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Ethyl decanoate was synthesized from capric acid and ethanol by using ferric potassium alum as catalyst.

以铁钾矾为催化剂,通过癸酸与乙醇反应合成了癸酸乙酯。

The results showed that new-type solid ferric potassium alum was a good catalyst for the synthesis of ethyl decanoate and the optimum conditions were as follows: molar ratio of acid to alcohol was 1∶2, the use level of catalyst was 0.6 g/0.05 mol capric acid, water-taking reagent benzene was...

结果表明,新型固体酸铁钾矾是合成癸酸乙酯的良好催化剂,在酸醇物质的量比为1∶2,催化剂用量为0.6g(0.05mol癸酸),带水剂苯为15mL,反应时间为2.5h的条件下,癸酸乙酯的酯化率可达98%。

The results showed that new-type solid ferric potassium alum was a good catalyst for the synthesis of ethyl decanoate and the optimum conditions were as follows: molar ratio of acid to alcohol was 1:2, the use level of catalyst was 0.6g/0.05 mol capric acid, water-taking reagent benzene was 15 mL, reaction time was 2.5 h and the yield of ethyl decanoate could reach 98%.

结果表明,新型固体酸铁钾矾是合成葵酸乙酯的良好催化剂,在酸醇物质的量比为1:2,催化剂用量为0.69(0.05 mol癸酸),带水剂苯为15mL,反应时间为2.5h的条件下,癸酸乙酯的酯化率可达98%。

Ethyl decanoate was synthesized from capric acid and ethanol by using ferric potassium alum as catalyst.

以铁钾矾为催化剂,通过葵酸与乙醇反应合成了癸酸乙酯。

The synthesis methods of ethyl lactate catalyzed by P-toluene sulfonic acid, cationic exchange resin, ferric chloride hexahydrate, stannous chloride, Aluminium chloride, modified zirconium oxid, ferric-potassium vitriol, ammonium ferric sulfate dodecahydrate, rave earth sulfate, sodium bisulfate monohydrate, complex solid superacid, heteropoly acid, molecular sieve, ionic liquid and lipase etal.

评述了对甲苯磺酸,阳离子交换树脂,六水三氧化铁,氯化亚锡,三氯化铭,改性氧化锆,铁钾矾,十二水合硫酸铁铵,稀土硫酸盐,一水硫酸氢钠,复合固体超强酸,杂多酸,分子筛,离子液体和脂肪酶等催化剂催化合成乳酸乙酯的合成方法。

The results indicated that new Lewis acid ferric potassium alum was a green catalyst for the synthesis of ethyl lactate.

研究了新型Lewis酸铁钾矾的制备,并以该Lewis酸为催化剂,通过乳酸和乙醇反应合成乳酸乙酯,考察了催化剂用量、反应时间、酸醇物质的量比对酯化率的影响。

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