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In this thesis, a series of complexes based on aromatic multicarboxylic acids have been successfully synthesized in solutions or under hydrothermal conditions. Their structure and properties are investigated.(1) Eight complex compounds have been synthesized and characterized by X-ray single crystal diffractive technology: The eight complexes are listed as following: [Cu242] complex 1 [Cd22(H2O)4]·4H2O complex 2 [Co(H2btc)(H2O)3] complex 3 [Co2(H2O)2]·H2O complex 4 [Ni22(H2O)4] complex 5 [Cu22(H2O)4] complex 6 [Co(H2biim)2(H2O)2](H2btc) complex 7 [Zn(H2biim)2(H2O)2](H2btc) complex 8 The structure of complex 1 is dinuclear complex resulted from weak interactions（0-D chain）; complex 2 is 1-D chain stucture result from interactions of water molecules; complex 3、4、5、6 are coordination polymers using hydrothermal synthses, where the first kind ligand is H4btc, the second kind ligand is phen and Co2+、Ni2+、Cu2+ as center ions, respectively. While the coordination enviroment of Co2+ is the same in complex 3, the coordination geometries around the Co atoms in complex 4 are obviously different because of the different reaction conditions. In complex 4, the 1-D chains are connected into 2-D layer through carboxy groups of ligand H4btc. The structures of complex 5、6 are 1-D chain stucture result from interactions of carboxy groups in ligand H4btc. Complex 7、8 are homeomorphy compounds. Either of them are linked to the 3-D chains through intermolecular hydrogen bonds. Each H4btc lose two protons and H2btc2- acts as negative electron balance.

合成了8个结构新颖的配合物，并用X-射线单晶结构分析方法确定了晶体结构，分别为： [Cu242] 配合物1 [Cd22(H2O)4]·4H2O 配合物2 [Co(H2btc)(H2O)3] 配合物3 [Co2(H2O)2]·H2O 配合物4 [Ni22(H2O)4] 配合物5 [Cu22(H2O)4] 配合物6 [Co(H2biim)2(H2O)2](H2btc)配合物7 [Zn(H2biim)2(H2O)2](H2btc)配合物8 配合物1是一个依靠弱作用连接的双核铜结构；配合物2借助水分子形成一维链状结构；配合物3、4、5、6是以H4btc为第一配体、phen为第二配体，通过水热法合成的配合物，其中，Co2+、Ni2+、Cu2+为中心离子；配合物3中的二价钴离子具有相同的配位环境，不同反应条件下得到的配合物4中的二价钴离子存在不同的配位环境，在配合物4中，一维链通过H4btc上的羧基形成一个二维层结构；配合物5、6是借助H4btc上的羧基形成的一维链状结构；配合物7、8属于异质同晶结构，它们的分子通过分子间氢键形成三维网状结构，H4btc上的羧基失去2个质子，作为一个二价负离子起到电荷平衡作用。

The contents are: measure and tuning of accelerating cavities, coupling cavities, measure of quality, field distribution, dispersion curve . and the way of measuring and eliminating the stop band, etc. At the same time, utilizing the test data and the dispersion equation of cavity chain, we make a fit dispersion curve by way of least squares fit, and we work out the width of stop band and the intercavernous coupling coefficient.

内容包括：加速腔频率韵测量和调谐、耦合腔频率的测量和调谐、品质因素的测量、场分布的测量、色散曲线的测量、禁带的测量和消除等，同时，论文还从腔链色散方程和测得的实验数据出发，利用最小二乘法进行拟合得到拟合色散曲线，并计算出禁带的大小和腔间耦合系数。

At first, setting up the arith relation between the signal input and the signal output of the generalized multi-carrier system of the Discrete Fourier Test spread-spectrum; then setting equilibria parameters of the frequency field equilibria subcarrier of the generalized multi-carrier system of the DFT spread-spectrum according to channel frequency response, channel noise variance and equilibria method; then calculating average power of useful signal, interferential average power between signals as well as noise variance of the generalized multi-carrier system receiving terminal of the DFT spread-spectrum according to the arith relation as well as the frequency field equilibria parameter, and recomputing available signal information noise ratio, so as to calculate the available signal information noise ratio of the generalized multi-carrier transmission system accurately, the method for estimating the available signal information noise ratio can be used for link self-adapting transmission solution of the generalized multi-carrier system based on Discrete Fourier Test spread-spectrum and radio material management.

一种DFT扩频的广义多载波系统的SINR估计方法，其通过首先建立所述离散傅立叶变换扩频的广义多载波传输系统的信号输入输出之间的数学关系，然后根据信道频率响应、信道噪声方差和均衡方法，设定所述DFT扩频的广义多载波传输系统的频域均衡子载波的均衡系数，再根据所述数学关系及所述频域均衡系数分别计算所述DFT扩频的广义多载波传输系统接收端有用信号的平均功率、信号间干扰的平均功率以及噪声方差，再计算有效信干噪比，如此以实现对广义多载波传输系统的有效信干噪比的准确计算，该有效信干噪比估计方法可用于基于离散傅立叶变换扩频的广义多载波传输系统的链路自适应传输方案和无线资源管理方面。

In this thesis, shikonin, cryptotanshinone and 5-fluorouracil (5-FU) were selected as the objects for several aspect studies: In Chaper 2, the electrochemical behavior of shikonin was investigated by cyclic voltammetry, linear sweep voltammetry, chronocoulometry and bulk electrolysis with coulometry on a glassy carbon electrode. Triple strand DNA modified electrode was preparated and used to investigate the interaction of shikonin with DNA. It was found that it is hydroquinone of shikonin to embed in DNA and interacted with guanine and adenine of DNA.

本论文以紫草素、隐丹参酮和5-氟尿嘧啶三种抗癌药物为研究对象，做了以下几个方面的工作：在论文的第二章，我们研究了紫草素的电化学基本性质，初步探讨了三链DNA 修饰电极的制备，并利用该修饰电极研究紫草素与DNA 的相互作用，得出主要是紫草素的氢醌与DNA 的G、A 碱基间发生嵌插作用的结论。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。