金属

Because of the fuel-rich propellant's high heat value and combustion temperature, the common stainless steel crucible and oxygen bomb's parts are always burned in the combustion heat testing process. In order to realize the proper testing of combustion heat, some fireproof materials characteristics and their application in the combustion heat testing of fuel-rich propellant were studied. Those fireproof materials include acid washing asbestos, C/C compound materials, Al2O3 chinaware and tungsten crucible.

含金属富燃料推进剂由于热值高、燃温高，在燃烧热测试过程中普通的不锈钢坩埚及附件经常被烧毁，为了正确测试金属富燃料推进剂燃烧热，对酸洗石棉、碳／碳复合材料、Al2O3陶瓷坩埚和金属钨坩埚的基本耐烧蚀特性和在金属富燃料推进剂燃烧热测试中的应用进行了实验研究。

In order to analyze the influence of filled metal particles on impact force for hydraulic pile hammer, analytical solution of mathematic model for pile hammer filled with metal particles considering effects of metal particles was presented. In the solution, lumped mass were used as metal particles, a spring was used as contact stiffness between metal particles and hammer body, different variable lumped masses were used as pile hammer, the ram and anvil, a spring and a dashpot were used as the anvil cushion and pile respectively.

为分析填充金属颗粒对打桩锤锤击力的影响，考虑填充金属颗粒的作用，用集中质量块表示填充的金属颗粒，用弹簧模拟金属颗粒与锤体相碰处的接触刚度，用不同的集中质量块表示桩锤、砧座和桩帽，用并联的弹簧、阻尼器表示锤垫，用弹簧表示桩垫，用阻尼器表示桩，建立了平衡方程。

All the compounds are characterized by IR and elemental analysis.we design and prepare a bipyridinium supramolecular compound and six coordination compounds, which are also characterized by IR, elemental analysis and X-ray structure analysis. According to X-ray structure analysis, hydrogen bonds and n-n stocking interactions participate in the architecture of three-dimensional framework [H2L1 (NO3)2 (H2O)2]n; one-dimensional zigzag coordination polymer [Hgl21.5CH3OH]n; binuclear metallamacrocycle (HgI2L2)2 3H2O; helical double-stranded one-dimensional coordination polymer [Co2(L2)2-2CH3OH]n; double-stranded one-dimensional coordination polymer [Co2(L3)2-CH3OH-CH3CN]n; and three-dimensional compound [Cu(C5H4NCOO)2(H2O)2]-H2O with hydrogen bonds, three-dimensional coordination polymer {[Cd(C5H6NCOO)2H2O]-DMF}n, which are indirectly obtained from the precursor ligand L3 through metal ion induced the hydrolysis of diamide and self-assembled with the hydrolyzate.

我们首次合成了一个双吡啶鎓超分子化合物和六个过渡金属配合物，并通过IR谱，元素分析和X-ray晶体衍射分析对它们进行了表征。X-ray晶体结构分析表明：超分子化合物[H_2L1·(NO_3)_2·(H_2O)_2]_n是由多种氢键和芳香环间的π-π堆积作用构建的三维无限结构；[HgI_2(L1)·1.5CH_3OH]_n是一维锯齿状配位聚合物；(HgI_2L2)_2·3H_2O是双核金属大环化合物；[Co_2(L2)_2·2CH_3OH]_n是具有一维双螺旋结构的配位聚合物；[Co_2(L3)_2·CH_3OH·CH_3CN]_n为一维双链结构的配位聚合物；以及由非直线形配体L3在金属离子Cu和Cd的诱导作用下发生水解，并且金属离子与水解产物——异烟酸根离子自组装，形成了三维氢键超分子化合物[Cu(C_5H_4NCOO)_2(H_2O)_2]·H_2O和三维配位聚合物{[Cd(C_5H_6NCOO)_2H_2O]·DMF}_n。

The former is to prepare polymolybdates coordinated' directly by organic ligands using Na2MoO4 and MoO3 precursors; The latter plays emphasis on exploiting a simple and effective routine to synthesize Keggin polytungstates in which the transition metal or Si acts as the heteratom by reaction precursor Na2WO4.We have synthesized a 4,4'-bipyridine bridging dumbbell-like polymolybdates a metatungs...

前者主要是制备有机配体键合的多金属钼酸盐；后者重点是探索出一个简易、有效的合成过渡金属或主族元素硅作杂原子的Keggin多金属钨酸盐的方法，然后通过变换过渡金属或有机配体的种类探讨对产物结构的影响，再对所得化合物的结构和组成通过物理测试手段进行表征，同时研究其在光、电、磁等方面的性质。

Furthermore, Taiwan's metal industry had lost its soul, not only becoming immutably making standard products and counterfeits, but also performing the mass production for foreign companies.

除了杨英风艺术大师的创作外，反观台湾在日据时代过后并未能见到金属工艺的长足精进，台湾本土的金属工艺品并未被社会所重视，大众总是偏爱外国产品，从贵重首饰、家俱摆饰到户外景观随处可见进口货，而台湾的金属工业也失去了自我的灵魂，除了一味地制造一成不变的标准品及仿冒外，要不就是成为外国厂商的代工者，而精致金属工艺则往往只能见於各个艺术家个人的表现。

Cables and wires of common metal; ironmongery, small items of metal

普通金属及其合金，金属建筑材料，可移动金属建筑物，铁轨用金属

The metallic bond has made develop the energy band theory arriving at a metallic bond , concrete annotation of model angry from classical free electron the nature that the metallic bond forms and metal crystal physical property.

金属键由经典的自由电子气模型发展到金属键的能带理论，具体地诠释了金属键形成的本质与金属晶体的物理性质。

However, the thermal stability of metallic coordination polymer hardly enhanced in comparison with the polymer never coordinated transitional metallic ions. The reason might be that the energy of coordinate bond formed between metallic ion and polymer was trival in comparison with that of covalent bond in polymer. It started with coordinate bond when the coordinate polymer decomposed under high temperature, so it engendered little for the thermal stability at high temperature.

而金属配聚物较未配位金属的配体高温热稳定性提高不大，可能是由于金属离子与配体之间形成配位键的键能与配位体内的共价键键能相比要小得多，当金属配聚物受热裂解时，首先从配位键开始，因此对高温热稳定性的影响甚微。

A preparation method of nickel oxide-base cathode of fused carbonate fuel cell is to select alkali earth metal oxide, transition metal oxide and rare-earth metal oxide, mix with carbonyl nickel powder in the proportion of 0.01-15.00 mol%, add assistant and mix even into a slurry; after the slurry is formed into a biscuit by doctor-blade casting, sinter it into a multi-porous nickel plate; dissolve lithium nitrate and cobaltous nitrate with mole ratio of Li:Co-1:1 and citric acid or PVA in the distilled water to make a solution with Li of 0.00-0.5 mol/L; immerse the multi-porous nickel plate or nickel oxide plate in the solution, keep for 10-60 minutes under vacuum below 200 millibar, then dry in an oven at 75 degrees centigrade further transfer to a crucible electric furnace preheated 650 degrees centigrade for keeping the temp.

要約 熔融碳酸盐燃料电池氧化镍基阴极的制备方法属于燃料电池领域。选取碱土金属氧化物、过渡金属氧化物和稀土金属氧化物，按0.01－15.00mol％的比例与羰基镍粉混合，加入助剂，混合均匀成浆料；混合浆料流延成型为素坯后烧结为多孔金属镍板；将摩尔比为Li∶Co＝1∶1的硝酸锂和硝酸钴以及柠檬酸或聚乙烯醇溶于蒸馏水中，制成为0.005－0.5mol/L的溶液；将多孔金属镍板或氧化镍板浸入溶液中，在真空度低于200毫巴下保持10－60分钟；置于75℃的烘箱中烘干，转移至预热到650℃坩埚电炉中保温1－10小时；将此过程重复一次或多次即可。

However, it is hard to prepare high valent Mn complexes with ligand with only neutral chelating nitrogen atom of two dpa arms in 〓. In order to get a Mn dimmer complex with high oxidation states of manganese to increase the possibility of storing more oxidizing equivalents necessary to oxidize water evolving oxygen, some N atoms are replaced by anionic phenolate groups.

本文以高价金属的稳定、氧化还原性能的改善、各金属离子之间联系的增强等作为主要研究内容，来改进以往模型中金属价态较低，氧化还原电位高，不利于形成氧化活性中间体；多核配合物的研究较少，且各金属活性中心相互协同作用弱等问题。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。