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It was found that because of the difference in component distribution and structure, the tendency that pores furcate and bend was smaller in amorphous precursor than in crystalline precursor, and for the amorphous precursor, the velocity of Al leaching-out and the expanding of specific surface area of catalyst were more sensitive to activation process parameters.

结果发现,由于两者在组元的分布及结构上的差异,非晶态前置体合金在活化过程中形成的微孔发生弯折、分叉的倾向要小于晶态前置体合金,同时前者在活化过程中的抽Al速率、以及所得到的催化剂的比表面积等对活化工艺更为敏感。

In addition, by using bondtype and polyhedron cluster type index methods to analyze the transformation of the microstructure, not only the key role of icosahedron in amorphous formation and stability can be explained, but also the solidification processes and the configuration characteristic of amorphous metals understood deeply.

此外采用键对及原子多面体类型指数法对凝固过程中微观结构组态变化的分析,不但能说明二十面体结构在非晶态合金形成和稳定性中所起的关键作用,又有助于对液态金属的凝固过程、非晶态结构特征的深入理解。

This damping mechanism well showed the damping properties of Zn-27Al alloys after modification, solution treatment and natural ageing were advanced for the increase of the phase interface and is's movability.

上述微观机理充分揭示了变质固溶时效后的Zn-27Al合金由于组织细化及非共格可动界面的增多,使合金阻尼大大提高的原因。

Rom forging to rolling, from sheet metal to titanium Simufact.forming has been developed to support in all forming applications, independent from process temperature, machine used or material processed: closed die forging or extrusion, drawing, upsetting, bending or free forging, flat rolling, profile rolling or tumbling cold, hot or semi-hot, mechanical press, hammer or screw press, rolling machine or orbital forging even coupled processes and spring-controlled tools, simple low-alloyed or stainless steel , aluminium or non-ferrous metal, titanium or nickel based alloys, massive or sheets, material flow or dieload analysis Simufact.forming is the integrated simulation environment for the optimization of all forming processes.

orming已经成功研制可支持目前所有制造业的软件应用程序,并可独立的仿真金属温度,机体使用情况或材料的处理:封闭模锻或挤压,钢绘,镦,弯曲或自由锻造,轧制,型材辊压或翻滚-冷,热或半热,机械压力机,锤或螺旋压力机,辗机或轨道锻造-更可加上流程以及spring-controlled工具,简单的低合金或不锈钢,铝或非铁金属,钛镍合金,大规模工程或床单工程,物质流或dieload分析。

Closed die forging or extrusion, drawing, upsetting, bending or free forging, flat rolling, profile rolling or tumbling cold, hot or semi-hot, mechanical press, hammer or screw press, rolling machine or orbital forging even coupled processes and spring-controlled tools, simple low-alloyed or stainless steel , aluminium or non-ferrous metal, titanium or nickel based alloys, massive or sheets, material flow or dieload analysis

Forming已经成功研制可支持目前所有制造业的软件应用程序,并可独立的仿真金属温度,机体使用情况或材料的处理:封闭模锻或挤压,钢绘,镦,弯曲或自由锻造,轧制,型材辊压或翻滚-冷,热或半热,机械压力机,锤或螺旋压力机,辗机或轨道锻造-更可加上流程以及spring-controlled工具,简单的低合金或不锈钢,铝或非铁金属,钛镍合金,大规模工程或床单工程,物质流或dieload分析。

The precision lapping technology to machine the copper substrate using semi-fixed abrasive plate was studied. The surface roughness and material removal rate as the evaluation of indicators, the influences of the different lapping parameters on the surface roughness and material removal rate were discussed and analyzed. Experimental results indicated that the copper substrate could be efficiently machined by semi-fixed abrasive plate of 800(superscript #) SiC abrasive, and the initial roughness Ra of a machined surface could be improved from 0.553μm to 0.28μm in 10min, produced an ideal rarely scratch surface. Then processed copper polished by diamonded grinding paste, it could be satisfied for the Ni-Pd-P alloy thin film growth.

主要研究半固着磨具精密研磨非晶态Ni-Pd-P合金薄膜铜片衬底,以铜片衬底的表面粗糙度和材料去除率为评价指标,探讨了研磨过程中不同的工艺参数对铜片表面粗糙度和材料去除率的影响结果表明:用800 SiC半固着磨具对铜片衬底进行研磨加工,10min后铜片表面粗糙度Ra可由0553μm减小到0.28μm,同时表面无深划痕:加工后的铜片再经金刚石研磨膏抛光可快速获得满足Ni-Pd-P合金薄膜生长用的铜片衬底表面。

The results show that ordered phases precipitated and formed a pseudobinary system; precipitated earlier than g phase by a congruent ordering + spinodal decomposition mechanism and thus produced a nonstoicheometric ordered phase, then the nonstoicheometric g phase precipitated by a non--classical nucleation and growth mechanism at the boundaries of phases, meanwhile, both of them transformed to stoicheometric ordered phases.

研究发现该合金沉淀过程中,析出D022结构的(Ni3V)相和L12结构的Ni3Al相,二者构成伪二元系;相先于相析出,相的沉淀机制为等成分有序化+失稳分解,相在相的相界处非经典形核,二者均先形成非化学计量比有序相,之后向化学计量比有序相转变;随Al浓度增加,相析出变慢,所占比例减少,而相反之,析出越来越早且所占比例增加。

The results showed that adding Sc to the alloy could cause the transformation of phase structure and the composition of the pre-separation phase in the transitional region of the quintary alloy.

6Al10Ti5五元锆基块体非晶态合金在非晶态-晶态过渡区中先析相的相结构及组织形态。

Based on the design of the interfacial free energy, the positive heat of formation, which is an unfavored factor for alloying, could be overcome for forming amorphous alloys in those equilibrium immiscible binary metal systems, thus confirming the thermodynamic model for metallic glass formation proposed previously by this research group.

二、通过界面能的设计可以克服正生成热的不利影响而制备出非晶态合金,论证了本研究组提出的非晶化相变的热力学模型的合理性。

This makes Ni-W-P powder more suitable for partial hydrogenation of dienes. The kinetic results suggest there are some different between the active sites of Ni-P and Ni-W-P powder. DSC, XRD and EXAFS results suggest that the tungsten codeposition makes Ni-W-P powder more amorphous than Ni-P powder.

动力学结果表明在两种合金微粒上,不仅环戊二烯与环戊烯的相对配位能力不同,而且它们各自的反应速率常数也不一样,表明非晶态Ni-P、Ni-W-P合金微粒的催化活性中心存在着一定的差异。

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