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In the same time, water-soluble bidental phosphines ligand BISBIS sulfonated 2,2''-bis(diphenylphosphinomethyl-1,1''-biphenyl was synthesized, and water-soluble rhodium complex Cl was synthesized in situ. This complex which was used as catalysts to catalyze the hydrogenation of avermectin was also tested. Although the rhodium complex containing bidentate phosphine BISBIS showed a higher catalytic activity than one containing TPPDS, the selectivity for ivermectin was lower. How to improve the selectivity will be needed to studied in futur.

同时我们用磺化的2,2''-二-- 1,1''--联苯,以及它们的水溶性威尔金森型铑配合物和环辛二烯的阳离子铑配合物,在利用这些配合物作催化剂,考察它们在各种反应条件下对阿维菌素的选择加氢,由于反应条件以及复合催化剂体系的组成还需要进一步优化,虽然双齿膦配合物显示了较高的活性,然而选择性还有待进一步提高。

As a result these types of fibre not only keep their own fine traits,but also own good conglomerating structure ,crystal limit ,calorifics performance and mechanics performance. Compared with the ordinary fiber ,the neatness of high-contracted polyester fiber increases and it s diameter also increases.

在力学分析方面:我们得到阳离子可染的涤纶纤维的于态断裂比强度较一般涤纶棉纤维的有所降低,断裂伸长反而上升:高收缩涤纶棉纤维干湿态的断裂强力和断裂伸长都较一般涤纶棉纤维的有所降低。

The network is based on a W〓Cu〓 cube-like unit with eight 〓 anions at the corners of the distorted cube and twelve 〓 cations at the middle of the edges, in which a coordination anion 〓 acting as template is capsulated in the cavity of the W〓Cu〓 cube.

该结构中的基本单元可看成是一个类似立方体的W〓Cu〓结构,其中八个〓阴离子位于立方体的顶角,十二个〓阳离子处于立方体的边上,并且有一个〓阴离子作为模板被包裹在此立方体所形成的空腔中。

This thesis studies the volcanic tectono-petrofacies, petrology, mineralogy, geochemistry, isotopic chronology, stratum and high-precision SHRIMP zircon U-Pb datings of the Mt.Yandangshan volcano-intrusive complex, and concludes that: Yandangshan volcanic rock units belong to high-K calc-alkaline acid rock associations, mainly ryholitic and trachytic dacitic in composition. They have A/CNK values of 0.9-1.2 (i.e., aluminium saturation and supersaturation), enriched LREE and LILEs and depleted HFSE. Their 8Eu values are 0.11-0.32, indicating a evident fractional evolution of plagioclase crystallization. Their ∑REE varied very limitedly,(87~Sr/(86)Sri ratios and eNd values are 0.7086~0.7095 and -10.20~-9.96 for volcanic rocks, and 0.7087~0.7095 and -7.6~6.92 for the central intrusive facies syenite, which means that all the igneous rocks from Mt. Yandangshan are evolutional products of magmas with the same source, and that they derived mainly from crust, but mixed with mantle components.

本文从火山构造岩相学、岩石学、矿物学、地球化学、同位素年代学、地层学等方面出发,同时结合高精度SHRIMP锆石U-Pb定年,对雁荡山火山岩进行了系统的研究,确定雁荡山火山岩为一套以流纹质和粗面英安质为主体的高钾钙碱性酸性岩石组合,A/CNK值集中在0.9~1.2之间,为铝饱和或铝过饱和类型;富轻稀土元素和大阳离子亲石元素、相对亏损高场强元素:负铕异常明显,δEu值为0.11~0.32,表明岩浆经历了以斜长石为主的强烈结晶分异作用:岩石样品的∑REE变化有限,火山岩样品的~(87Sr/~(86)Sr_i为0.7086~0.7095,εNd为-10.20~-9.96,中央侵入体石英正长岩~(87Sr/~(86)Sr_i为0.7087~0.7095,εNd为-7.6~-6.92,表明它们是同源岩浆分异演化的产物,物质来源主要为陆壳,但有地幔物质参与。

Research had also been carried out upon the release circumstance of daphnetin contained in the vesicles in simulated gastric and intestinal fluid.

选择生理上能接受的2种表面活性剂,即仿生磷酯阳离子表面活性剂PTA与阴离子表面活性剂SDS,按一定比例复配能自发形成稳定性囊泡,用负染色透射电镜和动态光散射对其进行表征,并以其作为药物瑞香素的载体开展其组成、温度对包封率的影响,以及在模拟胃液及模拟肠液中的释放情况的研究。

The formation and characters of the vesicles were demonstrated by negative-staining TEM and dynamic light scattering. Using the vesicles as the delivery of daphnetin, we carried out the research on the effect of formation and temperature upon entrapment efficiency. Research had also been carried out upon the release circumstance of daphnetin contained in the vesicles in simulated gastric and intestinal fluid.

选择生理上能接受的2种表面活性剂,即仿生磷酯阳离子表面活性剂PTA与阴离子表面活性剂SDS,按一定比例复配能自发形成稳定性囊泡,用负染色透射电镜和动态光散射对其进行表征,并以其作为药物瑞香素的载体开展其组成、温度对包封率的影响,以及在模拟胃液及模拟肠液中的释放情况的研究。

The relaxation modulus, the relaxation time spectra and the structure parameters C 1 and C 2 in the WLF equation were derived from the dynamic mechanical temperature spectra of the cationic dyeable PET fibres after heat setting.

对热处理的阳离子可染改性涤纶测得的动态力学温度谱,求得松弛模量,应力松弛谱以及WLF方程中的结构常数C1和C2,分析了试样超分子结构的变化,说明了热处理工艺改善纤维可染性的机理。

By the measurement of content of alkalinity degree and total iron, the product is indicated to be a kind of liquid with high alkalinity degree. The product shows the characteristic of electrolytical and is adapt to applying in wastewater treatment with fine physical property. It is without deposition in three months and mixed with water by unlimited scale.

2对产品的盐基度含量和总铁含量进行了测定,结果表明:实验室制备的产品是一种盐基度含量比较高的液体产品,在水溶液中呈现阳离子聚电解质的特性,产品的物理性质良好,三个月内无沉淀,与水可以以任何比例混合,适合于在废水处理中的应用。

Since the molecular clip of glycoluril is also an important supramolecular host but few studies have been done in the field of fluorescent chemosensor,we proceeded with some experiments and research in this field as a trial and designed a series of novel fluorescent chemsensors including different three-dimensional cavities by introducing the fluorophores into the receptor.Their recognition and sensing abilities toward various metal ions and neutral guests were studied.

因此,我们(来源:A1dBC论文网www.abclunwen.com)做了一些尝试性的研究,在传统的甘脲主体化合物上引入荧光发色团,设计了一系列新型的、拥有不同立体空腔的荧光分子夹,并研究了它们对各种金属阳离子以及酚类中性客体分子的识别和荧光传感性能。

After extraction by ethanol and purification by cationic ion-exchange column, a method of using reversed-phase high-performance liquid chromatography and precolumn derivatization with o-phthalaldehyde and 9-fiuorenylmethylchloroformate is employed for determination of free amino acids in tobacco . This method assures that amino acids with amino and imino groups can be determined simultaneously. The results of duplication experiment and recovery experiment are acceptable.

本试验用乙醇提取烟叶中的游离氨基酸,并用阳离子交换树脂纯化,再用邻苯二甲醛、氯甲酸芴甲酯联合柱前衍生、反相高效液相色谱分析测定了烟叶中的游离氨基酸,该方法能同时测定烟叶中的带氨基和亚氨基基团的氨基酸,并且分析方法的重现性和回收率均令人满意。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。