金属化

Secondly,a mixture of acetone and methyl formate was added into the methanol solution of sodium methoxide to prepare sodium formyl acetone by Claisen reaction.

以金属钠为原料，甲醇为溶剂，先制成甲醇钠的饱和甲醇溶液，再滴加丙酮和甲酸甲酯进行Claisen酯缩合制得丁酮烯醇钠，最后在强酸作用下与甲醇进行缩醛化反应合成了4，4-二甲氧基-2-丁酮，过程总收率达到73.1%，纯度98.7%。

The I-V characteristics of the diodes with 100μm diameter indicated that as the densities of V-defects on GaN films increased from 4.1×105cm-2 to 1.03×107cm-2, the Schottky barrier height decreased from 1.44eV to 1.19eV and the reverse bias leakage current at -1V is increased sharply from 10-10A to 10-7A . Further studies on a single V-defect using conductive atomic force microscope demonstrated that the value of forward current biased at 8V at V-defect side-walls appears to be one order higher than that of plain region, indicating that the conductivity mainly occurred at the side-walls of V-defect.

实验结果发现，随著V型缺陷密度由4.1×105cm-2增加至1.03×107cm-2，在氮化镓表面蒸镀镍金属所制成直径为100μm的萧基元件之所属能障从1.44eV下降至1.19eV，而且在-1V的操作下反向偏压漏电流从10-10A急遽的攀升至10-7A；为了了解V型缺陷对厘米尺寸n-GaN萧基元件电流传导机制之影响，我们进一步的利用导电原子力显微镜(Conductive Atomic Force Microscopy， C-AFM)，特别针对单一个V型缺陷进行微观电性之量测。

Granulate metal powder to obtaion regular spherical shapes of granulated powder which has high fluidity.

造粒机是专门设计用于对金属粉末进行颗粒化，以获得有规则的球形，目的在于使其在要进行冷压的刀头内具有高的流动性。

Effects include painterly look, line halftone (engraving, woodcut, guilloche, TV-screen), metallic effect, misc softening, sharpening, hi pass and edge-emphasizing methods.

特效包括美术外观，直线网板画（雕刻，木雕，连环节装饰，电视屏幕）金属效果，混杂软化，锐化以及边缘强化方法。

The results showed that the light stabilizer BHW1 by adding component chelating metal ion in HALS complex had better light stability and balanced performance than other HALS complex .

实验表明：引入金属离子螯合剂组成的复合光稳定体系BHW 1在农用聚烯烃棚膜中应用效果良好，具有更为均衡的光、热稳定性能；自然曝晒实验和大田实验证明复合受阻胺光稳定剂的光稳定性能优于单组份光稳定剂，光稳定剂复合化是聚烯烃防老化最有成效的解决方式之一。

The preparation of cabalt nanoparticles by the reduction of Cobalt chloride hexahydrate with Sodium borohydride in the reverse microemulsion solutions of water/ Didodecyldimethylammonium bromie/ toluene was investigated. i changed the Cobalt chloride hexahydrate concentration in the Didodecyldimethylammonium bromie/ toluene system to analysis the particle size.

在water/ Didodecyldimethylammonium bromie/ toluene的逆微乳化系统中，本人以硼氢化钠来还原系统中的Co的金属前驱盐氯化亚钴来做研究，在实验中本人改变在Didodecyldimethylammonium bromie / toluene系统时的氯化亚钴浓度以改变粒子的大小，本人也尝试改变反应的速度来研究对奈米粒子生成时所造成的影响。

Superscript 3C NMR spectra for metallocene polyethylenes were measured to confirm the existence of various branches from methyl to hexyl end longer chains and other structural units. DRI from rheological data were used to determine the level of long chain branching in mPEs, and the results were compared with each other.

采用高分辨度(上标 13)C NMR谱直接测定茂金属聚乙烯的支化度及其他微量异种结构单元的组成，并过流变数据获得DRI指数来表徵mPEs长支链结构；对二者的结果进行了比较。

Results The expression of MMP-2 and MMP-9 was detected in normal anterior hypophysis, non-invasive and invasive macropituitary adenomas.

采用免疫组化SP法检测正常垂体前叶组织、侵袭性和非侵袭性垂体腺瘤组织中基质金属蛋白酶-2和9及其组织抑制因子的表达，结果进行统计学分析。

In the immiscible Cu-Mo system, alloying was realized in a broad composition range. When the Cu content in the samples is less than 50 at.

在互不固溶的Cu-Mo系统中，利用IBAD方法在很宽的成分范围内实现了两种金属的合金化。

Using the method of linear response theory in lattice dynamics on the basis of Tyson's model, the response displacements of atoms on cleavage plane at the incipience of brittle fracture was derived and an expression for evaluating brittle fracture surface energy of metals was found.

本文在Tyson模型的基础上，应用点阵动力学线性响应的理论方法，导出了脆断发生时解理面上原子的响应位移，并进而给出金属脆断表面能的计算公式。这种处理方式既保持了解理断裂面是结晶的表现，避免了局域"熔化"和"沸腾"模拟脆断的简单模型中出现的非晶化问题，也对解理面上原子临界位移做了合理估计，避免了人为规定临界位移的随意性，同时，从理论上得出的脆断时产生的声发射信号与实际探测到的量级相近。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。