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After sodium bisulfite reacted with methanal at 60-65℃ for 0.5h, aniline was dripped into the system to synthesize phenylaminomethyl-sodium sulfonate subsequently, the diazol solution of p-nitroaniline was dripped into phenylaminomethyl-sodium sulfonate synthesized to form 4'-nitro-4-aminoazobenzene. The compound was then added into diazol solution of p-chloroaniline to obtain the object product, which was identified by IR spectrum and element analysis.

在60~65℃温度下,亚硫酸氢与甲醛反应半小时之后滴入苯胺生成苯胺基甲基磺酸,另将硝基苯胺重氮化得到重氮盐溶液滴入苯胺基甲基磺酸中得到4'-硝基-4-氮基偶氮苯,然后将其滴入氯苯胺重氮化后的重氮盐溶液中,得经红外光谱检验和元素分析证实的目标产物。

The study shows that almost all the feldspar in the alkali-granite is perthite, the host-crystal is microcline, the chadcrystal could be either albiter or oligoclase. The Alkali-amphibole is either manganese-magnesia-arfvedsonite or arfvedsonite, and all the alkali-pyroxene is aegirine.

结果表明,该区富碱花岗岩几乎所有的长石均为条纹长石,主晶为微斜长石或高微斜长石,客晶为长石或更长石,碱性角闪石为含锰镁质铁闪石或闪石,碱性辉石均为霓石。

In this paper, the composition of zinc phosphating solution used at environmental temperature was researched. The composition is as followings: phosphoric acid 100 mL, monometallic sodium orthophosphate 20 g/L, zinc oxide 25 g/L, bluestone 1 g/L, sodium molybdate 1 g/L, sodium fluoride 1 g/L, tartaric acid 1 g/L.

研究了配制锌系磷化液配方:1 L溶液中加入磷酸100 mL,磷酸二氢20 g,氧化锌25 g,硫酸铜1 g,钼酸1 g,氟化1 g,酒石酸1 g。

The results indicated that among sodium dodecyl benzene sulfonate, sodium oleate and glycol, the sodium oleate has good effect.

结果表明,在十二烷基苯磺酸、油酸和乙二醇3种不同的表面活性剂中,选用油酸效果最好。

Application fields of sodium hexametaphosphate was summarized.Production technologies,mainly include two-step sodium dihydrogen phosphate production process and one-step phosphorus pentoxide production process of sodium hexametaphosphate,as well as advantages and disadvantages of various methods were introduced in detail.

综述了六偏磷酸的应用领域,并详细介绍了六偏磷酸的制备方法以及各种方法的优缺点,主要有磷酸二氢两步法和五氧化二磷一步法。

Objective: To explore the effect of intramuscular injection of midazolam before intravertebral anesthesia on sedation luring operation and amnesia after operation. Methods: Selected 180 ASA cases at 1~2 stage with lower extremity surgery under combined spinal and epidural anaesthesia, and randomly divided them into midazolam group and phenobarbital sodium group. Gave patients in midazolam group intramuscular injection of midazolam at 0.1mg/kg 10 min earlier before operation, while gave patients in phenobarbital sodium group 0.1 g phenobarbital sodium 30 mm earlier.

目的:探讨椎管内麻醉前肌注咪唑安定对术中的镇静作用和对术后遗忘的影响:方法:选择ASA1~2级择期在腰硬联合阻滞下行下肢手术的患者180例,随机分为咪唑安定组和苯巴比妥组,咪唑安定组患者入室后(实施麻醉前10min)肌内注射咪唑安定0.1mg/kg,苯巴比妥组患者入室前30min肌内注射苯巴比妥0.1g。

Gave patients in midazolam group intramuscular injection of midazolam at 0.1 mg/kg 10 min earlier before operation, while gave patients in phenobarbital sodium group 0.1 g phenobarbital sodium 30 min earlier. With Ramsay sedation evaluation assessed mean arterial pressure and heart rate during anesthesia, before and after operation, respectively.

选择ASA1~2级择期在腰硬联合阻滞下行下肢手术的患者180例,随机分为咪唑安定组和苯巴比妥组,咪唑安定组患者入室后(实施麻醉前10 min)肌内注射咪唑安定0.1 mg/kg,苯巴比妥组患者入室前30 min肌内注射苯巴比妥0.1 g。

The anti-bacteria effect of the soda lime can be influenced by the chemical response between soda lime and CO2, the bacteria in the patient airway may be polluting the ventilation system of the anesthesia machine, so the hospital cross-infection was present in this repeat use of soda lime and ventilation tube. The hospital infection can be effectively prevented by using the one time ventilation tube, the virus/bacteria filter utensil and/or rechange the soda lime in the general anesthesia.

石灰具有杀菌作用,全身麻醉石灰与CO2起化学反应会影响石灰的杀菌作用,连台手术气管插管全身麻醉病人气道细菌有污染麻醉机通气系统引起交叉感染的机会,使用一次性呼吸管道,并合理使用一次性病毒/细菌过滤器及时更换纳石灰可预防医院感染。

The bacteria culture was done for the endotracheal tube, the expiration and inspiration entrance of the anesthesia machine, and the soda lime in eighty general anesthesia patients. Results There are no bacteria growing in the new and the polluted new soda lime at the different stages.

对麻醉机的CO2吸收剂石灰进行不同时期细菌培养,菌株污染新的石灰进行菌落计数, 80例气管插管全身麻醉病人在手术麻醉结束前对病人的气管导管端、麻醉机的呼气端、吸气端、石灰行细菌培养。

The following experimental results are obtained:(1) Through the dissociation and ionization of sodium amide in a shock tube with a magic hole to provide sodium ions and electrons, the three-body recombination rate coefficient of sodium ion with electron is determined under the condition of argon atoms acting as the third body in the collision process:〓. The experimental temperature range is from 1400 to 2700K, extending the limitation of the flame method.

实验获得了如下结果:(1)在魔洞型单脉冲激波管上以氨基粉的高温分解和电离提供离子和电子,测定了以氩原子为碰撞第三体时离子与电子的三体复合速率系数〓,实验测量温度范围1400~2700K,拓宽了火焰方法测量结果的局限。

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