非溶剂

In this study, nonionic surfactant sorbitan trioleate (Span 85) was modified with Cibacron Blue F-3GA to become an affinity surfactant (CB-Span 85) and to form affinity-based reversed micelles while dissolved in hexane. Since the CB molecule possesses a specific conformation that mimics nicotinamide adenine dinucleotide, it can bind strongly and specifically to a wide range of nucleotide-dependent enzymes such as dehydrogenases and kinases. Moreover, high protein transfer efficiency in the reverse micelles can be easily achieved by controlling the ionic strength of the aqueous phase.

本实验使用非离子型界面活性剂Span 85与蓝色染料分子Cibacron Blue F-3GA结合，形成具有亲和性的界面活性剂 CB-Span 85，由於CB染料分子具有与NAD+相似的结构，可与含核苷酸部位的蛋白质具有亲和力，将CB-Span 85溶於有机溶剂形成反微胞相，可有效的提高反微胞的选择率，可以只控制离子强度来调节蛋白质进出反微胞的效率。

In this work,the non\|aqueous carbonyl nickel slips were prepared by ball\|milling using Cyclohexanone\|butyl alcohol,Glycerol trioleate,Poly\|vinyl\|butyl and polyethylene glycol as the solvent,dispersant,binder and plasticizer,respectively.

本文以环己酮丁醇为溶剂，三油酸甘油酯为分散剂，以聚乙烯醇缩丁醛为粘结剂，聚乙烯乙二醇为增塑剂，通过球磨工艺制备了非水基羰基镍粉浆料。

Duplex cold crystal peak was also observed in the DSC of PET by vapour of unactive solvents.

双冷结晶峰现象在一些非反应性溶剂处理过的PET试样的DSC曲线也观察到。

The grafting effect and mechanism was charac- terized by FTIR,The heat stability of unvulcanized and dynamical mechanical proper- ty of vulc- lcanizates of SBR and SBR-g- were tested by TG and DMA respectively. medium-resistance properties of SBR and SBR-g- vulcan- izates were also investigated.The results showed that addition of St accelerated GMA grafting onto SBR and control the decomposition of SBR. When the conditions were GMA/St/DCP was 8/4/0.3 and grafting temperature was 160℃.

结果表明，St对提高接枝率、抑制SBR的降解起到了积极的作用；SBR中聚丁二烯的α－H和双键共同参与了GMA/St熔融接枝反应；当SBR/GMA/St/DCP=100/8/4/0.3、接枝温度为160℃时，SBR的接枝率较高（23.78%），SBR–g–硫化胶的拉伸强度和撕裂强度比SBR硫化胶的分别提高了119%和27.4%；SBR–（GMA--co-St）未硫化胶的Tg比SBR未硫化胶的高，而耐热分解性能优于SBR未硫化胶；SBR–g–硫化胶在低温条件下的刚性增大、弹性降低、具有较低的内耗，在常温下的阻尼性能较高，但弹性性能保持较好；SBR–g–硫化胶的耐热稳定性以及耐非极性有机溶剂的性能优于SBR硫化胶。

The "water pool" in reverse micelle is formed by surfactant spontaneously arraying in non-aqueous solvent. This provides an excellent micro-reactor for the preparation of nanoparticles.

表面活性剂会在非水溶剂中自发排列形成纳米尺寸的&水池&，这为纳米粒子的制备提供了优良的微反应空间。

With the assumption that the electrostatic field strength of met a l chelates can be measured by the ratio of electronegativity vs.

在C18柱上试验以各种有机溶剂洗脱金属螯合物，最终选择了甲醇-丙酮的非水体系作流动相。

The reaction can be carried out in a non-aqueous solution and 4-aminopyridine can be diazotized with this method.

这个方法表现出如下优点：1），整个重氮化与偶联反应均在非水溶剂中进行；2），改变原料不同投料比，可以分别得到含有一，二，四偶联产物为主的反应产物；3），可以合成在酸性水溶液中不易重氮化的4-氨基吡啶的偶氮化合物。

Compounds 3a-3d, 4a-4d, 5a-5d, 6a-6e and 7a-7e were prepared with a new efficient method, in which the aromatic amines were diazotized with isoamyl nitrite in EtONa/EtOH under refluxing condition, and mono -, bis -and tetrakis -substituted calix [4] arenes were obtained respectively as main product by diazo-coupling in different molar ratio to calix [4] arene.

一，提出了一个有效的新方法合成含有芳香偶氮基团的杯[4]芳烃衍生物3a-3d；4a-4d；5a-5d；6a-6e和7a-7e：即在非水溶剂乙醇中用亚硝酸异戊酯，在强碱乙醇钠存在下对芳香胺进行重氮化，得到芳香重氮酸盐沉淀，过滤，然后加入杯[4]芳烃的四氢呋喃溶液，通入CO〓气体调节溶液的pH值为7-9，使其发生偶联反应。

It might be due to unpolar solvent C6D6 disfavoring the charge separation of CTC, leading to no ion radical and no polarization either.

非极性溶剂C6D6不利于CTC的电荷分离，不能形成离子自由基对中间体，因此无极化现象。

Methods Anhydrous acetic acid as solvent, 0.1 mol/L perchloric acid as titrant, crystal violet solution as indicator to establish non-aqueous titrations and ODS column as stationary phase, methanol and a mixture of 0.025 mol/L sodium phosphate monobasic and 0.02 mol/L sodium dedecyl sulfate (80:20) adjusted with phosphoric acid to a pH (4.8±0.1J as mobile phase, 220 nm as detective wavelength to establish HPLC-UV method for determination of piperazinylethylestrone drug substance; FMOC-CL as a derivatization reagent, FD as a detector to establish an HPLC method with derivatization and column switching for determination of piperazinylethylestrone in dog plasma.

分别采用无水冰醋酸为溶剂，0.1mol/L高氯酸为滴定液，结晶紫指示液指示终点的非水滴定法和HPLC-UV法测定哌嗪雌酚酮原料药含量；以FMOC-CL为衍生化试剂，采用柱切换柱前衍生化萤光检测的HPLC法测定狗血浆中哌嗪雌酚酮含量。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。