非溶剂

The morphology of scaffolds shows a regular morphology at high molecular weight. Furthermore, pore size was increased with high phase separation temperature, long coarsening time, and high concentration of nonsolvent.

反之在没有非溶剂的存在下(100/0二氧陆环/水)，高分子溶液系统仅会出现固-液相分离，显示聚乳酸与二氧陆环是互溶性佳且稳定的溶液系统。

Our study indicates the pores in microspheres were formed by liquid-liquid phase separation induced by nonsolvent infiltration. The porous zone propagated inward with the increase of solidification time.

固化试验结果显示微粒内部之孔洞，为非溶剂渗入微粒中，造成液-液相分离所形成，随著以水相萃取时间之增加，孔洞往中心移动。

The phase separation behavior of different nonsolvent additives (methyl ethyl ketone, glycol methyl ether and diethylene glycol) on PPESK casting solution was studied at 20℃according the linerized cloud point correlation.

结合线性浊点关系，根据浊点滴定试验，通过三元相图研究了20℃下非溶剂添加剂(丁酮，乙二醇甲醚，一缩二乙二醇)对PPESK铸膜液体系的相分离行为。

The gel dynamics experiments showed that the gel formation law was similar with the other polymer systems, which wasrelated with dense surface under the soft coagulating condition and the thickening gel; the square of gel thickness was linear with coagulation time. The qualitative analysis of the surface puckers of fibers spun from wet spinning and dry-jet wet spinning was made. The positions where the die swell appeared were not the same and the die swell appeared at the air gap where the fiber would markedly been elongated and vary little in the coagulant, thus the surface of fiber spun from dry-jet wet spinning was more smooth. The radial component concentration gradient was responsible for the radial structure of PAN fiber spun from dry-jet wet spinning. The thicker surface with microvoid structure of

对湿纺和干湿纺进行比较表层沟槽的产生进行定性分析，原因在于孔口胀大区域出现在不同位置，在干湿纺中，溶液的孔口胀大出现在空气层，并在该区完成大部分形变，进入凝固浴后形变很小，纤维表面较为光滑；干湿纺PAN纤维径向结构存在差异，这与丝条内组分由于双扩散进行导致径向上存在浓度差异直接相关；凝固强度较大的体系，可以获得厚度较大且孔结构尺寸较小的皮层；含较少缠结的PAN原液在纤维成形后截面很圆整，但原液缠结浓度增大时成形后圆整度下降；PAN纤维成形是一个远离平衡的过程，凝固作用缓和的体系可以使成形过程靠近平衡，可获得更大尺寸的孔洞结构；原液中少量的非溶剂添加剂显著改变纤维径向结构，可获得孔洞尺寸更小和更为均一的径向结构，这与径向浓度差异的减小、分相时间的集中相关；PAN原液的成形纤维表面依赖于凝固强度；由AFM对相近凝固条件下成形的PAN膜进下

From the photophysical behaviors of 1, 3, 4-triaryl-2pyrazoline compound (TPP16) at low temperature, it can be considered that the twisted configuration between pyrazoline ring and the non-substituted phenyl group on the position 1 is the fluorescence configuration of conjugated system Ⅰ, and the twisted configuration between pyrazoline ring and P-nitrobenzene group is fluorescence configuration of conjugated system Ⅱ.

研究了1，3，4-三芳基-2-吡唑啉化合物TPP16在低温时的发光情况，发现：在低温77K下，共轭体系Ⅰ(苯基-N1-N2＝C3-苯基)在非极性溶剂中不发荧光，在极性溶剂中有较强荧光发射；而共轭体系Ⅱ(N1-N2＝C3-C4＝对硝基苄叉)在非极性溶剂或极性溶剂中均有荧光发射，表明N1所联取代基与吡唑啉环相扭曲的构象是共轭体系Ⅰ的发光构象，而对硝基苄叉与吡唑啉环相扭曲的构象是共轭体系Ⅱ的发光构象。

The method comprises the following steps of: preparing and scraping polymer casting solution on the surface of clutch gold; conducting humidification treatment on the polymer casting solution by a humidifier or conducting phase inversion in non-solvent until phase inversion occurs in the polymer casting solution and micro porous membrane is formed; making use of the electrodeposition technology to allow tin or tutania to deposit on the surface of the clutch gold; conducting thermal treatment on the clutch gold with the protection of idle gas to obtain a Li-ion battery composite cathode electrode tab.

该方法包括如下步骤：配制聚合物铸膜液，并将聚合物铸膜液刮涂在铜箔表面；利用加湿器对铜箔上的聚合物铸膜液进行加湿处理，或在非溶剂中进行聚合物的相转化，直到聚合物铸膜液发生相转移形成微孔膜；通过电沉积工艺，使锡或锡合金通过微孔膜膜孔沉积在铜箔表面；铜箔在惰性气体的保护下进行热处理，得到锂离子电池复合物负极电极片。

The application results from fluorination showed microwave heating could accelerate chemical reactions markedly. The reaction time could be shortened 50% at least than that of conventional heating. The relationship between fluorinating agents\' structure and their activity was studied systematically. In addition, an anhydrous KF with higher activity was prepared by using expansion effect of microwave heating. As we known, solvents were very important to reaction. The comprehensive study showed some less polar aromatic solvents could be used as dipolar solvents. In addition, they had better effect than dipolar solvents in some occasions, such as fluorination of chlorobenzaldehydes and chlorinated diphenyl ketones etc. The primary applications of ionic liquids were also studied which indicated reactions with ionic liquids as solvents were more efficient and simple.

研究表明，微波是一种节能高效的加热方式，在微波作用下的卤素交换氟化反应具有反应速度快、转化率高、选择性好的优点，其反应时间可较常规加热缩短50%以上；同时也系统地研究了氟化剂种类及制备方式对其反应活性的影响，并利用微波加热的膨化作用制备出了一种活性较高的KF，其活性与喷雾干燥KF相差不大；溶剂对反应具有重要的作用，在此系统地研究了强极性非质子溶剂和中等极性非质子溶剂的应用情况，发现一些中等极性的非质子溶剂如硝基芳烃和氯代芳烃类溶剂在氯代苯甲醛类化合物的氟化反应中具有比强极性非质子溶剂更好的使用效果。

As a result, dual fluorescence was observed in non-polar solvents. Long-wavelength emission was found to consist of two components:+D||A" exciplexes resulted by "harpooning effect" and +D^^A" exciplexes stablized by solvation.

研究结果表明：合成的化合物在非极性溶剂中有双重荧光的稳态发射行为；双重荧光中的长波长发射经时间分辨光谱研究为双指数发射衰减；其中的长寿命衰减是由于该类化合物在非极性溶剂中激发后经过分子内电荷转移形成了激基复合物所致，而产生该激基复合物的直接原因是由于在非极性溶剂中的&harpooning effect&所致，短寿命则来自于该类化合物激发后在溶液中发生了分子内电荷转移的直接衰减。

Results show that the morphology of HNS changes from short plane-like shape to long plane-like shape when non-solvent temperature changes from 25℃ to 50℃. The morphology comes through the variety of ellipsoid, short plane-like and club-shaped with pH value of non-solvent from acidity to neutral and finally basical, with the particle size distribution in 50-300 nm, 50-500 nm, and 50-600 nm, respectively. Ellipse plane-like and long club-shaped morphology HNS were obtained using white dextrine and sodium carboxymethyl cellulose as surfactants in non-solvent, with the particle size distribution in 50-300 nm and 50-600 nm.

结果表明：非溶剂温度由25℃升高到55℃后，HNS晶体形貌由短片状变为细长片状；pH值由酸性变化到中性再到碱性时，亚微米HNS的晶体形貌经历椭球状、短片状、棒状的系列变化，粒度分布分别处于50~300 nm、50~500 nm、50~600 nm；白糊精和羧甲基纤维素钠作为晶形控制剂修饰后的亚微米HNS晶体形貌分别椭圆片状和长棒状，粒度分布分别处于50~300 nm、50~600 nm。

The liberated freebase methamphetamine which seperates is solvent extrated with two, 75-100 ml ether portions and the ether/amine solution is first washed with 50 mls of distilled water and the ether/amine solution dried with anhydrous sodium carbonate.

The yield is 80 - 88%解放freebase分隔甲基安非溶剂extrated是两个， 75-100毫升醚部分和乙醚/胺的解决办法是第一次洗了50英里的蒸馏水和乙醚/胺溶液干燥无水碳酸钠。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了