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A new synthesis method of metal-free phthalocyanine using 1,3-diiminoiso- indoline as main material and trimethoxysilane as hydrogen donator was developed in this paper.

本文建立了以酞菁素为原料,喹啉为溶剂,三甲氧基硅烷为供氢剂,合成无金属酞菁的新方法。

It results from theformation of infusible salt or hydrates by the complexing reaction of metal ion andnegative ions in alkaline solution. The stability mechanism was discussed byemploying scanning electronic microscope and x ray photoelectronspectroscopy.

结果表明,在中性介质中,其稳定性较好,而在碱性介质中的稳定性较差,这是因为在碱性介质中金属离子与介质中的阴性离子络合形成难溶性的盐或氢氧化物,加速了GIC的分解所致。

Sulfide precursors were synthesized by conventional inorganic metal salts and a sulfurizing agent. Sulfide catalysts were prepared by isochoric impregnation using an impregnation solution containing sulfide precursors and a dispersion additive.

以常规金属无机盐及硫化剂为原料合成硫化物前驱体,在硫化物前驱体溶液中加入添加剂配成浸渍液,浸渍载体制成硫化型加氢催化剂。

The article introduces the anti-tumor and other pharmacologic effects of the isocoumarin s, reviews the methods of synthesizing isocoumarin s, and places an emphasis on introducing and comparing such methods of synthesizing syntheticroutes of dihydro isocoumarin s as ozone oxidation, organic metal sythesis, catalytic oxidation and so on.

介绍了异香豆素类化合物在抗癌和其他药理方面的作用,综述了异香豆素类化合物的合成方法,着重介绍其中的二氢类异香豆素化合物的臭氧氧化法、金属有机合成法、催化氧化法、分子间成环缩合法等合成方法,并进行了比较。

After As in WO3 is dissolved with NaOH solution, WO3 is coordinated by citric acid. In HCl medium, As is reduced to lwo valency As by KI and then low valency Asis reduced to gas AsH3 by SnO2 and metal Zn. After that, DDTC-Ag solution is applled as absorbent for colorimetric determinhtion.

用氢氧化钠溶液溶出三氧化钨中的砷之后以柠檬酸配位三氧化钨,在盐酸介质中用碘化钾将砷还原成低价砷,再用二氯化锡和金属锌将低价砷还原成砷化氢气体,以DDTC-Ag溶液吸收进行比色测定。

A method for removing sulfur compounds from gasoline was investigated involving the conversion of sodium metaborate to sodium borohydride by electrochemistry deoxidation and the incorporation of a kind of metal compounds.

研究了利用电化学方法将偏硼酸钠还原成硼氢化钠,并加入一种金属化合物,用于汽油脱硫的方法。

Based on the studies of moderate temperature isomerization catalysts carried out by domestic and foreign researchers, the paper systematically discussed the influence of a variety of factors in process of commercial preparation on the performance of catalyst which applied Pd as its metal component and HM as its acid carrier. The paper also explored the deactivated reasons of catalyst and its regenerating measure. Preparation of mordenite and scaled up production of catalyst, stability of catalyst was demonstrated in a 100kt/a commercial plant. The findings provide important basis for preparing Pd isomerization catalyst and industrial application.

本文在国内外学者对中温异构化催化剂及工艺研究的基础上,以钯作为金属组份,氢型丝光沸石作为酸性载体,系统研究了工业制备过程中各种因素对催化剂性能的影响,以及催化剂失活的原因及再生方法,进行了丝光沸石及催化剂的放大生产,并在10万吨/年工业装置上考察了催化剂的稳定性,为制备载Pd异构化催化剂及工业应用提供了重要依据。

Moreover, hydrogen passivation is beneficial to improve electricalproperties of cast multicrystalline silicon only after metallic impurities was gettered c

另外,氢钝化只有在金属杂质被吸杂之后才是最为有效的。

Niobic acid as a solid catalyst can be directly applied in the hydrolysis, esterification, condensation and alkylation reaction etc.

铌酸可直接作为固体催化剂,应用于水解、酯化、缩合、烷基化等反应中;铌酸也作为载体负载金属,应用于F-T合成、氧化反应和加氢等反应中;含铌化合物也可作为负载型催化剂,负载到不同类型的载体上;含铌化合物也作为助剂或光催化剂,广泛地应用于催化多种化学反应。

Generally, these compounds are derived from accessible α–oxoketen dithioacetals and the common methods of preparation involve regioselective sodium borohydride 1,2-reduce of α–oxoketen dithioacetals, 1,2-nucleophilic addition of organomatals such as organomagnesium, organolithium, Reformatsky regent to α–oxoketen dithioacetals, Baylis-Hillman reaction between polarized ketene dithioacetals and aldehydes.

主要方法包括:使用硼氢化钠1,2-选择性还原α-羰基二硫缩烯酮;利用有机金属化合物(如有机镁试剂,有机锂试剂,Reformatsky试剂等)对α-羰基二硫缩烯酮进行1,2-亲核加成;通过α-羰基二硫缩烯酮与芳醛进行Baylis-Hillman反应等获得。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。