铝

A chemical coagulatory coprecipitation method was used in the treatment of blast-furnace gas washing water.

用化学混凝共沉淀的方法处理高炉煤气洗涤水，实验确定了最佳的药剂为聚合氯化铝钙，工艺的最佳操作条件是聚合氯化铝钙加入量为33mg/L，PAM加入量为0.5mg/L，搅拌时间为60s，搅拌强度为90r/min。

Aim To explore the protective effects of total coptis alkaloids on the neurodegeneration caused by aluminium overload in mice.

目的 采用铝负荷致小鼠脑损伤模型，探讨黄连总生物碱对铝致神经元退行性变的防治作用。

This thesis studies the volcanic tectono-petrofacies, petrology, mineralogy, geochemistry, isotopic chronology, stratum and high-precision SHRIMP zircon U-Pb datings of the Mt.Yandangshan volcano-intrusive complex, and concludes that: Yandangshan volcanic rock units belong to high-K calc-alkaline acid rock associations, mainly ryholitic and trachytic dacitic in composition. They have A/CNK values of 0.9-1.2 (i.e., aluminium saturation and supersaturation), enriched LREE and LILEs and depleted HFSE. Their 8Eu values are 0.11-0.32, indicating a evident fractional evolution of plagioclase crystallization. Their ∑REE varied very limitedly,(87~Sr/(86)Sri ratios and eNd values are 0.7086～0.7095 and -10.20～-9.96 for volcanic rocks, and 0.7087~0.7095 and -7.6～6.92 for the central intrusive facies syenite, which means that all the igneous rocks from Mt. Yandangshan are evolutional products of magmas with the same source, and that they derived mainly from crust, but mixed with mantle components.

本文从火山构造岩相学、岩石学、矿物学、地球化学、同位素年代学、地层学等方面出发，同时结合高精度SHRIMP锆石U-Pb定年，对雁荡山火山岩进行了系统的研究，确定雁荡山火山岩为一套以流纹质和粗面英安质为主体的高钾钙碱性酸性岩石组合，A/CNK值集中在0.9～1.2之间，为铝饱和或铝过饱和类型；富轻稀土元素和大阳离子亲石元素、相对亏损高场强元素：负铕异常明显，δEu值为0.11～0.32，表明岩浆经历了以斜长石为主的强烈结晶分异作用：岩石样品的∑REE变化有限，火山岩样品的~(87Sr/~(86)Sr_i为0.7086～0.7095，εNd为-10.20～-9.96，中央侵入体石英正长岩~(87Sr/~(86)Sr_i为0.7087～0.7095，εNd为-7.6～-6.92，表明它们是同源岩浆分异演化的产物，物质来源主要为陆壳，但有地幔物质参与。

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area;2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support;3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier;4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling;5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene PolymerizationIn this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that:1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS;2.co-mlling time had no obvious effect on the texture of support after 12 hours;3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明，MAO不仅仅只和乙醇作用，MAO还与MgCl_2本身有一定的作用，这是一个极为重要的发现；3、通过ICP和EDX表征，发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布；4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能，特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化，并且催化剂寿命长，表现出稳定的动力学行为，最终获得了高堆密度(大于0.35g／ml)的球形聚乙烯颗粒；5、本文选择MSPC-5为研究对象，考察了聚合反应参数对催化剂的活性及其聚合物的影响，研究发现：不同的烷基铝对催化剂具有非常重要的影响，特别足TIBA对MSPC-5的助催化活性最高，烷基铝的加入量有一个较佳值，聚合温度为80度时活性最高，H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小；、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨，制备出了一种的新型的氯化镁载体，并将该载体用于多种单活性中心催化剂的负载化研究，研究表明：1、通过BET、XRD的表征，再次证实了MAO与MgCl_2之间具有直接作用，与XPS的研究结果相一致；2、当研磨时间高于12小时时，延长研磨时间对载体的结构没有显著的影响；3、将配合物3负载于共研磨时间不同的一系列载体上，乙烯聚合结果表明，尽管共研磨时间对负载催化剂的活性具有明显的影响，但是它对聚合物的性能以及催化剂的影响不明显。

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area; 2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support; 3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier; 4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling; 5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene Polymerization In this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that: 1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS; 2.co-mlling time had no obvious effect on the texture of support after 12 hours; 3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明，MAO不仅仅只和乙醇作用，MAO还与MgCl_2本身有一定的作用，这是一个极为重要的发现； 3、通过ICP和EDX表征，发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布； 4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能，特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化，并且催化剂寿命长，表现出稳定的动力学行为，最终获得了高堆密度(大于0.35g／ml)的球形聚乙烯颗粒； 5、本文选择MSPC-5为研究对象，考察了聚合反应参数对催化剂的活性及其聚合物的影响，研究发现：不同的烷基铝对催化剂具有非常重要的影响，特别足TIBA对MSPC-5的助催化活性最高，烷基铝的加入量有一个较佳值，聚合温度为80度时活性最高，H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小；、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨，制备出了一种的新型的氯化镁载体，并将该载体用于多种单活性中心催化剂的负载化研究，研究表明： 1、通过BET、XRD的表征，再次证实了MAO与MgCl_2之间具有直接作用，与XPS的研究结果相一致； 2、当研磨时间高于12小时时，延长研磨时间对载体的结构没有显著的影响； 3、将配合物3负载于共研磨时间不同的一系列载体上，乙烯聚合结果表明，尽管共研磨时间对负载催化剂的活性具有明显的影响，但是它对聚合物的性能以及催化剂的影响不明显。

Aluminum phosphate (AlPO 4) can be prepared by solid state synthesis with different templates, aluminum chloride and ammonium diacid phosphate at low temperature (180℃) within a short time (2 h).

以氯化铝和磷酸二氢铵为原料，在模板剂存在下用固相合成方法合成了磷酸铝类化合物，合成的化合物通过化学分析、ICP测定、XRD和 IR图谱对其进行了表征，研究了化合物对铬离子吸附性能，实验表明这类化合物对铬离子有较好的吸附能

The specialty makes the Al2O3/Cu composite material by internal oxidation of deeply aluminized pure copper matrix is more fine to be the diathermanous copper material of metallurgical equipment in the high temperature service condition than the ageing and solution alloy of aluminized deeply pure copper.

这种特性使得纯铜深层渗铝内氧化Al2O3/Cu复合材料在高温服役条件下比纯铜深层渗铝固溶时效合金更适合用作冶金设备用传热铜材料。

Another example is about the synthesis of AlPO〓-21, it was prepared by using diethylamine as template.

该链是一条亚磷酸铝链，在水热反应过程中，在相关模板剂的协同作用下，P物种经过缓慢的氧化-还原反应原位转变生成P物种，并通过水解与缩合的自组装路线而生成相关类型的磷酸铝分子筛。

The nano-aluminum phosphate powder was prepared through adjusting the pH value of aluminum dihydric phosphate by dropping ammonia water at a proper temperature in the presence of additive CTAB.

在有机调整剂CTAB的作用下，将磷酸二氢铝溶液用氨水调节pH值在一定温度下合成纳米磷酸铝粉体，然后经高温烧结制得致密陶瓷薄膜。

A large number of microgranular dioritic enclaves occur in some post-collisional metaluminous-peraluminous granites, in Kubusunan orebody, in Kalamaili area, eastern Junggar, North Xinjiang.

新疆东准噶尔卡拉麦里地区库布苏南晚古生代后碰撞准铝质过铝质花岗闪长岩体中广泛发育大量的暗色微粒闪长质包体。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。