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A new method for measurement of liquidus temperature of aluminum electrolyte system with one meter connected to COM port of a computer is introduced. Liquidus temperature is determined based on cooling curve by using thermal analysis method.

研究了一种新的铝电解质初晶温度的测定方法:采用数字万用表与计算机串口相结合的测量技术,利用热分析法,根据步冷曲线确定电解质体系的初晶温度。

Through the thermodynamic calculation of the reaction that aluminum and magnesium reduce anhydrous scandium chloride molten salt to prepare aluminium-magnesium-scandium master alloy, we got that the standard equilibrium constant of the reaction is 1.074 ×10~(19), and the experimental equilibrium constant of it is approximately 6.874 × 10~(14)under around 1200 K and 1 standard pressure, which demonstrate that the reaction can take place and proceed thoroughly.

通过铝镁热还原无水氯化钪熔盐制备铝镁钪中间合金反应的热力学计算,得出:在1200K左右温度,1标准大气压下,该反应的标准平衡常数K为1.074×10~(19),经验平衡常数K′约为6.874×10~(14),这说明铝镁热还原无水氯化钪熔盐法制备铝镁钪中间合金的反应能够进行,而且进行的很彻底。

Using metal Al and TiO2 powders as starting materials TiN/Al2O3 composite ceramics were prepared by aluminothermic reduction of TiO2 in coke bed and a flowing nitrogen stream.

以金属铝粉和钛白粉为原料,在流动氮气和匣钵埋碳保护气氛下采用铝热还原氮化法制备了TiN/刚玉复合陶瓷。

CoAPO-5 molecular sieve was hydrothermally synthesized using pseudo-boebmite, phosphoric acid (85%), tetrahydrate cobaltous acetate as raw material and N, N-diehtyl-ethanolamine as tern- plating agent.

以拟薄水铝石、质量分数85%的正磷酸、四水合醋酸钻为原料,N, N-二乙基乙醇胺为模板剂,水热法合成了CoAPO-5分子筛。

In this paper, finite element software ANSYS is used to simulate the thermal conductivity and pressureless infiltration technique is used to produce aluminum infiltrated silicon carbide composite with high volume fraction of SiC. The influence of interfacial thickness and temperature on thermal conductivity and CTE have been investigated and analysed.

本文采用有限元软件ANSYS对铝渗碳化硅复合材料的有效热导率进行了数值模拟,用无压浸渗法制备了高体积分数的铝渗碳化硅复合材料,研究了界面层厚度和温度等对铝渗碳化硅复合材料的热导率和热膨胀系数的影响,并进行了分析。

Mechanics of microwave pyrogenation is dicussed, the suitable values of microwave power and Al3 +/SO_4~(2-) are determined as well as a well - perform -d sample of solid polyaluminum choride is obtained.

论述了微波热解的机理,确定了微波热解功率和Al3+的水相转移抑制剂离子配入的最佳值,得到了性能较好的聚合铝样品,验证了微波法的可行性。

This paper, aimed at the problem of drying aluminum fluoride trihydrate, studied the most possible binding format of crystal water, and hereby deduced the process of crystal water dehydration.

本论文针对三水氟化铝的干燥脱水问题,应用晶体结构理论、价键理论以及各种相关化学原理推测了三水氟化铝可能的结晶水结合形式,并据此推断了其结晶水的脱除过程:对氟化铝干燥特性进行了实验研究,研究了温度和升温速率对氟化铝干燥效果的影响:采用非等温TG-DTG法,对三水氟化铝进行了热分解行为和热分解动力学分析,进一步验证了三水氟化铝的脱水过程,并得出了其脱水和水解过程的动力学参数及方程。

In this thesis, the phase diagram of Zn-Al binary system on 10~69.5 w% was reinvestigated by using differential scanning calorimeter, X-ray diffraction and pushrod dilatometer. The process of isothermal transformation during the aging of high-Aluminum-Zinc-based alloy was studied by using differential scanning calorimetry, and the aging behavior of the alloy was analyzed at the aspect of thermal analysis kinetics. The change of microstructure which the alloy was being heated was observed on high-temperature metallurgical microscope. The microstructure and wear-friction properties were compared among the alloys treated with several different heat treatment processes, and a model for heat treatment processes was proposed based on artificial neural network,so as to predict the relationship between friction coefficient and parameters of aging treatment such as aging temperature and time.

本文采用高温X射线衍射、示差扫描量热分析、热膨胀等方法重新测定含锌量范围为10%~69.5%的Zn-Al系二元相图,利用示差扫描量热分析法,研究高铝锌基合金时效等温转变过程,并从热分析动力学的角度分析高铝锌基合金合金时效行为;使用高温金相显微镜观察合金加热时的组织变化;比较几种不同热处理工艺对高铝锌基合金显微组织与耐磨性能的影响并利用人工神经网络建立高铝锌基合金热处理工艺模型,预测合金摩擦系数随时效温度及时间变化规律。

Our product is a titanium , sparse noble metal material such as nickel, Mu , tantalum , zirconium processes; The tube , stick , silk , belt , board , foil , net , cake are encircled by reaching alloy products; Reaction equipment (500 L reaction boilers , titanium steel compound reaction boilers , titanium outside plate manage the warmup reaction boiler , the nickel steel compound reaction boiler); Heat exchanger (the titanium enumerates a pipe heat exchanger , titanium plate-type heat exchanger , the nickel heat exchanger , titanium helix plate-type heat exchanger); Compound board (titanium steel compound board , titanium copper compound board , titanium aluminium compound board finished product); The accessory and the heater titanium net are blue , the titanium flange , titanium nut titanium filter , titanium pump , titanium plate manage , the positive electrode , titanium centrifugal machine , titanium heater , various mistake are labeled with equipment and the accessory.

我们的产品是钛、镍、钼、钽、锆等稀贵金属材料加工;管、棒、丝、带、板、箔、网、饼环及合金制品;反应设备(500L反应釜、钛钢复合反应釜、钛外盘管加热反应釜、镍钢复合反应锅);换热器(钛列管式换热器、钛板式换热器、镍换热器、钛螺旋板式换热器);复合板(钛钢复合板、钛铜复合板、钛铝复合板成品);配件及加热器(钛网蓝、钛法兰、钛螺母钛过滤器、钛泵、钛盘管、阳极、钛离心机、钛加热器、各种非标设备及配件。

The distribution of thickness rolled and profile are simulated by considering roll system elastic deformation theory, distributions of tension stresses theory and roll thermal crown theory during rolling of wide strip and high speed aluminum foil roughing mill the rolling technology and thermochemistry parameters are tested, etc, the paper verifies above theories.

采用差分法模拟了具有分段冷却装置的宽幅高速铝箔粗轧机轧辊的温度场及热凸度分布。对轧辊热形为特性进行了全面的研究。首次考虑铝箔轧制的辊系弹性变形理论。张应力分布理论及轧辊热变形理论模拟了宽幅高速铝箔粗轧机的轧后断面形状及板形。

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