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Methods:Sparfloxacin sodium was synthesized in alkaline condition with sparfloxacin, and then sparfloxacin sodium react with zinc sulfate to sparfloxacin zinc;Sparfloxacin zinc ointment was prepared with vaseline and lanolin as drug excipient and the concentration of sparfloxacin zinc was analyzed with ultraviolet-visible spectrophotometer;Burn patients were treated with sparfloxacin zinc ointment and other routine techniques.

用司帕沙星做原料,在碱性条件下反应生成司帕沙星,司帕沙星再和硫酸锌反应生成司帕沙星锌:以凡士林和羊毛脂为基质制备软膏剂,用分光光度法检测主药的含量,以临床烧伤患者为使用对象,司帕沙星锌软膏剂配合其他常规治疗方法治疗烧伤疾病。

The possible pathway of ABAS degraded by Zoogloea HP3 was that ABAS was first cleaved to produce o-phthalic acid and products. The former was further degraded and the composites of the latter were 2-amino-3-hydroxyl-5bromobenzenic sulfonic sodium and 2, 3-dihydroxyl-5-bromobenzenic sulfonic sodium.

动胶菌HP3作用下溴胺酸可能的降解途径为蒽醌环开裂生成中间产物邻苯二甲酸,邻苯二甲酸被进一步降解;溴胺酸降解后的最终产物为2-氨基-3-羟基-5-溴苯磺酸和2,3-二羟基-5-溴苯磺酸

The lactated Ringer's gis given in group L and the acetated sodium in group A.

目的 比较术中输入乳酸林格液和醋酸林格液血乳酸盐及血气的变化。

Objective TO compare the different changes of blood lactate and blood gases when given the lactated Ringer's solution and acetated sodium solution during operation.

e# 目的比较术中输入乳酸林格液和醋酸林格液血乳酸盐及血气的变化。

Objective TO compare the different changes of blood lactate and blood gases when given the lactated Ringer's solution and acetated sodium solution during operation.

中国论文联盟http://www.lwlm.com 目的比较术中输入乳酸林格液和醋酸林格液血乳酸盐及血气的变化。

Objective TO compare the different changes of blood lactate and blood gases when given the lactated Ringer's solution and acetated sodium solution during operation.

转载于中国论文联盟 http://www.lwlm.com 目的比较术中输入乳酸林格液和醋酸林格液血乳酸盐及血气的变化。

Chemiluminescent immunoassay is one of the advanced immunoassay ofnon-radioisotopic immunoassay because of its high sensitivity, wide dynamic range,high accuracy, stable labeled protein, full automation and extensive application field.CLIA using acridinium ester derivatives as chemiluminescent label has advantages oflow background, high signal-to-noise ratio, no need of catalyst and simpleluminescence system. Different aspects associating the DMAE·NHS-based CLIA were studied in thisthesis, including synthesis of acridinium ester, chemiluminescentcharacteristics of DMAE·NHS, labelling antibody or streptavidin with DMAE·NHS,two-site sandwich chemiluminescent immunoassay for TSH, two-sitesandwich chemiluminescent immunoassay involved biotin-streptavidinsystem for TSH, and competitive chemiluminescent immunoassay usingbiotin-streptavidin system for TT〓. The desired acridinium ester, DMAE·NHS, was synthesized according to thereference method with some modifications. The products were identified by IR, NMR,MS and elemental analysis. In our method, KOH was used in place of NaOH tosynthesize benzyl ester of 3,5-dimethyl-4-hydroxybenzoic acid,2',6'-dimethyl-4'-(n-succinimidyloxycarbonyl) phenyl-acridinium-9-carboxylate waspurified on a silica gel column with chloroform/ethylacetate(4:1, v/v) as eluent andfurther purified by triturating with hexane/acetone(2:1, v/v).

DMAE·NHS的合成是本论文的关键和难点,我们对文献方法进行改进:文献方法用氢氧化与3,5-二甲基-4-羟基苯甲酸反应制得3,5-二甲基-4-羟基苯甲酸,再用3,5-二甲基-4-羟基苯甲酸与苄氯作用制备3,5-二甲基-4-羟基苯甲酸苄酯,我们用氢氧化钾代替氢氧化,使合成取得成功;在合成2',6'-二甲基-4'-苯基-吖啶-9-甲酸酯时,文献方法对粗产品进行两次硅胶柱层析纯化,第一次柱层析用氯仿/乙酸乙酯(4∶1,V∶V)作溶剂和淋洗剂,第二次柱层析用己烷/丙酮(2∶1,V∶V)作溶剂和淋洗剂,按照文献方法得到的不是所需要的化合物,我们只进行第一次柱层析纯化,然后用己烷/丙酮(2∶1,V∶V)进行研磨,过滤,洗涤,除去溶于己烷/丙酮(2∶1,V∶V)的部分,得到所需要的产品。

Acridone 1 reacted with benzyl chlorides 2 in NaH/DMF/KI to give 10-benzyl-9-acridones 3 in high yields. Subsequent reduction of 3 with NaBH4 gave 10-benzy1-9,10-dihydroacridine derivatives 4 with yields of 88%~96%.

吖啶酮1与氯化苄及其衍生物2在氢化/N,N-二甲基甲酰胺/碘化钾中反应高产率生成10-苄基吖啶酮类化合物3; 3经硼氢化氢化还原生成10-苄基-9,10-二氢吖啶类化合物4,产率88%~96%。

The results show that the mineral compositions of feicui is more complex. Its main mineral is jade, and the other minerals are aegirine vryite and so on.

研究结果表明,翡翠的矿物组成比较复杂,主要矿物为硬玉,其次有霓石、透辉石、钙铁辉石、铬辉石和长石,还有少量绿泥石,铬铁矿,褐铁矿和赤铁矿等。

The feldspar in A-type granite is perthite, the dark alkali-minerals in which are arfvedsonite or manganese-bearing magnesia- arfvedsoniteand aegirine.

碱性花岗岩中的长石为条纹长石,暗色矿物为铁门石或含锰镁质铁门石及霓石。

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