间苯二酚

At different reaction times, some primary products (such as catechol, resorcinol, hydroquinone etc.) failed to be detected

在不同反应时间，某些初级产物(如邻苯二酚、间苯二酚、对苯二酚等)没有检测到，

With the addition of hexamethylenetetramine, an ambient pressure drying technique was developed for the fabrication of resorcinol-formaldehyde-based carbon aerogels.

以间苯二酚和甲醛为反应物、六次甲基四胺HMTA为催化剂、去离子水为溶剂，所合成的间苯二酚－甲醛凝胶能够在常压条件下直接进行干燥得到有机气凝胶；并经炭化，得到炭气凝胶。

The proposed method is based on the inhibitory effect of resorcinol on the reaction of potassium periodate oxidation of pyronine Y in phosphoric acid medium.

在磷酸介质中，痕量间苯二酚对高碘酸钾氧化吡咯红 Y使其荧光猝灭具有抑制作用，据此建立了动力学荧光法测定痕量间苯二酚的新方法。

Six calix[4]recorcinarenes are synthesized by the reaction of resorcin as substrates with six aromatic aldehydes, respectively.

以间苯二酚为反应底物，分别与六种芳香醛合成了相应的杯[4]间苯二酚芳烃，并通过红外光谱和氢核磁共振谱对这些化合物进行了表征。

The suitable synthesis conditions were defined as follows: the molar ratio of DCPP and resorcin was 2.1:1;the dosage of catalyst made by myself was 1.5% of the amount of the resorcinol;the first reaction temperature was 120～130℃,the reaction time was about 60min,the second reaction temperature was160～170℃,the reaction time was 60min,the third reaction temperature reaches to 210～220℃ for removing the unreacted phenol and superfluous DCPP.

确定了反应的最佳工艺条件：DCPP和间苯二酚的物质的量之比为2.1：1；使用自制的催化剂，用量为间苯二酚质量的1.5％；起始反应温度为120～130℃，反应时间约为1h；第二步反应温度为160～170℃，反应时间约为1h，最后把温度升到210～220℃除去残留在产品中的苯酚和过量的DCPP，产品收率约为92.0％。

The protein had the specificity on substrate recognition, which could decompose 3,4-dihydroxybenzoic acid to catechol but not 2,4-dihydroxy- benzoic acid to resorcin. The ligand at C-3 site of benzene ring had no effect on enzyme activity.

蛋白质还具有底物识别的特异性，能够催化3，4-二羟基苯甲酸转化为邻苯二酚，而不能催化2，4-二羟基苯甲酸转化为间苯二酚，这表明苯环上3'位的配基对酶活无影响。

Producted RF and CRF aerogels by process of sol-gel technics, dynamic-exchange, CO2 supercritical drying, and procedural increase in temperature carbonization methods, which have eximious capability and nanometer network structure; Systemic analysis various factors which effect gel course, such as ratio of reactants and the dosage of catalyst, and probed into the better experiments conditions(the concentration of resorcinol and formaldehyde is more than 2% and the value of R/C is between 50 and 300); During gel course , primary investigated the viscosity curve and particle size distribution of sol-solution, and analyzed the reason of catalyst dosage effects particle size of gel, and confirmed that the up-growth of gel follows the theory of " polymerize increase ".The experiment results indicated that ultrasonic with unvarying temperature disposal shortened gel time and optimized quality of gels, and the factors of ultrasonic effect gel reaction velocity were analyzed; Prepared organic aerogels using compounds of resorcin and hydroquinone substitute resorcinol reacts with formaldehyde the first time, and also optimized the proportion of resorcinol and hydroquinone (the proportion of hydroquinone in 10%～40%).

采用溶胶-凝胶工艺结合动态溶剂交换、CO2超临界流体干燥与程序升温碳化方法制备出性能优良、具有纳米网络结构的RF与CRF气凝胶；深入研究了反应物配比催化剂用量等条件对凝胶过程的影响，得到了较佳的RF凝胶制备条件(RF浓度应大于2%，R/C值取50～300)；初步研究了凝胶过程中的粘度、粒径变化情况，分析了催化剂用量影响凝胶中粒子尺度的原因，在实验上印证了凝胶生长遵循"聚增长"的理论；通过引入超声波改进了RF气凝胶的制备工艺，缩短了凝胶反应时间，提高了凝胶品质，并探讨了超声波促进RF凝胶反应作用的原因；首次用对苯二酚与间苯二酚复配制备了混合有机气凝胶，优化出复配比(对苯二酚含量为10%～40%)。2。

The effects of transition metal salt catalyst,reaction temperature and time on the yield of resorcinol were investigated.

考察了过渡金属盐催化剂、反应温度、时间等对间苯二酚收率的影响，结果表明在催化剂与硫酸摩尔比0.008∶2、反应温度220 ℃，反应时间9 h条件下，间苯二酚收率达到90.2%。

The sulfonation and oxidation processes for manufacture of resorcinol are compared in environment benefit and some suggestions on the development of resorcinol are proposed.

介绍了间苯二酚的主要用途和国内外生产现状，并对主要的生产方法磺化法和氧化法从环境效应上进行了比较，对今后我国间苯二酚的生产发展提出了建

The linear range for resorcinol is 5.0×10^(-9)~1.0×10^(-4) mol/L with the detection limit of 3.0×10^(-9) mol/L. The relative standard deviation is 3.5% for 1.0×10^(-6) mol/L resorcinol in 11 repeated measurements.

该法测定间苯二酚的线性范围为5.0×10^(-9)~1.0×10^(-4)mol/L，检出限为3.0×10^(-9)mol/L，相对标准偏差为35%（1.0×10^(-6)mol/L间苯二酚，n=11。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。