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The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles

本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究,实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先,利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维,比较不同的热处理温度与反应时间的改变对产物生成产生影响,进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示,结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现,若热处理温度在100~4750C下可得到Cu23Cl奈米粒,475~4900C 可得Cu奈米粒,450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时,可产生直径比较细的纤维,纤维直径为107 88±21 01nm;且由於奈米金属颗粒镶嵌在二氧化矽纤维中,直径比较细的纤维,可以得到比较小的奈米金属颗粒,这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时,由於表面电浆子共震关系,而使纤维颜色由淡白黄绿色变成黄绿色,再变红褐色。由实验结果得知,利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度,可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。

Realistically designed as a floral spray, the two flower-heads set with oval cabochon rubies within an undulated border of brilliant cut diamonds, the stem set with baguette diamonds, the leaves with eight and brilliant cut diamonds.

栩栩如生的花束造型,两朵花的花瓣镶嵌椭圆形鹅蛋红宝石,波浪形边缘镶嵌明亮切割钻石,花茎镶嵌长方形钻石,叶子镶嵌八斜面及明亮切割钻石

As the first set of high-relief, technology medals mosaic "to wear gold Lunar New Year," 2 of the series, wearing medals Taurus is divided into four specifications, were used .999 pure silver .999 pure gold inlaid mosaic sapphire diamond production, the overall image of the product Like a coin through the cattle, realistic style.

作为国内首套高浮雕、镶嵌工艺纪念章"穿金生肖"系列的第二款,穿金牛纪念章分为四种规格,分别采用。999纯金镶嵌钻石。999纯银镶嵌蓝宝石制造,产品的整体形象好像一头穿过金币的牛,造型逼真。

Therefore only a full understanding of the features of bakelite and the specialty of the inlaying machine and a correct operation of inlaying machine will assure a safe and effective inlaying of metallographic specimen.

只有在充分了解电木粉的特点以及镶嵌机的特殊之处,并正确地操作镶嵌机,才可以保证安全、有效地实现金相样品的镶嵌。

Inlaying is a key step in the specimen preparation process for the metallographic research process and it can be realized through various methods such as mechanic inlaying, resin inlaying and special inlaying.

镶嵌是金相研究过程中试样制备阶段的一个步骤,可采用机械镶嵌法、树脂镶嵌法以及特殊镶嵌法。

Crassipes and other aquatic plants pulssingall combination in series showed efficiant removing ability for nitrogen and phosphorus,and the inlay combination of E. crassipes, Trapa manshurica and Nymphaea tetragonashowed better removal efficiency for redox organic pollutants than the inlay combinationadding other combination in series.

人工复合生态系统试验表明,凤眼莲与水生植物的镶嵌组合加各级串联组合能有效去除氮磷,而对于还原性有机污染物,凤菱睡镶嵌组合的去除效果相对要好于镶嵌组合加各级串联组合。

The mosaic technology includes auto mosaicking, mosaicking by drawing a mosaic line, gray mosaicking, color mosaicking, mosaicking by drawing a mosaic line for mosaicking complex area by drawing a mosaic line, gray mosaicking, color mosaicking for eliminating the difference of geometry and color.

镶嵌技术包括自动镶嵌、镶嵌线镶嵌、基于灰度的镶嵌与基于彩色的镶嵌等技术,镶嵌线镶嵌用于接边区域比较复杂需要画镶嵌线来辅助镶嵌,基于灰度的镶嵌与基于彩色的镶嵌用于进一步消除影像几何差异与辐射度差异。

The mosaic technology includes auto mosaicking, mosaicking by drawing a mosaic line, gray mosaicking, color mosaicking, mosaicking by drawing a mosaic line for mosaicking complex area by drawing a mosaic line,gray mosaicking, color mosaicking for eliminating the difference of geometry and color.

镶嵌技术包括自动镶嵌、镶嵌线镶嵌、基天灰度的镶嵌与基于彩色的镶嵌等技术,镶嵌线镶嵌用于接边区域比较复杂需要画镶嵌线来辅助镶嵌,基于灰度的镶嵌与基于彩色的镶嵌用于进一步消除影像几何差异与辐射度差异。

Dial, the hour mark to 8 diamonds and elegant Arabic numerals were highlighted out of hours can also be form ring showing a day / night comparison of state, all-black city ring can bring out the elegant mother-of-pearl Pui dial, black crocodile also allows leather strap and crown on the charming agate better, in order to allow this expression to the perfect realm, which table table inlaid circle has 54 diamonds (1.95 carats), and stainless steel watchcase embraced each other.

拨号,一小时至8钻石标志,优雅的阿拉伯数字强调了几个小时内也可以形成环呈现出昼/夜的状态相比,全黑的城市环能带出的优雅的珍珠母贝表盘,黑鳄鱼还允许在迷人的玛瑙更好的皮表带及冠,以便让这种完美的境界,这表的表圈镶嵌的表达有54个钻石(1.95克拉),和不锈钢表壳互相拥抱。

The infamous logo from the movie is on the body, a Captain Jack Sparrow voodoo doll is on the headstock, and the fingerboard inlays are lovely, blood-red skull and crossbones!

在胴体上有来自电影的那个&臭名昭著&的商标,一个船长杰克斯帕罗的巫毒教玩偶在它的头部,并且指板上镶嵌的雕刻是可爱的,血红的头骨和两个交叉骨头的图形!

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In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

。但是,在否定句或疑问句里,这种带有"do"的方法表达的效果却没有什么强调的意思。

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