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Preparation of the cathode includes:shaping under the press of 40Mpa, sintering at 550℃for 1 hour and at 900℃for 8 hours and threading with molybdenum bar; Considering the literatures we choose CaCl2 as salt for preparation titanium. Pretreatment of salt is for 1 hour at 100℃and for 2 hours at 300℃. Partial pressure of oxygen which need lower than 5.11×10-7Pa to reduct titanium oxides and hygroscopic property of salt need a sealed equipment to electrolyse. And finally successfully designed a satisfied one and the results show that the equipment can be satisfied the requirment of the experiment. Flow of the inert gas is 1.5L/min, the voltage is 2.8 V, temperature is 850℃and time is 2 hours during pre-electrolysis. Flow of the inert gas is 0.2L/min, the voltage is 3.1 V, temperature is 900℃and time changes with the mass of TiO2 during electrolysis, namely the greater need the longer time; To eliminate influence of salt and other impurities, the products need to wash with distilled water and dilute chlorhydric acid , then wash with dilute hydrochloric acid under supersonic wave assistant. Finally, electrometical properties of the electrolysis of TiO2 is researched by cyclic voltammetry and chronoamperometry, and results show that there are two main reodox steps, namely from TiO2 to TiO and from TiO to Ti.

阴极制备主要包括40MPa压力下模压成型、两段式烧结(1小时内升至550℃保温1小时,再1小时升温至900℃保温8小时)及烧结后TiO2块打孔用钼棒串接三个主要环节;实验中选用CaCl2作为电解熔盐,并对其进行预处理(100℃,保温1小时; 300℃,保温2小时);经热力学计算,还原氧化物的氧分压至少要低于5.11×10-7Pa,结合电解过程中所用熔盐CaCl2有极强的吸水性的特点,电解装置应有较高的密封性,自行设计了一套密封性可靠的电解装置,便于实验过程中熔盐预处理和氧分压的控制;通过干燥处理预电解过程中Ar流量大约为1.5L/min、电压为2.8 V、温度为850℃、时间为2小时,电解过程中Ar流量大约为0.2L/min、电压为3.1V、温度为900℃,实验结果表明电解时间与TiO2质量密切相关,质量越大需要电解的时间越长;通过自来水冲洗—稀盐酸浸泡、洗涤—在超声波辅助作用下稀盐酸洗涤,可减少熔盐及其它杂质对电解产物检测结果的影响;最后,通过循环伏安法、计时电流法对电解机理的研究,确定电解还原TiO2制备金属主要经历了TiO2-TiO-Ti的过程。

using computer-aided designation2-D titanium armor plates could obtain the better clinal effect.

应用数字化成型二维网修复体修复颅骨缺损的效果优于三维易塑型网修复体。

The invention discloses a synthetic using method of smelting high-furnace dust, which comprises the following steps: grinding the high-furnace dust with 1.5-15% zinc; proceeding magnetic cobbing; reclassifying to obtain the refined ferric ore; disposing ore tail through waste acid of titanium dioxide with 15-30% sulphuric acid; transmitting the zinc oxide in the solution at zinc sulfate pattern; separating solid and liquid solution through lime; obtaining refined zinc ore through S2-, CO32-, HCO3- ion; floating the immersed slag through neutral oil.

一种炼铁高炉炉尘资源综合利用的方法,含锌1.5%~15%的高炉炉尘经磨矿、磁选、重选回收铁矿物获得铁精矿,选矿尾矿用含硫酸15%~30%的白废酸处理,使其中的氧化锌以硫酸锌的形式转入溶液中,固液分离得出的溶液用石灰中和除铁后,再用S2-、CO32-、HCO3-离子沉锌获得锌精矿,浸出渣用中性油浮选获得炭精矿。该方法将白废酸和高炉炉尘结合在一起,使之成为互为所需的原料和试剂,有效地将两种废弃物变成了有价资源,较好解决了环境污染问题,同时又能产生好的经济效益。

In the condition of keeping F、 K、Na content fixed, To improve slag structure and raise slag melting point and viscosity, MgO content is raised and TiO〓 is added. the main content is as follows:(1) Keeping CaO/SiO〓 fixed, MgO content rises from 10% to 16%, the free running temperature goes up 106℃, the viscosity goe down at bigger than 1425℃, but difference is little; keeping /SiO〓 fixed, MgO content rises from 10% to 16%, the free running temperature rises 87℃, the viscosity rises too; adding TiO〓 to 5%, the free running temperature goes up 98℃, the viscosity rise a little.(2) Powder crystal x ray diffraction and microscopic analysis shows: increasing MgO content, the cuspidine will decreace or even disappear, the monticellite goes up with MgO content rising, keeping /SiO〓 fixed, Akermanite content goes up, for high melting point minerals appear or go up, the free running temperature of the slag bearing F is raised; Adding TiO〓, high melting point mineral—Perovskite forms, it can making other minerals'crystalling fast, it is the reason that TiO〓 raises the free running temperature of the slag bearing F.

2对测定粘度的冷凝渣所进行的X粉晶衍射及显微分析和鉴定表明,增加MgO含量,渣中枪晶石将减少甚至消失,而钙镁橄榄石则随MgO含量增加而增加,在/SiO〓不变时,黄长石含量也有所增加,高熔点矿物的出现和增加,提高了含氟熔渣的熔化性温度;加入TiO〓熔渣中将形成高熔点矿物-钙矿,钙矿的形成还促使黄长石的结晶,这是TiO〓提高含氟熔渣熔化性温度的根本原因。

The grains of 6063 aluminum alloy made of electrolytic low-titanium aluminum alloy are small equiaxed grains too.

本文介绍一种新的添加的晶粒细化方法,即电解加法,并研究了细化效果。

Based on the experiment, microstructure and mechanical properties of the material in heating area of Ti-6Al-4V alloy were further analyzed under multi scanning, and the microstructure transfers from small equiaxial αβ+ to large 'α martensite.

在工艺试验的基础上,本文进一步对多次扫描条件下Ti-6Al-4V合金的微观组织与力学性能进行了测试分析,结果发现经过多次扫描后扫描区的微观组织由细小的等轴αβ+组织向粗大的马氏体'α组织转变。

Titanium ethoxide was directly prepared using titanium as sacrificial anode in absolute ethanol.

采用海绵为&牺牲&阳极,在无隔膜电解槽中,电化学一步法制备了纳米TiO2 前驱体酸乙酯Ti 4 。

We have tested several terrestrial samples, such as Mo, Ti, Ni, ilmenite, titanite, rutile, pyrite, forsterite and melilite. We have also attempted to analyze our first meteorite sample.

我们已经测试了许多地球标本,包含了钼、、镍与铁矿、楔石、金红石、黄铁矿、镁橄榄石和方柱石,同时也尝试了我们第一个陨石的标本。

In this regard, our goal is to develop a glow-discharge method to functionalize titanium surfaces by the covalent immobilization of bioactive organic molecules.

金属圆片先以氩气电浆去除表面污染物,来产生可重复取得的清洁表面,接著用丙烯胺电浆处理,使丙烯胺聚合在金属表面,再以交链剂戊二醛将白蛋白与丙烯胺的胺基(-NH2)键结。

Effects of sulfate ions and hydrolytic temperature on the TiCl4-derived TiO2 powders properties were investigated in detail.

研究了四氯化水解法制备的二氧化纳米晶工艺中水解温度和硫酸根离子对粉体性能的影响。

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The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了,排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意,我建议我们在价格上大家各让一半。

After an hour and no pup, look for continued contractions and arching of the back with no pup as a sign of trouble.

一个小时后,并没有任何的PUP ,寻找继续收缩和拱的背面没有任何的PUP作为一个注册的麻烦。