饱和

SM6 and SM7 of uncrystal were analyzed through GC-MS, the results showedthat SM6 main contained unsaturated fatty aldehyde with fragrance, i.e.-2,4-decadienal(58%), tetradecanoic acid (55.78%), 2-decenal(50%), Phthalic acid isobutylundecyl ester(47%), 2, 4-Decadienal(41%), 2-Undecenal (31%), 2-Methyl-Z,Z-3, 13-octadecadi-enol(18.84%), and SM7 contained saturation alkanes, i.e. 1, 2-Benzenedicarboxylic acid, butyl cyclohexyl ester(23.90%), Triacontane(22.63%),Nonacosane(21.04%), Heptadecane(18.84%), Octacosane(13.58%). Toxicological experiments were done to insure the pigment safety.

并对紫红丝膜菌色素非晶体部分的黄色油状物SM6和紫色粉末物SM7作了GC-MS分析，结果显示SM6中主要为具有香气成分的不饱和脂肪醛，其中含量较高的依次为：-2，4-癸二烯醛(58％)、十四烷酸(55.78％)、2-癸烯醛(50％)、邻苯二甲酸异丁基十一烷酯(47％)、2，4-癸二烯(41％)、2-十一碳烯醛(31％)、2-甲基-Z，Z-3，13-十八碳二烯酸(18.45％)等；SM7中主要为饱和直链烷烃，其中含量较高的依次为：1，2-苯二羧酸丁基环己酯(23.90％)、三十烷(22.63％)、二十九烷(21.04％)、十七烷(18.84％)、二十八烷(13.58％)。

Results Twenty-seven fatty acids were identified.Satisfied fatty acid were 18 species (51%),the major components were hexadecanoic,and there were 8 species odd-numbered fatty acid.

结果 共检出27种脂肪酸，饱和脂肪酸18种，占脂肪酸总量的51%，主要成分为十六酸，其中奇数脂肪酸8种；不饱和脂肪酸9种，占总量的49%，主要为亚油酸、油酸和亚麻酸。

The model is used to count several engineering example.Comparing the 2D numerical results with electrical simulations,it is proved that the seepage model can count the seepage surface and the location of search results in dam well and truly.Comparing 3D results with 2D results at close section,the results are tally well except the difference of meshes and the interceptive position of section.So the model is credible and has upper practicality value.In the projects,the spending of account is increasing because of the bigger account field.

将饱和—非饱和渗流模型用于几个工程实例，其二维模拟结果同渗流电模拟实验结果进行了对比，证明本文的渗流模型完全能够准确计算坝内的渗流浸润线以及逸出面位置；三维数值模拟的结果在相近剖面处与二维结果作了比较，考虑三维网格剖分及剖面截取位置的差异，三维结果与二维结果吻合的较好，证明本文的饱和—非饱和渗流模型在三维计算中是可靠的且具有较高的实用价值。

Thus,α,β-unsaturated ketones were prepared by base-catalized aldol condensation between substituted arylaldehydes and acetones. Using iodosobenzene diacetate as oxidants, the resulting α,β-unsaturated ketones will be transformed to β,γ-unsaturated carboxylic acid esters.

以不同取代的芳香醛跟丙酮缩合后可以得到α，β-不饱和酮，再用iodosobenzene diacetate做氧化剂氧化，可以成左卤o到β，γ-不饱和碳酸酯类化合物。

It was suggested that only if the protein is just eluted with a isocratic model.

提出了在等浓度条件下洗脱条件蛋白能够在色谱柱保留时的饱和吸附量为其有效吸附量，在这种条件下的流动相的组成，才是研究溶质饱和吸附量的合适组成。

Furthermore, the one-dimensional complexes 26 and 28 with strongπ-πpacking interactions are prepared from DMF solvent, which indicates that the traditional solvent volatilizing method could bring low-dimensional complex.4. By measuring the enthalpy changes of the liquid phase formation reaction for complexes a~e, and calculating the electronic densities of five 5-substituted derivation of isophthalic acid, we can make a conclusion that 5-substituted group changing of the ligand has a little influence on oxygen atoms of carboxyl groups.5. Fluorescence experiments of these complexes indicated that they could be used for luminescence materials in future.6. Using packing saturation rule we calculated and analyzed these series of complexes, and the results showed that the changes of complexes with changes of ligands could be explained from the rule.

在DMF溶剂中得到了具有强π-π堆积作用力的一维配位聚合物[Ln(5-NO_2-bdc)(NO_3)]Ln=Pr(26和Ho(28)，表明传统的溶剂挥发合成条件可以得到低维的配合物。4、通过配合物a～e的液相生成反应焓的测定，以及配体阳离子的电子密度计算，进一步佐证了间苯二甲酸的5位取代基变化对配体的羧基氧原子配位能力影响不大的结论。5、荧光特性表明此类配合物可以用于发光材料。6、利用堆积饱和规律对所得系列的配合物的进行计算和分析，发现随着配体的变化，配合物的变化可以从堆积饱和规律出发进行解释。

The results show that the optimal value of CoCl2 concentration is 0.2 mol/L and the maximum adsorbed amount is 19.674 mg/g onto this adsorbent. The adsorption capacity of phosphine onto CoCl2-modified ACF decreases with the increase of temperatures. The maximum absorbed amounts are 19.674 mg/g at 298 K, 13.537 mg/g at 313 K and 11.087 mg/g at 328 K, respectively. It is found that the Freundlich equation is more suitable for the description of phosphine adsorption process than the Langmuir equation. The isosteric heat of adsorption decreases with the increase of the surface loading on CoCl2-modified ACF, which means that CoCl2-modified ACF adsorbent has an energetically heterogeneous surface. Meanwhile, adsorptive phosphine removal performance may be a dominant of physical adsorption when the heat of adsorption is 16-24 kJ/mol, the CoCl2-modified ACF adsorbent will be one of the candidates for tail gas purification of airtight calcium-carbide furnace and recycle of phosphine.

研究结果表明：浸渍液浓度最佳值为0.2 mol/L，此改性ACF对PH3的饱和吸附量为19.674 mg/g；PH3在CoCl2改性ACF上的吸附量随温度升高而迅速降低，在298，313和328 K时PH3的饱和吸附量分别为19.674，13.537和11.087 mg/g；Freundlich吸附等温方程较好地模拟了PH3在改性ACF上的等温吸附；PH3气体在改性ACF上的等量吸附热随吸附量的增大而减小，表明改性ACF吸附剂表面能量的不均匀性；吸附热在16~24 kJ/mol范围内，过程为物理吸附，有利于密闭电石炉尾气的净化。

On the basis of molecular design and assembly, the polyoxometalate compounds supported by Keggin, Dawson, lacunary Keggin, and Silverton-type etc. polyanions on the basis of well-known and novel polyanions as building blocks were successfully synthesized by the hydrothermal technique, which are"decorated"or"bridged"by organic N-donor and/or O-donor ligands. The study on synthetic conditions and rules for these hybrid compounds and characterization by X-ray crystallography, spectroscopic, thermal, electrochemical and magnetic properties are carried out.

本文主要利用水热合成方法，从分子设计及组装的思想出发，借助不同N和含O的有机配体对多金属氧酸盐阴离子结构进行&修饰&或&桥连&，合成了一些以饱和Keggin结构、饱和Dawson结构、缺位Keggin结构和Silverton结构等阴离子为构筑模块的多金属氧酸盐化合物，研究了这些化合物的合成条件及规律并对它们的晶体结构、谱学性质、热性质以及磁性质进行了研究。

The Wien effects of three variable charge soils (red soil, lateritic red soil and latosol) saturated with various chlorides in electric field were different. The relative electrical conductivities of red soil saturated with various chlorides increased apparently with the increase in field strength, whereas that of latosol were almost equal to 1 in the test field strength (15 kV cm-1 to 250 kV cm-1), the increase of △EC in lateritic red soil were between that of red soil and latosol.

各氯化物饱和红壤悬液的相对电导率随着场强的增加而明显增大，且不同的氯化物饱和悬液的△EC之间差异明显；砖红壤悬液的△EC随着场强的增加没有出现变化，在所测场强下（15 kV cm -1到250 kV cm -1）各悬液的△EC都几乎为1；而赤红壤悬液中的现象处于前两者之间。

The Wien effects of three variable charge soils (red soil, lateritic red soil and latosol) saturated with various chlorides in electric field were different. The relative electrical conductivities of red soil saturated with various chlorides increased apparently with the increase in field strength, whereas that of latosol were almost equal to 1 in the test field strength (15 kV cm-1 to 250 kV cm-1), the increase of △EC in lateritic red soil were between that of red soil and latosol.

各氯化物饱和红壤悬液的相对电导率随著场强的增加而明显增大，且不同的氯化物饱和悬液的△EC之间差异明显；砖红壤悬液的△EC随著场强的增加没有出现变化，在所测场强下（15 kV cm -1到250 kV cm -1）各悬液的△EC都几乎为1；而赤红壤悬液中的现象处于前两者之间。

This paper discusses design and realizable methods of remote test output interface from logical design angle.

本文从逻辑设计的角度讨论遥测输出接口的设计及实现方法。

This also 星体投射plies to buildings, structures and geological features.

这也适用于建筑物和地质特征。