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铝化

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Using the fiber-optic probe technique, the time when the shock wave reachs the different places in steel plate and steel-aluminum plate under contact explosion with insensitive RDX and aluminize RHTL had been separately measured.

利用光纤探针测试技术,实验测量钝化RDX和含铝炸药RHTL分别与钢板、钢-铝板两种靶板接触爆炸条件下,靶板中不同位置的冲击波到达时间。

Experimental investigation indicates that shock wave velocity and shock wave pressure of beginning which were produced with aluminize RHTL were smaller than that of insensitive RDX in steel plate, however, attenuating velocity of shock wave velocity and shock wave pressure which were produced under contact explosion with aluminize RHTL were quciker than that of insensitive RDX in steel plate, when steel- plate had been separately operated under contact explosion with insensitive RDX and aluminize RHTL, and shock wave press had changed suddenly in the interface between steel and aluminum, In the circumstances, the shock wave velocity had ascended suddenly and shock wave pressure had descended suddenly.

实验研究表明:RHTL炸药爆炸加载钢板下,介质中的冲击波初始速度和初始压力相对RDX较小,衰减相对较快;钝化RDX和含铝炸药RHTL分别作用于钢铝复合板时,在分界面处冲击波速度和压力都发生突越,冲击波速度突跃,冲击波压力突降。

The changes of free energy and enthalpy were calculated in terms of depolarization values on Al cathode. Thermodynamic meaning of depolarization was discussed in details and the empirical relation between binary alloy type and depolarization type was proposed.

根据锂离子在铝阴极上产生的去极化值求出铝和锂发生合金化反应的热力学意义,提出二元合金类型与极化类型之间的经验关系。

Better film quality with oxygen free content and higher electron mobility can be achieved with InN film with AlN buffer layer .

氮化铝缓冲层的加入,可大幅提升氮化铟薄膜的电子移动率,并能在400℃制作出晶相单纯之氮化铟薄膜。

Both the protection and deprotective group methods for the amino-group on side chain of a new N-pivot lariat crown ether were studied comparatively.

研究了一种新的氮支套素冠醚侧链上氨基的保护和脱保护基方法,结果表明,由过量乙二胺与对甲苯磺酰氯反应得到的单保护乙二胺(N-对甲苯磺酰基乙二胺4a),经N-烷基化环化反应,然后在氢化铝锂存在下脱除保护基,即可制得最佳产率的N-(2-氨基已基)单氮杂-12-冠-4(1)。

By using the a device being similar to water segregator and by controlling the temperature, cyclization of the intermediate product in chloroform reduced carbonization and gave 2-dodecaneanthraquinane in 68.1% yielding.

以十二烷基苯和苯酐为起始原料,经酰基化、关环和磺化三步反应合成了3-十二烷基蒽醌磺酸;并进一步改进和优化了合成工艺条件:即在催化剂三氯化铝过量50%并有三乙胺存在的条件下,中间体2-(4-十二烷基苯甲酰基)苯甲酸收率为72.45%;关环反应采用氯仿作溶剂,利用类似分水器的装置有效控制反应温度以减少碳化,2-十二烷基蒽醌的收率为68.1%。

The catalysts such as tetraphenyl tin,aluminium isopropoxide and boron trifluoride etherate complex were used to catalyze the copolymerization.In addition,the copolyester can be given by copolycondensation after monomers were hydrolyzed by phosphoric acid.Boron trifluoride etherate complex was chosen as the catalyst because the catalytic activity was the best among the catalysts.

由于γ-戊内酯为五元环结构,难以进行开环聚合,因此分别考察了四苯基锡、异丙醇铝、三氟化硼乙醚络合物等催化剂,以及以磷酸为催化剂的水解缩聚反应,结果发现三氟化硼乙醚络合物的催化活性最高,因此选择三氟化硼乙醚为本体开环聚合的催化剂。

The total synthesis of the title compound 10 was accomplished starting from 3,5-dimethoxybenzoic acid (1) and p-hydroxybenzaldehyde (6). In the process, esterification, reduction, bromination and Wittig-Homer reaction were performed.

以3,5-二甲氧基苯甲酸为起始原料,经过甲醇酯化、氢化铝锂还原、四溴化碳溴代和Wittig-Homer反应,高产率的合成了Wittig-Homer试剂(5)。

Ib was synthesized by condensation of phthalic anhydride with 2-methylresorcinol in fused AlCl〓/NaCl (5∶1), followed by selective acetylation, methylation, NBS bromination and condensation with sodium ethoxide.

邻苯二甲酸酐在熔融的三氯化铝-氯化钠(5:1)中和-2,6-二羟基甲苯环合得1,3-二羟基-2-甲基蒽醌〓后经选择性乙酰化、甲基化、NBS溴化、乙醇钠缩合得1-甲氧基-2-乙氧甲基-3-羟基蒽醌。

It has raised great interests of research on interface of heterogenic material combination in resent years. In this research program, Al2O3, AlN and Si3N4 ceramics include Si samples had been surface metallized by pulsed high energy density plasma gun, and micro and macro behavior of interface between metallic film and substrate were studied in detail.

异质材料结合的界面研究是近年来材料研究的热点之一,本课题采用脉冲高能量密度等离子枪对氧化铝、氮化铝和氮化硅等纯陶瓷以及纯硅片材料基片表面进行金属化,进而对于金属膜/基底界面的微观和宏观行为进行了研究。

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