钠的

Based on the previous literatures, the following major innovation works were carried out in this dissertation:(1) The derivatization reaction conditions of ephedrine and pseudoephedrine with sensitive derivation reagent in aqueous system were studied and two new methods were developed for the assay of them by microemulsion electrokinetic chromatography and micellar electrokinetic chromatography with LIF detection. The sensitivity and analysis times were greatly improved compared with the previous reports;(2) A new method of CZE with indirect LIF detection was developed for the simultaneous determination of six coumarin compounds (esculin, esculetin, isofraxidin, genistein, naringin and sophoricoside) with fluorescein as the probe. The proposed method enlarges the application range of LIF detector, and provides new approach for the analysis of certain compounds difficult to derivatize;(3) Based on the above research, an MEKC with indirect LIF detection method for the simultaneous determination of adenine and guanine in DNA extracts from fungus, maize and soybean was established;(4) A new method for the investigation of the complexes formed between human serum albumin and ampicillin sodium under the simulated physiology conditions using laser light scattering technique was developed.

该论文在综述前人工作的基础上，开展了如下未见文献报道的创新性的研究工作：(1)使用灵敏的衍生试剂对麻黄碱和伪麻黄碱在水体系中的衍生反应条件进行了系统研究，建立了微乳电动色谱-激光诱导荧光检测法和胶束电动色谱—激光诱导荧光检测法测定麻黄碱和伪麻黄碱的灵敏分析新方法，与以前的报道相比，灵敏度和分析时间均有很大改善；(2)使用荧光素钠作为背景荧光试剂，建立了同时分析测定六种黄酮类化合物(秦皮甲素、秦皮乙素、异秦皮定、染料木素、柚皮苷和槐角苷)的毛细管区带电泳—间接激光诱导荧光检测新方法，扩大了激光诱导荧光检测的应用范围，对难衍生化合物的分离分析提供了一种新思路和新途径；(3)以荧光素钠作为背景荧光试剂，建立了一种用于同时测定食品提取DNA中的腺嘌呤和鸟嘌呤含量的胶束电动色谱—间接激光诱导荧光检测新方法；(4)用动态和静态激光散射法研究了模拟生理条件下人血清白蛋白与氨比西林钠盐相互作用所形成的复合物，为药物分子与蛋白质的相互作用、药代动力学等的研究提供了一种新思路。

The optimun technological conditions were studied on the synthesis of 9-flourenylmethanal by the reaction of flouren and ethyl formate , and the synthesis of 9-flourenylmethanol by the reaction of 9-flourenylmethanal and methanal with sodium ethylate as catalyst.

研究了乙醇钠为催化剂，由芴与甲酸乙酯合成芴甲醛，再由芴甲醛与甲醛合成苯甲醇的工艺条件，结果表明：合成芴甲醛时，当芴为 16g时，催化剂乙醇钠 4 。

After esterification, the ethyl-2-chloro-3-phenylpropionate reacts with diethyl malonate under the catalysis of sodium ethylate, and we obtain the corresponding triethyl ester. The-benzylsuccinic acid is formed by the triethyl ester reacting with concentrate hydrochloric acid and taking place hydrolyzation and decarboxylation reaction at the same time. In order to avoid the formation of cinnamic acid, the sodium ethylate and diethyl malonate must be react sufficiently. The course has simple operation, inexpensive materials and better yield.

具体制备工艺为：首先以L-苯丙氨酸为原料采用重氮化方法得到-2-氯-3-苯基丙酸，再经酯化得到-2-氯-3-苯基丙酸乙酯后在乙醇钠催化作用下和丙二酸二乙酯缩合，发生SN2反应，得到相应的三乙酯，然后经水解和脱羧，得到-苄基丁二酸；在实验中乙醇钠要和丙二酸二乙酯充分反应，避免生成肉桂酸乙酯；该过程操作简单，原料便宜，产率较高，总收率可达到26.8%。

Kidney beans is a rare high potassium, high magnesium, low sodium food, hectogram 1520 mg of potassium, magnesium, 193.5 mg of sodium is only 0.8 mg, this feature come in handy in nutritional treatment.

芸豆是一种难得的高钾、高镁、低钠食品，每百克含钾1520毫克，镁193.5毫克，钠仅为0.8毫克，这个特点在营养治疗上大有用武之地。

Based on the laboratory conditions, the application of the static scale experimental study of the sodium scale corruption, discussed the time, temperature, sodium humate concentration, alkalinity and calcium ion concentration on the impact scale.

本文在实验室条件下，应用静态阻垢实验法研究了腐钠阻垢性能，讨论了时间、温度、腐植酸钠浓度、碱度及钙离子浓度等因素对阻垢的影响。

Difluorodiphenylsulfone and 4, 4"-difluorodiphenylketone are sulfonated by 50 % sulfuric acid. A new biphenol monomer containing six-membered ring imide is synthesized by reaction of 1, 4, 5, 8-naphthelenetetracarboxylic acid dianhydride with 3-aminophenol or 4-aminophenol sodium.

以50%发烟硫酸为磺化试剂，以4，4′-二氟二苯砜和4，4′-二氟二苯酮为原料反应得到双磺化的4，4′-二氟-3，3′-二磺酸钠-1，1′-二苯砜和4，4′-二氟-3，3′-二磺酸钠-1，1′-二苯酮。

However,the removal of soil noncrystalline aluminum with DCB soultioncaused an obvious decrease of soil SSA.3.The hydroxy aluminum in the interlayer of 1.4nm intergrade mineralhad an important negative effect on the cation exchange capacity ofsoil colloids.Its removal would cause a significant increase in CEC valuesof the soil colloids.4.Free aluminum was the major carrier of phosphate adsorption of soilcolloids.Particularly,the active aluminum had a decisive effect on thecapacity of phosphate adsorption of soil colliods.5.Addition to the effects of other soil constituents on soil surfaceproperties,it was thought that the effect of soil free aluminum,especially active aluminum on soil surface properties,deserved closeattention.

焦磷酸钠、草酸铵、DCB、柠檬酸钠和NaOH提取的土壤铝对提高土壤CECv、AEC、PZC和PZNC起重要作用，尤以活性铝的作用较大。2）用草酸铵处理除去铝后，土壤比表面积变化不大或略有增加；用DCB处理除去土壤铝后，土壤SSA明显降低。3）层间羟基铝对土壤胶体的阳离子交换量有显著负贡献，用柠檬酸钠将之除去后，土壤胶体的阳离子交换量明显增加。4）土壤胶体中的游离铝是土壤胶体吸附磷的主要载体，尤其是其中的活性铝，对土壤胶体的磷吸附能力起决定性作用。5）除其它土壤组分对土壤表面性质的影响外，土壤中的游离铝、尤其是活性铝对土壤有关表面性质的影响，值得引起特别的重视。

Treatment of hyponatremia involves administration of sodium and elimination of intravascular free water.

低钠血症的治疗包括补钠和排除血管内游离水。

Based on molecular kinetic theory, a microscopic model was developed for determining the evaporation and condensation rates of sodium in a reactor bundle.

采用蒙特卡罗方法分析钠冷快堆在假想冷却剂丧失条件下燃料棒束的钠两相流传热问题。

Result zinc sulfate, sodium selenite and zinc sulfate together with sodium selenite had the effects of antagonism to DNA amage caused by mercury chloride in vero cells.

结果 硫酸锌和亚硒酸钠，以及两者合用都具有拮抗氯化汞致vero细胞DNA损伤的作用，两者最佳组合是1.5 mg/L硫酸锌+1.0μmol/L亚硒酸钠。

Shop assistant: Please check at the door.

店员：请您到门口柜台交费。

In the end, transportation of PAHs in the environmental matrix was preliminarily investigated and discussed according to PAHs data of soils and sediments from a certain region in Shanghai. The result indicated that there are two or more pathways on PAHs transportation in the environmental matrix.

最后，对上海特定地区内PAHs在环境介质中的迁移径途进行了分析讨论，结果表明上海市土壤和沉积物等环境介质中PAHs的迁移存在多种途径。