量热

The effects of 1, 4-dinitropiperazine on the combustion characteristics and thermolysis of CMDB propellants were studied by differential scanning calorimetry and burning rate test.

用燃速测试和高压差示扫描量热法试验，研究了 N，N -二硝基哌嗪逐渐取代改性双基推进剂中的黑索今后，对推进剂燃烧性能和热分解特性的影响。

Their structure and thermomagnetic properties were studied by DSC, XRD and SQUID.

采用示差扫描量热法，X射线衍射和超导量子磁强计研究了其结构与磁热性能。

Preliminary study of the modification mechanism thermal stability of the membrane was performed by using fourier transform infrared spectrophotometry-attenuated total reflectance and differential scanning calorimetry.

研究硼酸对丝胶／聚乙烯醇膜材料的力学性能和耐溶失性能的影响，利用红外光谱分析和差示扫描量热分析研究硼酸对材料的改性机制和热稳定性。

In this paper migration theory and techniques related to the high-energy TEGN gun propellant are presented, and some methods determining the migration of RDX are analyzed and compared. As a result, chemical and thermal analyses are employed associatively to test the content of RDX in different position of TEGN gun propellant stored different period. The antimigration capability of TEGN gun propellant making use of two different granularity of RDX is also been studied.

本文以高能太根发射药及其相关技术为研究对象，分析研究了迁移理论以及目前国内外测定RDX迁移性能的方法，对这些方法的优缺点进行了比较，并采用化学分析法、热失重法、差式扫描量热法相结合的方法对各种不同储存时期高能太根发射药不同部位中RDX含量进行了测定，研究了使用两种不同粒度RDX制备的太根发射药的抗迁移性能。

Thermal stability and structure of Dy-Gd-Co-Al alloys were investigated by differential scanning calorimetry and X-ray diffraction, respectively.

并利用差示扫描量热计分析Dy-Gd-Co-Al合金的热稳定性、用X射线衍射仪来确定合金的结构。

The crystalline behavior and mechanical properties of the blends were investigated by differential scanning calorimetry and tensile measurements.

用差示扫描量热仪和电子拉力试验机分别测定共混物的热性能和力学性能。

By the testing means of electron-spectroscopy for chemical analysis , thermogravimetric analysis , differential scanning calorimetry , transmission electronmicroscopy , the results have shown that the emulsion polymerization in situ in the presence of nano-particle of calcium carbonate can happen smoothly and successfully and the surface of nano-particle of calcium carbonate have been capsulated by polymer of acrylates, which prevent from the agglomerating of nano-particles of calcium carbonate. Because the copolymer of acrylate has good compatibility with some plastics such as PVC, ABS, AS and so on, so the dispersion of nano-scale calcium carbonate as nanometer size in these plastics can be reached more easily and the effects of nanometer can happen.

通过X射线光电子能谱、热失重分析、动态扫描量热分析、透射电子显微镜等手段，证实在纳米碳酸钙原生粒子存在下，可以进行丙烯酸酯类的原位乳液聚合，乳液聚合顺利，纳米碳酸钙表面被丙烯酸酯类聚合物所包覆，使纳米碳酸钙粒子间的团聚不易发生，同时由于丙烯酸酯类聚合物与PVC、ABS、AS等极性聚合物具有较好的相容性，从而使纳米碳酸钙在聚合物基体中能达到纳米状态分散，从而发挥纳米效应。

This polyurethane prepolymer was used to copolymerize with vinyl monomer to synthesize the polyurethane-acrylate hybrid emulsion through free-radical emulsion polymerization.

用红外光谱仪、差示量热扫描仪，热重分析、马尔文粒度分析等测试手段，对合成产物进行了结构和性能表征。

DSC and dilatometry were carried out to determine the phase transformation temperature of a high speed steel used for centrifugal cast rolls.

采用差式扫描量热法及热膨胀法测定了离心铸造轧辊用高速钢的相变点，根据高速钢的临界转变温度，进行了退火、淬火和回火实验。

FT-IR spectra shows that the polyaniline is present primarily in the emeraldine salt form, and the polymeric chains interact with inorganic framework, most likely via V=O…HN hydrogen bonding. XRD,TG and DSC indicate that the lamellar structure of the V_2O_5 is preserved, PAn chains eliminate water form the interlamellar region and are partially inserted between the layers, and exist with extended-chain conformation owing to the confined environment.Electrochemical investigation in the range of 1.8~3.8V vs.

红外光谱表明复合物中PAn主要以导电聚苯胺盐的形式存在，PAn链与V_2O_5晶格之间可能形成了V=O…HN氢键。X射线衍射、热重和差示扫描量热证实了PAn/V_2O_5复合物保持了较规整的层间排列结构，PAn取代了V_2O_5干凝胶中的层间水而部分嵌入其片层间，由于受空间的限制，PAn分子链以比较伸展的链构象存在。

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。