量热

The image showed that the ratio of raw material of RPC and particle distribution accorded with maximum packing density theory, and the porosity of accumulation was the least. The DSC showed the reaction rate of RPC was very fast and main hydration process focused in shorter time; SEM and X-ray showed that structure of the harden body of RPC was much denser, which mainly composed of some abnormal flat grains that got maximum packing density, and hydration products were mostly composed of Ⅲ type C-SH gel and a small amount of Ca2 and no AFt crystal.

由图象分析可知，即C原材料的比例及颗粒度符合密实堆积原理，堆积物的孔隙率达到最小；差示扫描量热分析表明，RPC的水化反应速度很快，主要的水化过程集中在较短时间内；扫描电镜及X衍射试验表明，RPC硬化体的结构非常致密，主要由一些不规则状的扁平粒子紧密堆积在一起，水化产物主要是Ⅲ型C-S-H， Ca2晶体的量稀少且没有钙矶石。

By means of FTIR,SEM,DSC,TGA and XRD,we studied the microstructure,particle shape,meltage temperature,decomposition temperature and crystal degree,and gained better understanding about influences of different degrees of substitution on microstructure and thermal property of starch acetates.

用傅立叶红外、扫描电镜、差示扫描量热、热失重和X射线衍射测试技术对淀粉醋酸酯的结构、形貌、熔融温度、分解温度和结晶度进行表征，分析了不同取代度对醋酸酯淀粉的热性能及其结晶结构的影响。

H2SO4. By means of FTIR, SEM, DSC, TGA and XRD, we studied the microstructure, particle shape, meltage temperature, decomposition temperature and crystal degree, and gained better understanding about influences of different degrees of substitution on microstructure and thermal property of starch acetates.

用傅立叶红外、扫描电镜、差示扫描量热、热失重和X射线衍射测试技术对淀粉醋酸酯的结构、形貌、熔融温度、分解温度和结晶度进行表征，分析了不同取代度对醋酸酯淀粉的热性能及其结晶结构的影响。

The aim of this study was to develop a novel amphiphilic functional block poly(ε-caprolactone) bearing ketone groups MPEG-b-P(OPD-co-CL. 2-oxepane-1, 5-dione was copolymerized with ε-caprolatone in which methoxy poly (MPEG, Mn=5 000) and stannous octoate were used as initiator and catalyst, respectively. The syntheses were conducted by bulk and solution polymerization. 1H NMR results showed that peak position and splitting of the polymers synthesized through solution polymerization were consistent with theoretical data, demonstrating the products were designed block copolymers. While in the bulk polymerization, polymer peak position was changed due to their high reaction temperature, suggesting their structural variation.

将带有羰基官能团的4-羰基己内酯和ε-己内酯分别在甲氧基聚乙二醇(MPEG，Mn=5 000)为引发剂，异辛酸亚锡为催化剂溶液和本体体系中开环聚合，合成了两亲性侧基带有羰基官能团的聚己内酯嵌段共聚物MPEG-b-P(OPD-co-CL.1H NMR结果表明采用溶液聚合法合成的聚合物各峰的峰位置和分裂情况与理论一致，证明了产物是实验所设计的嵌段共聚物，而采用本体聚合法合成的聚合物由于温度的影响，聚合物各峰的峰位置发生了变化，说明其结构发生了变化；差示扫描量热法分析结果表明随着OPD单体含量的增加，聚合物的熔点，玻璃化转变温度和熔融焓增加；热失重测试结果表明OPD单体的引入增加了聚合物的热敏感性。

The thermal dynamic properties、glassing transition temperature and melting point of soybean proteins are studied by Differential Scanning Calorimetry , Thermogravimetry Analysis —Differential Thermal Analysis .

利用差示扫描量热分析、热重法-差热分析对大豆蛋白热力学性质、玻璃化转变温度和熔点等进行了研究，这些数据对于研究大豆蛋白可生物降解材料具有重要参考价值。

The paper mainly refers to the thermal stabilities of three nitrates n-propyl nitrate (NPN, isopropyl nitrate and 2-ethylhexyl nitrate by using Infrared spectrum experiment, ARC and DSC.

本论文主要采用了红外光谱实验，加速度量热仪和差示扫描量热仪等手段研究三种硝酸酯（硝酸正丙酯NPN、硝酸异丙酯IPN、硝酸异辛酯EHN）的热安定性。

The structure, morphology and thermal properties of the iron nanoparticles were investigated by means of X-ray diffraction, transmission electron microscopy, oxygen bomb calorimeter and themogravimetry.

采用X射线衍射能谱、透射电子显微镜、氧弹量热计和热分析测试技术表征了纳米铁微粒的结构、形貌及热性能。

Curing kinetics of epoxy resin and the effects of different compositions on curing reaction were researched by using the differential scanning calorimeters. Relationship between curing temperature and curing converting rate had been studied. Curing conditions for the system were determined. Modified nano-Al2O3/epoxy resin and core shell/epoxy resin composites were prepared by means of blending method. The influence of the composition on the properties was discussed. The thermal and dielectric properties of these composites were investigated using differential scanning calorimetry, Thermogravimetry and dielectric analyzer.

首先，论文通过差示量热扫描仪分析研究了环氧树脂与酸酐固化体系的固化反应动力学及固化工艺；然后，通过共混法和超声分散法制备了一系列纳米氧化铝/环氧树脂及核壳粒子/环氧树脂两相复合材料；进而通过DSC及热重分析仪测试了复合材料的玻璃化温度、热降解温度等热学性能，并采用介电分析仪测试分析了复合材料的介电常数、介电损耗等介电性能，讨论了组成对复合材料的热学性能及介电性能的影响。

Thermal behavior of RSRF was not affected by ultrasonic treatment, but it remarkably changed in the esterified RSRF. The Differential Scanning Calorimeters curves revealed the maximal thermal decomposition peak of cellulose and lignin in RSRF were disappeared, which reflected characters of RSRF were modified through esterification.

差示扫描量热法研究结果表明，超声波处理对RSRF的热性能没有影响，但酯化改性使RSRF的纤维素与木质素最大分解峰消失，主要反映为酯的性质，且热稳定性增强。

The structure of the copolymer was characterized by infrared spectrum, glass transition temperature and maximal heat decomposition temperature were analyzed by different scanning calorimetry and thermo gravimetric analysis.

利用红外光谱表征了共聚物结构，利用差示扫描量热法和热重分析测试了共聚物的玻璃化转变温度和最大热分解温度。

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。