钒酸

The research on the new process of vanadium extraction from vanadium containing stone coal by acid leaching under oxygen pressure is described.

介绍了含钒石煤氧压酸浸提钒新工艺的研究情况。

In China,the extracting vanadium from stone-coal on the circs of investigation and the craft status quo were summarized in this thesis,and the traditional craft and the new craft of oxygen pressure acid leaching were contrasted.

综述了我国石煤提钒的研究情况和工艺现状，对目前我国石煤提钒传统工艺和改进工艺进行了分析评述，并介绍了氧压直接酸浸出提钒新工艺，提出了我国石煤提钒工艺应有的发展方向。

NMR and ESI-MS techniques were used to study the interactions between diperoxovanadates and small organic molecules such as pyridine, imidazole, arginine, picoline ester, and picoline amide. Spectroscopic methods were established to explore this type of interactions.

在合成数种双过氧钒化合物的基础上，利用多种NMR技术结合ESI-MS等谱学方法系统研究了双过氧钒化合物和咪唑、吡啶、取代吡啶、精氨酸、皮考啉酯以及皮考啉酰胺等有机配体的相互作用，建立了一套适合研究过氧钒化合物与有机小分子相互作用的谱学方法。

Although the charge number of isopoly and heteropoly anion was high, they existed mainly in aqueous solution as trivalent and tetravalent anions transferred across the W/NB interface.

系统研究了同多钼酸、同多钨酸、磷钨杂多酸、钒取代的磷钨杂多酸和双1∶11的镝的硅钼杂多酸阴离子在W/NB界面的转移行为，探讨了转移机制和它们在溶液中的存在形式，并计算了有关界面的热力学和动力学参数。

The results show that the optimal parameters of this technique are as time of 3 h, temperature of 150 ℃, ratio of liquor to solid of 1.21, H2SO4 additions of 25%, 85% material granularity of 0.095 mm. The one-step leaching percent of vanadium can reach 77%, the leaching percent obtain 90% after two-step countercurrent leaching. The vanadium leaching percent have growth and decline relation to occupation ratio of vanadium in in-soluble silicoaluminate mineral.

结果表明：该工艺的最佳工艺参数如下，即时间3 h、温度150 ℃、液固比1.21、硫酸用量25%、85%矿石粒度粒经小于0.095 mm；在此条件下，钒的一段浸出率为77%左右，而矿石经过两段逆流浸出后，钒浸出率可达90%；钒浸出率与矿石中难溶硅铝酸盐相中的钒占有率呈现消长关系。

The paper studied the semi-industrial test of extracting Vanadium pentoxide by the pelletization-rotary kiln roasting-low acid leaching-ion exchange technology from the Vanadium-containing kaolin.

对含钒高岭土进行了制粒-回转窑焙烧-低酸浸出-离子交换提取五氧化二钒的半工业试验，试验结果表明，回转窑焙烧过程钒的转化率达到74%以上，全流程五氧化二钒回收率达到71。

The paper studied the semi-industrial test of extracting Vanadium pentoxide by the pelletization-rotary kiln roasting-low acid leaching-ion exchange technology from the Vanadium-containing kaolin.

对含钒高岭土进行了制粒-回转窑焙烧-低酸浸出-离子交换提取五氧化二钒的半工业试验，试验结果表明，回转窑焙烧过程钒的转化率达到74%以上，全流程五氧化二钒回收率达到71.82%，产品质量达到国家标准GB3283-87要求。

The mechanism of vanadium removal from ammonium molybdate solution by ion-exchange was studied. It is found that V and Mo existing in ammonium molybdate solution are in the forms of V3O(superscript 2- subscript 9) and MoO4(superscript 2-), respectively, when V2O5 concentration is about 0.5g/L and the p!

对钼酸盐溶液离子交换钼钒分离机理进行研究研究结果表明，在钼酸盐溶液中V2O5含量约为0.5g/L，钒与钼在pH值为6.5~8.5的范围内分别以V3O(上标 3-下标 9)和MoO(上标 2-下标 4)的形态存在。

The results showed the content of acid soluble fraction, reducible fraction, oxidisable fraction and total vanadium showed positive relationship with the adding vanadium in soil, while residual fraction kept constant.

结果表明，土壤中酸可溶态、可还原态、可氧化态钒及总钒与钒施加浓度呈正相关，残渣态钒含量保持稳定。

The results showed that the mixed-addenda heteropolyacids H6PM o9V3O40,H10PMo5V7O40and H11PMo4V8O40 c an improve the conversion of 2-octanol,selectivity for hexanoic acid and the r ate of production.When the amounts of heteropoly acid are 14%,10%and 14% of the weight of 2-octanol,co...

结果表明：H6PMo9V3O40、H10PMo5V7O40、H11PMo4V8O40等多元杂多酸均可提高仲辛醇的转化率、己酸产率和己酸选择性，并确定了这3种催化剂的最佳用量：当它们分别为仲辛醇质量的1 4%、1 0%、1 4%时，仲辛醇转化率可达98 3%、97 6%、100%；己酸的选择性可达85 7%、85 8%、78 8%；其性能明显优于钒催化剂。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。