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We investigated constituent of triterpenoid saponins ofAlbizzia, two new compounds together with two known compounds were isolated from Albizzia julibrissin Durazz. by using column chromatography (macroreticular resin, silica gel, Sephadex gel, reverse phase silica gel),preparative HPLC methods et al.On the basis of spectroscopic analysis, including IR,ESI-MS,~1H-NMR,~(13)C-NMR,HMBC,HMQC,~1H-~1HCOSY and chemical methods, the structure of two new compounds were identified as 3 - O -[β-D-xylopyranosyl(1→2)-β-D-fucopyranosyl (1→6)-β- D -2- deoxy - 2 - acetoamidoglucopyranosyl] -21-O-[(6S)-2- trans- 2,6-dimethyl - 6 - O-β- D - quinovopyranosyl -2,7- octadienoyl] - acacic acid- 28 - O-β-D-glucopyranosyl(1→3)[α-L-arabinofuranosyl(1→4)]-α-L-rhamnopyranosyl(1→2)-β-D-glucopyranoside acacic acid 3- O -β- D- glucopyranosy(1→3)-β- D- fucopyranosl(1→6) [β-D- xylopyranosyl (1→2)]-β-D-glucopyranoside ;two known compounds were acacic acid lactone 3- O -β-D- xylopyranosyl-(1→2)-β-D-fucopyranosl (1→6)- 2-deoxy -2 -acetoamido -β-D- glucopyranoside ; acacic acid lactone 3- O-β-D-xylopyranosyl(1→2)-α-L- arabinopyranosl (1→6)- 2- deoxy - 2- acetoamido -β-D-glucopyranoside . The study lays chemical foundation and chemical reference substance for enhancing quality standard of Albizzia julibrissin Durazz.

本研究论文在综述国内外对合欢属Albizzia三萜皂苷化学成分和药理作用研究进展的基础上,利用传统植化分离手段和现代分离技术,包括大孔树脂、硅胶、葡聚糖凝胶、反相硅胶等柱色谱,制备高效液相色谱法等技术从中药合欢皮中分离得到了4个化合物,其中,2个新化合物和2个己知化合物,并进一步通过现代分析技术IR,ESI-MS,~1H-NMR,~(13C-NMR,HMBC,HMQC,~1H-~1HCOSY等和化学方法鉴定了2个新化合物的结构分别是:3-O-[β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖基]-21-O-[(6S)-2-反式-2,6-二甲基-6-O-β-D-吡喃鸡纳糖基-2,7-辛二烯酸基]-金合欢酸-28-O-α-L-呋喃阿拉伯糖基(1→4)[β-D-吡喃葡萄糖基(1→3)]-α-L-吡喃鼠李糖基(1→2)-β-D-吡喃葡萄糖苷,金合欢酸3-O-β-D-吡喃葡萄糖基(1→3)-β-D-吡喃夫糖基(1→6)[β-D-吡喃木糖基(1→2)]-β-D-吡喃葡萄糖苷;2个已知化合物结构分别是:金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷,金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-α-L-吡喃阿拉伯糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷。

Cavalli's signature animal prints were confined to a leopard coat and a giraffe pattern (faintly stamped on a suede jacket), as well as to the backstage VIP area. And the Florentine artisanal treatments that are another signature were present in the way that leather and suede were subtly tooled (one skin had a striking brocade effect). A suede duffel lined in astrakhan and a closing coat of lustrous monkey fur evoked the willful, rockin' excess of alt-Cavalli (which is, face it, how the world learned to love him).

放眼望去整场秀,我们一直看到重复搭配的西服套装/套头毛衣/衬衫和领带、合腰身的剪裁以及锐利平整的肩线,直至快结束时,Roberto Cavalli招牌的动物图纹皮草单品才华丽豋场:如美洲豹、长颈鹿花纹的麂皮大衣(当然据说在后台VIP室也是布置满满动物花纹);而佛罗伦斯老牌工匠们织造手法的精湛,更不著痕迹表现在那些温暖厚实的大外套上:像是麂皮外套内里的稀有阿拉斯加卷毛羊皮、牛皮夹克上金线织花的细腻图样、以及经过特殊处理闪烁光泽的猴子毛短外套。

Objective: To investigate the effects of staphylococcal enterotoxin A and B in the pathogenesis of atopic dermatitis.

目的:探讨金葡菌肠毒素A和金葡菌肠毒素B在特应性皮炎发病机制中的作用。

At El Sordo's camp Pilar exchanges badinage with Joaquin, a young man who wanted to be a bullfighter before the war, while Jordan confers with the leader.

在"聋子"的营地,趁着乔丹同那位队长商议的空当,皮拉尔跟华金相互打趣起来。华金是个年轻小伙子,战前曾想当名斗牛士。

Http://www.zshare.net/audio/671213750036217a/ Yungztuh 403 tha realest on da scene triple beam only seventeen yungin dont give phuc lazz it down foh ma homies on da streets nay mean fake ass snake be ducking around running around like their in a phuc'in track meet so im comming back wid da fourty five leave these hataz 6 feet deep and still alive ima keep it live yo foh son young asian cat wid da gun, dis 187 shiet has just begun want beef 2 sicc wid dis leave ya deseased rest in piss on avenue corner of your block straight banging dis set till midnight clock batttle field got da caps peeled back on side be chillin makin these tracks makin these paper stacks rising these tax on these foos young and dangerous u see cant phuc wid a asian g burry your carcus in a cemetary bettah know yo place laz it down 403 soaked up on hennessy, give ya hataz a taste give me face or ya whole life will be a waste...

http://www.zshare.net/audio/671213750036217a/ Yungztuh 403三重塔realest梁大舞台上只有17 yungin不要给伏lazz下来文物之友达街道马兄弟,在NaY平均假像蛇屁股回避他们的周围到处乱跑在phuc'in田径运动会等即时通讯回来妇女参与发展达45给这些hataz 6 英尺深,仍然活着的IMA保持住哟亚洲青少年文物之友子猫妇女参与发展的大枪,解散187 shiet刚开始要牛肉二上咨妇女参与发展的存款保险计划给你块遐deseased休息角落小便大道直上敲打时钟设置,直到午夜解散batttle外地回来了侧面大帽去皮这些轨道是待在马金马金纸堆上升这些ü税这些福斯古惑仔妇女参与发展的一个倾斜伏见亚洲克伯里公墓bettah您卡库斯在知道哟地方拉撤路下来浸泡轩尼诗了403起,给予亚hataz味道给我的脸庞,还是遐一生将是一个废物。。。

Hongsheng specializing in the production of decorative materials such as: special silver, black, silver pieces, small horizontal line, gold line, gold pieces, 1 / 4 gold box, gold line spectrum, Silverstrand spectrum, gray gold stripes, black gold stripes , pearl white, pearl black, pearl light gray, dark gray pearl, red laser wire, white wire laser, laser transparent silk, gray silk laser, laser dark gray silk, silk blue laser, red wood, silver gray in stripes, blue silver box and so on.

鸿盛专业生产装饰材料如:银特,黑皮,银碎,小横线,金横线,金碎,1/4金方格,金线谱,银线谱,灰金条纹,黑金条纹,珠光白,珠光黑,珠光浅灰,珠光深灰,红镭射丝,白镭射丝,透明镭射丝,灰镭射丝,深灰镭射丝,兰镭射丝,红木纹,银灰中条纹,兰银方块等等。

NSG had acquired a 20% stake in the British company; Pilkington had bought some American firms in which NSG had a stake.

NSG先是获得了皮尔金顿公司的20%的股权,随后皮尔金顿收购了NSG拥有股权的一些美国公司。

Guangdong Gold Coast giant renowned global brand building, Austrian Peter window hardware, Knauf insulation materials, Dili Krupp Elevator family Pilkington Low-E glass sea Habitat, Germany Taino Wind Sealing Technology , pure noble descent in Europe and America, with the Canton real estate, luxury sea view new movement in China.

金广东海岸荟萃全球建筑品牌巨擘,丝吉利亚-奥彼窗门五金件、可耐福保温材料、帝森克虏伯电梯世家、皮尔金顿Low-E海居玻璃,德国泰诺风密封技术,纯正欧美贵族血统,与金广地产,共谱中国海景豪宅新乐章。

Gibson's first "semi-acoustic" the ES-335, which was neither totally solid nor fully acoustic, is the guitar of choice used by many famous guitarists such as Andy Summers, Elvin Bishop, Lee Ritenour, Jay Graydon, Robben Ford, Freddie King, John McLaughin, Jimmy Page, Chuck Berry, Tony Mottola, Johnny Rivers, Jack Wilkins, Bono, Grant Green, Eric Clapton, Stevie Ray Vaughan, Alvin Lee, BB King, Emily Remler, Otis Rush, Pete Townshend, John Lee Hooker, and Larry Carlton.

吉布森的第一个"半声"的ES - 335,这既不是完全稳固的,也不可能完全声,是由诸如安迪萨默,埃尔文主教,李莱特诺,杰伊格雷顿,罗本福特,弗雷德金许多著名吉他手使用的选择吉他约翰McLaughin,吉米佩奇,查贝里,托尼莫托拉,约翰尼河流,杰克威尔金斯,波诺,格兰特绿色,埃里克克莱普顿,史蒂维雷沃恩,阿尔文李,比比金,埃米莉Remler,奥的斯拉什,皮特汤森,约翰李胡克,和拉里卡尔顿。

Funded bypass road to facilitate the procurement of seedlings of flowers around the visitors, we have the varieties: Jinshan Spiraea; Gold Flame Spiraea; large day lily flower; Medicago Iris; Euphorbiae; Euonymus fortunei; Ivy; Yingchun; fruit pomegranate; pomegranate flower; persimmon; wistaria; Rosaceae; sumac;úìè; Japan Cherry blossom; Sorbaria sorbifolia; lu tong; red roses; Red Prince Weigela; Prunus cistena;×; Ruby Begonia; paste Haitang rod; Malus micromalus; Diamond Begonia;Begonia;·; beauty Mei; leaves Betau; green Betau; Euonymus; Buxus microphylla; North Korea boxwood; Euonymus; Jiaodong Euonymus; Golden God vicaryi;ìé; Empoasca berbamine; clove; Ziwei; Hibiscus; phillyrin; bauhinia; gold and silver wood; honeysuckle; Huang Rosa; Phnom Penh Water Prince; Hung Shui Mu; Lamei; Taiping flower; wood Hydrangea; ping sticks Xunzi; silk wood; Floribunda Roses; large flower Rose; Mannheim Rose; red rose; Kim Mary Rose; Jintaiyang; laughter;±±èí; tower cypress; sand vulgaris;÷°; Henan cypress; cypress hodginsii ball; Xi'an cypress; Shu cypress; side cypress; tabulaeformis;¤white; cedar; Longbai; spruce; Magnolia; Dianthus plumarius; multicolored carnation; by Carnation; Phlox; Golden Caryopteris; sisal; Malanje; wood Hydrangea; Paeoniflorin; Canna; Cristata; short string of red; National Ju; Semiothisa;ú×±; acacia; Jiangnan Cassia;¨±; Amorpha fruticosa; Acacia;·¨; Paulownia;à; Chunnian 1000;÷; torch; game tree; Duzhong; Ginkgo biloba;·; Fraxinus; Xinjiang Yang; fast-growing Salix; willows; gordejevii; trowel head Liu; golden weeping willow ; bamboo: 124 varieties, such as, door-to-door if you purchase, we are very hospitable, the guests have a meticulous care, child Mindsto the bottom of the price, the best quality, best service, you Just check the number of points to check the quality of all organizations, sourcing, find a car load, are we responsible for.

出资修路搭桥,以方便各地来客采购苗木花卉,我们的品种有:金山绣线菊;金焰绣线菊;大花萱草;紫花鸢尾;地锦;扶芳藤;常青藤;迎春;果石榴;花石榴;柿子;紫藤;蔷薇;黄栌;美国红栌;日本樱花;珍珠梅;禄棠;红玫瑰;红王子锦带;紫叶矮樱;紫叶李;红宝石海棠;贴杆海棠;西府海棠;钻石海棠;垂丝海棠;榆叶梅;美人梅;红叶碧桃;绿叶碧桃;大叶黄杨;小叶黄杨;朝鲜黄杨;北海道黄杨;胶东卫矛;金爷女贞;红叶小檗;绿叶小檗;丁香;紫薇;木槿;连翘;紫荆;金银木;金银花;黄刺梅;金边水腊;红瑞木;腊梅;太平花;木绣球;平枝荀子;丝绵木;丰花月季;大花月季;曼海姆月季;红帽子月季;金玛丽月季;金太阳;欢笑;北京桧;塔桧;沙地柏;洒金柏;河南桧;桧柏球;西安桧;蜀桧;侧桧;油松;白松皮;雪松;龙柏;云杉;白玉兰;常夏石竹;五彩石竹;地被石竹;福禄考;金叶莸;剑麻;马兰;木绣球;芍药;美人蕉;鸡冠花;矮串红;国庆菊;国槐;龙爪槐;洋槐;江南槐;香花槐;紫穗槐;合欢;法桐;泡桐;青桐;千头椿;椿树;火炬;弈树;杜仲;银杏;五角枫;白腊;新疆杨;速生柳;垂柳;黄柳;镘头柳;金丝垂柳;竹子:等一百二十四个品种,你若上门采购,我们非常好客,对客人有着无微不至的照顾,童叟不欺,以最底的价格,最好的质量,最优质的服务,你只需检查质量点查数目,一切组织货源,找车装车,都有我们负责办理。

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I didn't watch TV last night, because it .

昨晚我没有看电视,因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来,在北京的很多小区里,电梯液晶电视被撤了下来。

I'm running my simile to an extreme.

我比喻得过头了。