铁氰化钾

Chicken chorioallantoic membrane ; angiogenesis ; hemoglobin ; potassium ferrocyanide

鸡胚尿囊膜；高铁氰化钾法；新生血管；血红蛋白

A HPLC method for determination of sorbic acid,benzoic acid and sodium saccharin in dairy drink was studied.The comparison of five methods of precipitating protein showed that the solution of potassium ferrocyanide and zinc sulfate as protein's precipitant was appropriate.

探讨含乳饮料中山梨酸、苯甲酸、糖精钠的HPLC含量测定方法，在比较5种沉淀样品中蛋白质的方法后，确定以亚铁氰化钾与硫酸锌溶液为沉淀剂，采用C18反相柱，以甲醇：乙酸铵溶液(0.02 mol/L)=15∶85为流动相，紫外230 nm检测，结合保留时间及二极管阵列检测器光谱分析信息定性。

In this bath, maleic acid was an inhibitor, when its concentration was kept at 20 mg/L, the deposition rate could reduce to 6.17μm/h, the content of nickel decreased to 1.74% and the resistivity was 7.51μΩ·cm; Potassium ferrocyanide inhibited deposition of copper, when its content was 0.5 ppm, the deposition rate decrease to 3.38μm/h, the content of nickel was 2.03%, the resistivity can reduced to 5.41μΩ·cm, the copper deposits also had higher (111) plane orientation. Thiourea was also an inhibitor in this system, when its concentration was kept at 0.8 ppm, the deposition rate was 4.72μm/h, the content of nickel in the film was 1.20%, the resistivity can reduced to 5.46μΩ·cm, at the same time, the deposition at (111) plane orientation become more favorable.

结果表明，马来酸在该体系中是抑制剂，当其浓度为20 mg/L时，镀速降为6.17μm/h，镀层镍含量降为1.74%，表面电阻率降为7.51μΩ·cm，铜层颗粒细小均匀，更有利于在(111)面上的结晶；亚铁氰化钾的加进可以明显降低镀，当其浓度为0.5 ppm时，镀速为3.38μm/h，镀层镍含量降为2.03%，表面电阻率降为5.41μΩ·cm，铜层颗粒细小均匀，(111)晶面衍射峰增强；硫脲在体系中也显示为抑制剂，当其浓度为0.8 ppm时，镀速降到4.72μm/h，镀层镍含量为1.20%，表面电阻率降为5.46μΩ·cm，形成的铜颗粒很小，同时(111)晶面衍射峰增强，有利于铜在(111)面上结晶。

Methods: The protein and other impurity in the sample were precipitated by zinc acetate and potassium ferrocyanide after dipping of the sample. N,N-dichlorocyclohexylamine derived from sodium cyclamate by sodium hypochlorite in the filtrate was extracted by hexane. The HPLC separation was carried out with a phenomenex Gemini-C18 column using acetonitrile-water(7+3) or methanol-water (8+2) as mobile phase and detected by UV monitor at 314 nm. External standard method was used for quantification.

样品中甜蜜素浸提后，用乙酸锌和亚铁氰化钾试剂沉淀蛋白质等干扰杂质，过滤，用次氯酸钠将样品溶液中的甜蜜素转化为N，N-二氯环己胺经正己烷萃取后，在phenomenex Gemini-C18柱上，以乙腈－水(7+3)或甲醇－水(8+2)为流动相进行分离，HPLC-UV检测器在314 nm测定，外标法定量。

The materials are gold mine of low sulfur content, calcine or gold contain abatement. Cyanogens lixiviant is alkaline thiourea, stabilizer is sodium sulphite or sodium silicate, they constitute high stability alkaline thiourea system, and bland oxidizing agent is potassium ferricyanide with moderate electric potential during sunking process.

本发明以低硫含量的金矿、焙砂或含金废料为原料，以碱性硫脲为无毒的代氰浸出剂，以亚硫酸钠或硅酸钠为稳定剂，组成高稳定性碱性硫脲体系，浸出过程中以具有适中电势的铁氰化钾为温和氧化剂。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。