金属氢

The Xray diffraction analysis of the compounds (3) and (4) shows the presence of an intramolecular coordination of oxygen to the tin atom giving rise to a fivemembered ring in which the metal exhibits a distorted trigonal bipyramidal geometry.

并通过X-射线衍射测定了（3）和（4）的晶体结构，其空间群均为P2〓/c，晶胞内分子数Z=4，分子结构是以锡原子为中心金属原子、含分子内O→Sn配位键五员环的扭曲三角双锥结构，碳碳双键的两个氢是顺式构型。

The second part is about that five-membered rings compounds were synthesised using aromatic aldehyde,α-bromoketone and imine ester in the present of zinc power.

2以芳香醛，α-溴代苯乙酮与氨基酸酯亚胺类化合物在金属锌粉的作用下，生成一系列的四氢吡咯化合物。

The main steps include as follows: CO2 is led into the mother liquor of sodium meta-aluminate to carry out carbon content decomposing; the primary separation between the aluminum and the gallium is realized by primary carbonatation to filter out sodium hydroxide; secondary carbonatation is carried out on the filtrate to obtain the deposit of the complex salt of gallium and aluminum; a sodium carbonate crystal is obtained after the filtered filtrate is condensed and vaporized; the deposit of the complex salt of gallium and aluminum is dissolved in the mother liquor of sodium meta-aluminate; the processes are repeated until the proportion of gallium and aluminum in the complex salt of gallium and aluminum is larger than 1/340; then the complex salt of gallium and aluminum is added into the NaOH liquor and electrolyzed, thus obtaining the metal gallium with a purity larger than 99.9 percent which reaches the level of 3; simultaneously, the byproducts of the aluminum hydroxide and the sodium carbonate during the process of carbonatation by steps are obtained.

主要步骤包括：向铝酸钠母液中通入CO 2 进行碳分分解，一次碳酸化实现铝镓的初次分离；过滤出氢氧化钠，滤液进行二次碳酸化获得镓铝复盐沉淀，过滤后滤液经浓缩蒸发获得碳酸钠晶体，铝镓复盐沉淀溶解在偏铝酸钠母液中，重复上述过程直至铝镓复盐中的镓铝比例大于1/340，将其加入到NaOH溶液中，电解可获得纯度＞99.9％的金属镓，达到3N级水平同时在分步碳酸化的过程中获得氢氧化铝和碳酸钠副产品。

The selective hydrogenation of crotonaldehyde to crotyl alchol was carried out over finely dispersed polyvinylpyrrolidone-stabilized ruthenium clusters.

以聚乙烯吡啶烷酮稳定的钌纳米金属簇为催化剂，进行了巴豆醛的选择性催化氢化。

The content of diffusible hydrogen in welded metal was determined according to the Glycerine method.

按照甘油法测定焊缝金属扩散氢的含量。

The welding wire thus obtained a weld containing not more than 5 ml of diffusible hydrogen per 100 g deposited metal.

这样得到的焊丝形成的焊件每100g熔敷金属含有不超过5ml的扩散氢。

A series of standards,such as GB/T 3965 、 GB/T 5117、GB/T 5118、GB 12337、 GB 50094、JB/T 4747 etc,have some different requirements of diffusible hydrogen content in deposited metal.

通过GB/T 3965、GB/T 5117、GB/T 5118、GB 12337、GB 50094J、B/T 4747等标准焊条熔敷金属扩散氢方面要求的不一致进行阐述，对相关标准的编制以及球形储罐高强低合金钢焊条的使用与管理提出了一些建议。

Bromoesters can react with diselenide s by metallic tin in THF to give α-selnoesters in moderate togood yields.

本文报道在四氢呋喃中通过金属锡促进α-溴代酯与二硒醚反应生成α-硒代酯，反应条件温和，产率良好

It was revealed that they all had better electrocatalysis than graphite electrode.

研究表明，与石墨电极相比，金属/聚吡咯电极对电解析氢反应有较好的催化性能。

Supported noble metallic catalysts were prepared with different kind of noble metals and of supports,their catalytic performance for furoic acid hydrogenation were investigated in fixed bed micro-reactor in water under different conditions such as reaction pressure,temperature,H2 space velocity,space velocity of furoic acid and solvent and so on.

采用水作溶剂的固定床操作系统，用钌、铑、钯、铂等作为担载金属，氧化硅、活性炭、γ-三氧化二铝等作为载体，制备了多种负载型催化剂，评价了它们的糠酸选择性杂环加氢催化性能。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。