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In addition, IR-spectra of DNA and DNA-indirubin adduct imply indirubin interacts with the phosphate groups of DNA by hydrogen bond or electrostatic interaction.

另外,在最优化条件下,靛玉红峰电流的降低与DNA的浓度在一定范围内存在良好的线性关系,以此进行了DNA样品回收率的测定,结果满意。

Objective:To establish a HPLC method of Indirubin in Folium Isatidis.

目的:建立大青叶药材中靛玉红的含量测定方法。

Odoquinazolin-4(3H)-one,7-methyl-4(3H)-quinazolinone,7-bromoquinazolin-4(3H)-one were synthesized by using anthranilic acid、2-amino-5-nitrobenzoic acid、2-amino-4-nitrobenzoic acid,6-nitro--4(3H)-quinazoline-one、o-amino-terephthalic acid, 2-amino-4-hydroxy benzoic acid、2-amino-5-bromo-benzoic acid、2-amino-5-iodine acid,1、4-butynediol、L-glutamine、isatin anhydride、formamide as starting materials and utilizing microwave-assisted synthetic approach.

本文利用微波辅助合成的方法,以邻氨基苯甲酸、2-氨基-5-硝基苯甲酸、2-氨基-4-硝基苯甲酸、邻氨基对苯二甲酸、2-氨基-4-羟基苯甲酸、2-氨基-5-溴苯甲酸、2-氨基-5-碘苯甲酸、5-甲基-2-氨基苯甲酸等为原料与甲酰胺反应,以及以1,4-丁炔二醇、L-谷氨酰胺与靛红酸酐反应,共合成了13个喹唑啉酮衍生。。。

Methods: According to the degree of color change, the ozone in the ambient air causes the indigo disulfonic acid sodium discoloration response a new colorless production.

空气中的臭氧使吸收液中蓝色的靛蓝二磺酸钠褪色,生成无色靛红二磺酸钠,根据颜色减弱程度比色定量。

Based on the analysis and comparison of various methods of mensuration of effective ingredients of indigowoad root,phenol-vitriolic colorimetry has been choosen to be the method of mensuration of amylose in indigowoad root, and standard amylose graph has been made,in which c=22.476A+0.5309, correlation rate r=0.9970; Direct colorimetry has been choosen to be the method of mensuration of indigotin and Indirubin,and based on all above,the maximal absorb wavelenghes of indigotin and Indirubin have been determined through experiment.

在分析比较各种板蓝根有效成分测定方法的基础上,选用苯酚-硫酸比色法作为板蓝根多糖的定量测定方法,作山了多糖的标准曲线:c=22.476A+0.5309,其相关系数r=0.9970;选择直接比色测定法作为靛蓝、靛玉红的测定方法,并在此基础上通过试验确定了靛蓝、靛玉红的最大吸收波长及显色稳定性。

Using the crystal structure of CDK2 complexed with indirubin-5- sulphonate as the template, models of CDK4 complexed with indirubin and its analogue were built by homology modeling and molecular docking.

以获得晶体结构的CDK2与5-磺酸根-靛玉红的复合物为模板,通过同源模建和分子对接的方法构建出的CDK4与靛玉红及其衍生物的结合模式。

Huapai products:pchlorophenol,ochlorophenol,2,4dichlorophenol,2,6dichlorophenol,2,4,5trichlorophenol,2,4,6trichlorophenol,4chloro2benzyl phenol,pbromophenol,2,4,6tribromophenol,1chloro4(1,1dimethyl ethyl) benzene ether,3bromoanisole,mbromofluorobenzene,2tetra hydrofuran,αbromo4chloro acetophenone,αbromo4methoxy acetophenone,4chloro benzophenone,4chloro2methylaniline,n(2hydroxyethyl)ethane diamine; n(2aminoethyl)ethanolamine,2,3dibromopropionyl chloride,4bromo benzene sulphonyl chloride,terephthaloyl chloride,isophthaloyl chloride,nchlorosuccinimide,nbromosuccinimide,pchloranil;tetrachloro1,4benzoquinone,5chloroisatin.

华派公司产品:对氯苯酚,邻氯苯酚,2,4二氯苯酚,2,6二氯苯酚,2,4,5三氯苯酚,2,4,6三氯苯酚,4氯2苄基苯酚,对溴苯酚,2,4,6三溴苯酚,对氯苯基叔丁基醚,间溴苯甲醚,间溴氟苯,α溴甲基四氢呋喃,α溴代4氯苯乙酮,α溴4甲氧基苯乙酮,4氯二苯甲酮,4氯2甲基苯胺,N(2羟乙基)乙二胺, 2,3二溴丙酰氯,对溴苯磺酰氯,对苯二甲酰氯,间苯二甲酰氯,N氯代丁二酰亚胺,N溴代丁二酰亚胺,四氯苯醌,5氯靛红

The method has high sensitivit,it is based on the nitrite catalysed discoloring reaction of indigo carmine by potassium bromate in phosphoric acid medium.

基于磷酸介质中NO-2催化溴酸钾氧化靛红的褪色反应,建立了测定痕量NO-2的新方法,并讨论了其动力学条件。

The polypyrrole film modified electrodes incorporated with redox indicator indigo carmine were prepared firstly. The influence of polymerization conditions on the electrochemical behavior of resulting films was studied in detail. The films were characterized by XPS, SEM and UV-Vis spectra.

本文首次制备了掺杂氧化还原指示剂靛红的聚吡咯膜修饰电极,研究了聚合条件对所得膜电化学行为的影响,并用XPS,SEM,UV-Vis光谱等手段进行了表征。

Methods Indirubin, cholic acid and borneol were identified by TLC. The content of indirubin and cholic acid was determined by HPLC.

采用薄层色谱法鉴别靛玉红、胆酸、龙脑;采用高效液相色谱法测定制剂中靛玉红和胆酸的含量。

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