品，香草醛－高氯酸为显色剂，采用紫外－可见分光光度法在575 nm处测定远志总皂苷含量。结果：以此方法对远志木部及皮部中总皂苷含量进行比较、分析，为远志皮部总皂苷含量为3.33 %、木部总皂苷含量为0.69 %。结论：远志中皮部总皂苷含量远远大于木部，远志总皂苷主要存在于根皮中。

The reaction mechanism was studied and the proposed methods were applied to the determination of SOD activity.Second, baded on sodium terephthalate trapping HO, an automated spectrofluorimetry for determining HO with flow injection analysis was developed. It was applied to the anti-oxidation determination of maize pollen polysaccharose and natural foods.

一设计合成了两种用于超氧阴离子自由基识别检测的荧光探针——香草醛缩-8-氨基喹啉和2-吡啶甲醛苯并噻唑啉，用普通荧光法和流动注射荧光法对超氧阴离子自由基进行分析测定，研究了反应机理，并将其用于超氧阴离子自由基和超氧化物歧化酶活性的测定。

With the new synthesized fluorescence reagent, a novel fluorescence quenching method for determination of superoxide radical was developed by coupling the reaction of pyrogallic auto-oxidation reaction.

合成了一种新的荧光探针试剂香草醛缩苯胺，利用元素分析、红外光谱等手段对探针试剂进行结构表征；结合部苯三酚的自氧化作用，建立了一种荧光法测定超氧阴离子自由基O2

RESULTS: 12 compounds were isolated and identified as aurantiamide acetate (1), aurantiamide benzoate (2), physcion (3), scopoletin (4), vanillin (5), coniferyl aldehyde (6), syringaldehyde (7), syringic acid (8), luteolin (9), apigenin (10), azelaic acid (11), dotriacontanic acid (12), respectively.

结果：从羊耳菊全草的氯仿和乙酸乙酯部分共分离得到12个化合物，分别鉴定为橙黄胡椒酰胺乙酸酯(1)，橙黄胡椒酰胺苯甲酸酯(2)，大黄素甲醚(3)，东莨菪亭(4)，香草醛(5)，松柏醛(6)，丁香醛(7)，丁香酸(8)，木犀草素(9)，芹菜素(10)，壬二酸(11)，三十二烷酸(12)。

To clarify the relationships between phenolic compounds and continuous cropping obstacle of Rehmannia glutinosa, the accumulation amounts of ferulic acid, vanillic acid, vanillin, and β-hydroxybenzoic acid in continuously cropped R. glutinosa soil were measured, and the effects of these four phenolic acids on R. glutinosa growth were studied with water culture.

为了探究酚酸物质与地黄连作障碍之间的关系，检测了重茬地黄土壤中阿魏酸、香草酸、香草醛和对羟基苯甲酸等4种酚酸物质的积累量，并通过水培条件下添加酚酸，研究了4种酚酸对地黄生长的影响。

The costuslactone and dehydrocostuslactone in the supercritical CO 2 extract of aucklandia were identified by TLC using a mobile phase of petroleum ether,ethyl acetate and benzene (70∶5∶15) and the colour developing reagent of 5% vanillic aldehyde dissovled in sulfuric acid.

用薄层色谱法，以ψ(石油醚∶乙酸乙酯∶苯)=70∶5∶1 5为展开剂，质量分数为 5 %香草醛硫酸为显色剂对木香超临界萃取物中的木香烃内酯与去氢木香内酯进行鉴别；并建立高效液相色谱法同时测定木香烃内酯与去氢木香内酯的含量方法。

Chapter three: A CE method to separate and determine the five active components, gastrodin, vanillyl alcohol, p-hydoxvhenzyl alcohol, \inllln and p-hydroxybenzyl aldehyde in Chinese herb Gastrvdiri Juiti Bl. and its preparations was developed.

第三章：建立了分析和分离中药天麻及其制剂中5种有效成分—天麻素、对羟基苯甲醇、香草醇、香草醛、对羟基苯甲醛—的毛细管区带电泳方法。

The special proportion showed 1:2～3 between vanilla aldehyde and lilac aldehyde in aged brandies.

研究发现经橡木桶陈酿的白兰地中香草醛与丁香醛之间特定的比例关系为1：2～3。

The TLC of them were concordance.They presented the same color fluorescence in the corresponding position at the ultraviolet light(365nm). After the vanillic aldehyde sulphuric acid ethanol solution developed, violet color spots presented at the same place. Reference substance of Polysaccharide presented violet color ,but in the corresponding position the crude and the prepared didn't show the spots .

生远志正丁醇部位色谱和蜜远志正丁醇部位色谱基本一致：紫外灯（365 nm）下二者在相应位置呈相同颜色荧光，香草醛硫酸乙醇溶液显色后二者在相应位置的几个斑点均呈紫罗兰色，且远志皂苷元对照品斑点呈紫罗兰色，而在与其相应位置生远志供试品和蜜远志供试品均未检视到相应斑点。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。