面元素

The results of the dissertation were concluded as follows:(1) It is essential to deposit a basic additive on the Mo-based catalysts for the synthesis of CH_3SH. The potassium-doped Mo-based catalysts exhibit the highest activity than that of the catalysts doped with the otherⅠA andⅡA group basic promoters. H_2-TPR and LRS characterizations suggest that the addition of a base leads to the transformation of octahedrally coordinated Mo to tetrahedrally coordinated Mo, thus leads to the split of low temperature reduction peaks. The interaction between the basic components and Mo lead to the formation of B-Mo interface phase, which are closely correlated with the formation of CH_3SH.(2) It has been found that Fe, Co, Ni and Te have evident promoting effects for the K-Mo/SiO_2 catalysts.

主要结果归纳如下：(1)在Mo基催化剂中，必须添加碱才具有可观的合成甲硫醇活性，在IA和IIA族元素中，K是最佳的碱促进剂，当K/Mo摩尔比为2，前驱体为K_2CO_3，采用共浸法制备的K-Mo催化剂活性最高。H_2-TPR和LRS表征显示，碱的加入导致表面八面体钼氧物种向四面体转化，催化剂的低温还原峰发生分裂，碱助剂与钼之间存在强相互作用形成了B-Mo"界面相"，该物种与合成甲硫醇密切相关。

It was detected that the surface is made up of mainly 4 elements: C, O, N and Al, with little P and F in abaxial leaf.

结果表明，茶树表面主要由C，O，N和Al等四种元素组成，在茶树叶远轴面还有少量的P和F。

The copper atom is in a planar coordination site of [N_2O_2] and it devites from the mean plane by only 0.80 pm. Byπ-πstacking interactions, a alabastrine structure was obtained.(2)Schiff-base complex [Cu(H_2O)]·H_2O, where H3GS is the 3-carboxyl -salicylidene glycine, was synthesized and characterized by elemental analysis, IR spectra and single-crystal analysis. The crystal belongs to monoclinic system, space group P2(1)/c, a=848.46(3)pm, b=681.54(3)pm, c=1967.16(8)pm,β=95.8210(10)°, Z=4, R_1=0.0279, wR_2=0.0724. The copper atom is in a square-pyramidal field with the base

结果表明该晶系属单斜晶系，空间群P2(1)/c，晶胞参数：a=848.46(3)pm，b=681.54(3)pm，c=1967.16(8)pm，α=90°，β=95.8210(10)°，γ=90°，Z=4，R_1=0.0279，wR_2=0.0724，Cu原子位于轻微变形的四方锥场底心，底面被氮原子、酚氧原子、甘氨酸羧基的一个氧原子和一个水分子氧原子占据，而甘氨酸羧基的另一个氧原子占据相邻分子的锥顶，因而形成一维链状结构；合成了单核双聚配合物Na_2[Cu_2_2]·2H_2O ，铜三核配合物Cu_3_2·5H_2O和铜锌异三核配合物ZnCu_2_2·5H_2O，并用元素分析，IR光谱，电子光谱和磁化率测定对配合物的组

Hot corrosion behavior of Na2SO_4 coated B-1900 alloy was studied in air at 827 and 750℃.Corrosion kinetics of the coated alloy was gravimetrically measured,and contents of water soluble ions in the reaction products were chemically analyzed.X-ray diffraction and EMP techniques were employed to determine the components and morphology of the corrosion product scale.

用涂 Na_2SO_4盐膜法研究高温合金 B-1900在827℃和750℃于空气中的热腐蚀行为，测定其腐蚀动力学曲线，用 X -射线衍射和电子探针元素面扫描方法分析腐蚀产物的相组成和成份，还对其中的水溶性离子进行化学定量分析。

It is proved that the method using the BEM to calculate the load distributions on the contact lines of involute gear pair, in which the applied load is taken in the form of a concentrated one at a single node, is not suitable. A method in which the tractions of the BEM are made to imitate the Hertzian pressure of the gear using 8 nodes isoparametric elements is introduced.

本文解决了边界元法在空间啮合副计算中存在的系数矩阵的存储，奇异单元积分的计算、表面不连续点处面力一点多值和求解未知量的线性方程组矩阵元素的计算等问题，编制了比不采用上述处理方法的一般边界单元法节省近一半内存和计算时间的适合空间啮合副的三维边界元法计算程序。

The model is composed of six primitive and six objects. The primitive elements are vertex, segment, triangle, secund quadrilateral, QTPV and DEM, respectively. And the objects are point, line, surface, volume, complex and spatial object, respectively.

模型包含顶点、线段、三角形、侧面四边形、似三棱柱体元和DEM 6个基本元素，同时包含点对象、线对象、面对象、体对象、复杂对象、空间对象等6个对象。

That clear, perpetual outline of face and limb is but an image of ours, under which we group thema design in a web, the actual threads of which pass out beyond it .

人类那轮廓分明，长久不变的面颜和肢体，不过是一种表象，在它那框架之内，我们好把种种化合的元素凝聚一团——这好象是蛛网的纹样，那织网的细丝从网中穿出，又引向他方。

The fracture morphology were found that the interface bonds between ductile α-Ti matrix and the brittle Ti〓Si〓 phases were divided, which companied with little lancinated edge and small cleavage facets.

与其它元素相比，适量的硼改善Ti-Si共晶合金的塑性最为显著（ε〓=11.5％），其断裂机制为韧性的基体与第二相之间的界面解键，伴有少量撕裂棱和小解理面，属于准脆性断裂。

Copper nanoparticles were modified by surface modifier, methyl - methylacrylate, and minified by use of fluid-flow comminuted method, the disper sity and dispersion stability of the modified copper nanoparticles as additive i n CD 15W/40 engine oil were evaluated by high velocity centrifuger; its morpholo gy and particle size were tested by TEM and XRD analysis; and its tribological p roperty in CD 15W/40 engine oil was investigated by ball on pan tribo-tester.

采用化学改性法与液流粉碎机械法对纳米铜微粒进行了表面改性和分散研究，采用高速离心机考察了表面改性后纳米铜微粒作为添加剂在CD15W/40柴油机油中的分散性及分散稳定性，采用TEM、XRD测试了表面改性纳米铜微粒的形貌及粒径大小，采用球盘磨损试验机考察了表面改性纳米铜微粒作为CD15W/40全配方调配油添加剂的摩擦学性能，用SEM、EDS观察了磨损表面的形貌、线扫描、面分布及元素含量，分析了纳米铜微粒在摩擦过程中的减摩润滑机理。结果表明：甲基丙烯酸甲酯化学改性结合液流粉碎方法处理后纳米铜微粒的粒径进一步均匀、细化，平均粒径为24nm，并在CD15W/40油中分散性好，悬浮稳定时间长。

At the same time,a tension stress is applied on theγ′phase interfaces along the direction parallel to the stress axis,which results in the lattice expansion ofγ′phase to trap the Al,Ta atoms with the bigger radius.This brings out the accumulation of the solute atoms to form the N-type rafted structure.Al,Ta atoms with bigger radius diffuse to the {100} plane to form the linked bond of the heterogeneous atoms and the stable stacking mode,this is a main reason of promoting the transformation ofγ′phase into the N-type rafted structure.And the change of the strain energy density in different interfaces of the cubical-likeγ′phase is thought to be the driving force of the elements diffusion and theγ′phase directional growth during creep.

拉伸蠕变期间，类立方γ\'相中与施加应力轴垂直的界面受水平切应力，使晶格收缩可排斥较大半径的Al、Ta原子；与应力轴平行的界面受拉伸张应力，使晶格扩张可诱捕较大半径的Al、Ta原子，由此引起的原子偏聚形成γ\'相是自由能降低的过程；其中，较大半径的Al、Ta原子扩散迁移至{100}晶面，形成异类原子结合键及稳定的堆垛方式，是促使γ\'相形成N-型筏状结构的主要原因；而γ\'相不同界面的应变能密度变化是元素扩散及γ\'相定向粗化的驱动力。

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。