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25% arketai water dispering agent, 70% imiler water dispering agent, 4.5% high active cypermethrin emulsifiable solution and 20% haoniandong emulsifiable solution had strongest toxic effect on Coccinella septempunctata. 10% liuyangmycin and 1.1% matrine powder had weakest toxic effect, which should he avoided in production.

结论]25%阿克泰水分散剂、70%艾美乐水分散剂、4.5%高效氯氰菊酯乳油和20%好年冬乳油对七星瓢虫的毒杀作用最大,生产中应尽量避免使用。10%浏阳霉素和1.1%苦参碱粉剂的毒杀作用最小。

ABSTRACT Objective To apply near infrared diffuse reflectance spectrophotometry and chemometrics for the quantitative analysis of azithromycin dispersible tablets.

目的 应用近红外漫反射技术和化学计量学的方法对阿奇霉素分散片进行定量分析。

The majority children with MPP are 1 to 3 years of age. The extrapulmonary complications can occur in multiple systems. The test of serum MP-IgM should be conducted for early diagnosis.

儿童MPP好发于婴幼儿,肺外并发症可累及多个系统,血清学MP-IgM检测是早期诊断的必要手段,阿奇霉素是有效的治疗药物。

The majority children with MPP are 1 to 3 years of age. The extrapulmonary complications can occur in multiple systems. The test of serum MP-IgM should be conducted for early diagnosis. Azithromycin is an effective agent to treat MPP.

儿童MPP好发于婴幼儿,肺外并发症可累及多个系统,血清学MP-IgM检测是早期诊断的必要手段,阿奇霉素是有效的治疗药物。

After avilamycin 8mg/kg was fed to Cyprinus carpio, the quantity of the intestinal aerobic and the facultative anaerobic bacteria, the percent of Enterobacteriaceae, and the quantity of Lactobacillus decreased significantly on the 14~ d, at the same time , the percent of Flavobacterium increased evidently, the quantity and percent of Bacteriodes decreased evidently during the first 28 d of the experiment.3 After Cyprinus carpio was fed with narasin, the percent of Corynebacterium increased.

投喂阿维拉霉素8mg/kg在试验第14d使鲤肠道好氧及兼性厌氧菌总数、肠杆菌科所占百分比、乳杆菌属数量显著降低,黄杆菌属所占百分比显著升高;在试验的前28d使拟杆菌属数量及其百分比显著下降。

The chromatographic conditions were as followed: C8 column, 0.045 mol/L ammonium phosphate monobasic solution∶acetonitrile (2∶1)(adjusted to pH7.35 with triethylamine) as mobile phase, temperature: 40℃, the flow rate: 1.0 ml/min, detection wavelength: 210nm.

采用C8柱,以0.045mol/L磷酸二氢胺溶液∶乙腈(2∶1)(用三乙胺调pH至7.35)为流动相,流速1ml/min,检测波长210nm,柱温40℃。结果阿奇霉素的线性范围为50.3~1006μg/ml,平均回收率100.1%,r=1.0000,RSD=0.8%(n=9)。

The chromatographic conditions were as followed: C8 column, 0.045 mol/L ammonium phosphate monobasic solution∶acetonitrile (2∶1)(adjusted to pH7.35 with triethylamine) as mobile phase, temperature: 40℃, the flow rate: 1.0 ml/min, detection wavelength: 210nm.

采用C8柱,以0.045mol/L磷酸二氢胺溶液∶乙腈(2∶1)(用三乙胺调pH至7.35)为流动相,流速1ml/min,检测波长210nm,柱温40℃。结果阿奇霉素的线范围为50.3~1006μg/ml,平均回收率100.1%,r=1.0000,RSD=0.8%(n=9)。

ABSTRACT Objective To establish an HPLC method for the determination of azithromycin powder.Method The chromatographic conditions were as followed: C8 column, 0.045 mol/L ammonium phosphate monobasic solution∶acetonitrile (2∶1)(adjusted to pH7.35 with triethylamine) as mobile phase, temperature: 40℃, the flow rate: 1.0 ml/min, detection wavelength: 210nm.

阿奇霉素为氮杂内酯类抗生素,日抗基和《中国药典》2005年版[1]均采用微生物检定法测定其含量,《欧洲药典》4.6版和USP26版中均采用HPLC法,专属性较强,试验周期短,但均使用的是聚合物极性柱,《欧洲药典》柱温为70℃,USP采用电化学检测器,其采用的设备在我国药检部门尚未普及[2]。

Anhui Institute for Drug Control, Hefei 230051ABSTRACT Objective To establish an HPLC method for the determination of azithromycin powder.Method The chromatographic conditions were as followed: C8 column, 0.045 mol/L ammonium phosphate monobasic solution∶acetonitrile (2∶1)(adjusted to pH7.35 with triethylamine) as mobile phase, temperature: 40℃, the flow rate: 1.0 ml/min, detection wavelength: 210nm.

阿奇霉素为氮杂内酯类抗生素,日抗基和《中国药典》2005年版[1]均采用微生物检定法测定其含量,《欧洲药典》4.6版和USP26版中均采用HPLC法,专属性较强,试验周期短,但均使用的是聚合物极性柱,《欧洲药典》柱温为70℃,USP采用电化学检测器,其采用的设备在我国药检部门尚未普及[2]。

Objective To observe the clinical value of famotidine and pectic bismuth plus kalamycin and amoxicillin for the treatment of digestive ulcer with positive helicobacter pylori.

目的 观察法莫替丁、果胶铋、克拉霉素和阿莫西林联合治疗幽门螺旋杆菌阳性消化性溃疡的临床价值。

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