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We have used GC to follow up the formation of epoxy acid and established the acidify condition; we have done series of parallel experiments to better the pivotal condensation reaction between acid and amine; In the cyclization step, we use cheap and available reagent-Lithium amide , rather than expensive LiHMDS, to proceed the reaction; and at last, we introduced green reagent-ozone to clear the phenyl group of nitrogen to avoid using heavy metal reagent-CAN. The total yield for this method is 29.8%.

通过GC监测,确定环氧酸的最佳酸化条件;对关键的酸和胺的缩合步骤,平行试验了多种条件;在环合一步,用价廉易得的氨基锂及催化量的HMDS代替昂贵的LiHMDS进行反应;氮上苯基的脱除采用臭氧,避免了重金属试剂-硝酸铈铵的使用,总收率为29.8%。

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Main products are: ultrasonic plastic welding machine, micro-computer precision spot welding machine, ultrasonic mold, voltage resistance tester, lithium battery protection board tester; company has strong technical strength, with high-quality talent reserves - the development of experienced design engineers, skilled staff; advanced production equipment, superior manufacturing processes and high-quality and efficient after-sales service.

主营产品有:超声波塑焊机,微电脑精密点焊机,超声波模具,电压内阻测试仪,锂电池保护板测试仪;公司技术力量雄厚,拥有高素质人才储备--经验丰富的开发设计工程师、技术精湛的员工;先进的生产装备、卓越的制造工艺以及优质快捷的售后服务。

The structure and appearance of the glass-ceramics after heat-treat...

随着热处理温度的升高,β-石英固溶体转变成β-锂辉石固溶体,而且微晶玻璃相应的变为不透明的乳白色,同时红外光谱可以检测到Al—O键的配位状态,且温度越高,Al—O键所占的比重越大。

The research indicate that the performance of brazing joint using Al-Ge-Si brazing filler metal precedes to the one using HL401 brazing filler metal. And the main reason is that brittle compound such as Cu2Al is not appeared in brazing joint.

本研究建立的2090Ce铝锂合金钎缝组织形态成长模型以及母材溶解厚度控制模型对钎料的选择、钎焊工艺参数的选择及接头钎焊间隙的确定等具有重要的参考和指导作用。

Seven efficacy: playing diverse and enjoyable; conducive thigh adductor adductor and external training; conducive to children's ability to exercise coordination and balance; promote bone growth and normal development of the leg; children overcome inside and outside the eight-character legs and the formation of O-shaped legs; Body body, let your body bodybuilding charming; thin weight loss (30 minutes per 400 calories consumed, is walking and cycling twice) Small electric cars This is a lithium battery-powered bicycles, gently press a button on the handlebar, the car will be able to come and go, people riding in the above can only control the direction.

玩法多样,其乐融融;★有利于大腿内收肌和外收肌的锻炼;★有利于少年儿童锻炼协调能力与平衡能力;★促进骨骼生长及正常腿部发育;★克服儿童内、外八字腿及O形腿的形成;★美体塑身,让你的身材健美迷人;★减肥瘦身(每30分钟消耗400卡洛里,是步行及骑单车的两倍)小型电动车,这是一种以锂电池为动力的自行车,轻轻按下车把上的一个按钮,车子就能来去自如,人骑在上面只需控制方向就可以。

Generally the catalysts have high activity and good selectivity. At present the coupling reactions of organoborahes with terminal olefins s acid chlorides and aryl halides play an important synthetic approaches in organoborane chemical. The catalysts can be used by many kinds of organometal compounds such as: irons cobalt nickel ruthenium rhodium palladiums titaniums zirconiums tins indium and lithium organic compounds; The achievement has been amazed in preparing of unsaturated or saturated compounds and in synthesizing of natural products bioactive molecules and chiral compounds.

目前,卤代烃与不饱和烃的偶联反应和有机硼试剂与酰卤和卤代烃的偶联反应已成为有机合成的研究热点,此类反应可用铁、钴、镍、钌、铑、钛、锆、锡、铟、锂等多种有机金属化合物来催化,用于形成含饱和或不饱和C-C键的化合物,并已在天然产物、液晶、具有生理活性物质和手性化合物的合成中应用。

The results indicated that the adsorbance of adsorbed CO in the presence of alkali and rare-earth metal oxide decreased, and thus suppressed the nick loss in the form of Ni〓 in the POM process.

CO-FTIR的结果表明,锂和镧的添加可明显减少CO在NiO/γ-Al〓O〓上的吸附,从而抑制反应过程中羰基镍的生成和流失,同时也抑制了CO的歧化积碳和在表面进一步氧化成CO〓。3。

In this study, as a original strain, antagonistic bacterium Ata28 was mutated by UV, UV+LiCl, DES and Microwave irradiation; the very goal of the research is to improve the control efficiency of Ata28 strain against tobacco brown spot and obtain strains advanced both in antagonism and biological characteristics, further provides theoretics and practical experience to the production.

采用紫外线和氯化锂复合诱变Ata28菌株,通过预备实验,计算Ata28菌株在不同诱变时间的致死率和正变率,选择该菌株的最佳诱变时间10s,15s诱变;通过平板对峙培养,筛选出8个突变菌株在PDA平板上可明显抑制Tbs3的生长,抑菌带高于出发菌株Ata28,抑菌带最大值达9.7mm;经温室控病初筛和复筛试验,获得了对烟草赤星病有较好防效的突变菌株Uv1-190、Uv1-199,烟苗经Uv1-190、Uv1-199菌液处理3d后,接种Tbs3的防治效果达51.3%、54.9%,比出发菌株Ata28的防治效果好。

The liquid electrolytes at the heart of traditional lithium-ion batteries can catch fire, but the Fraunhofer scientists say they've figured out a way to make them with a new, solid polymer that's inflammable, and, since it's solid, won't leak.

在传统锂离子电池的中心的液态电解液能着火,但Fraunhofer的科学家说他们已想出一种方法,用一种新的不可燃的固体聚合物来制造电池,并且由于是固态的,不会泄漏。

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With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务,乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐,因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。

Closes the eye, the deep breathing, all no longer are the dreams as if......

关闭眼睛,深呼吸,一切不再是梦想,犹如。。。。。。