量热

Differential Scanning Calorimetry and Small Angle X-ray Diffractometry were used to characterize the phase transitions in lamellar liquid crystal systems containing water, alkyl polysorbates, sorbitan esters, stearyl alcohol and oil. The order-disorder transition temperatures of the gelled O/W and W/O globular onion lamellar phases L(subscript O1) and L(subscript O2) and planar gelled lamellar phase L(subscript β) were measured as a function of system compositions.

采用示差扫描量热法和小角X射线衍射测试技术表征了由聚氧乙烯醚失水山梨糖醇脂肪酸酯、失水山梨糖醇脂肪酸酯、直链脂肪醇和挥发性物质组成的层状液晶体系的相转变特性，测定了水包油和油包水球形洋葱层状液晶L(下标 O1)和L(下标 O2)及平面层状液晶L的有序－无序的转变温度与体系组成之间的关系。

Cold crystallization process of N-(1-naphthyl) succinimide below glass transition temperature was monitored by differential scanning calorimetry and X-ray diffraction.

采用x射线粉末衍射和差示扫描量热分析方法，跟踪研究了N-（1-萘基）琥珀酰亚胺的液氮淬冷样品在室温(25℃)即在玻璃化转变温度以下的冷结晶行为。

The denaturation of lysozyme was analyzed under two different denaturants ethanol, dimethyl sulphoxide (DMSO using differential scanning calorimetry and the isoconversional method.

利用差示扫描量热法研究了溶菌酶在变性剂影响下的变性过程，并用等转化率法对该过程进行了分析。

Infrared spectroscopy indicates that glycorel decreases the in termolecular hydrogen bonding of starch and the size of starch molecules is reduced.

甘油分子减弱了淀粉分子中的氢键缔合，有效地减小了淀粉分子间作用力；差示扫描量热分析研究发现。

MAIN OUTCOME MEASURES: Differential scanning calorimeter was used to detect thermotical property; polarizing microscope was utilized for the microstructure observation; Antimicrobial activity and slow-release effect were determined by in vitro bacteriostasis and release, respectively.

主要观察指标：差示扫描量热仪表征其热学性能，偏光显微镜观察微观结构；通过体外释放及抑菌实验检测抗菌活性和缓释效果。

From error of trapezia quadrature and hardware design of calorimeter, we introduce sampling factor to obtain factual temperature and adopt shorter interval to perform cooling emendation.

提出以内外桶温差导致的量热系统温度变化的速度对主期测量时间进行积分的冷却校正计算模型。

3,6-Bis(1 H -1,2,3,4-tetrazol-5-yl-amino)-1,2,4,5-tetrazine was synthesized by triamino- guanidinium nitrate with 2,4-pentanedione of condensation, followed by oxidation and substitution reaction. The product was characterized by elemental analysis, IR, NMR and DSC.

以三氨基胍硝酸盐、戊二酮为起始原料，经缩合、氧化、取代等反应合成了3，6-双(1 H -1，2，3，4-四唑-5-氨基)-1，2，4，5-四嗪，并通过元素分析、红外、核磁、差示扫描量热法等分析手段对其进行了表征。

Cone calorimeter ; oxygen consumption principle ; decomposition heat ; polymer composites ; alumina trihydrate ; magnesium hydroxide

锥形量热仪；耗氧原理；分解热；聚合物复合材料；氢氧化铝；氢氧化镁

The organic/inorganic nanometer composite phase change heat storage materials of the bentonite/trihydroxy methyl propane and bentonite/TMP+neopentylglycol have been prepared with exchanged reaction, and characterized by XRD and DSC.

利用X射线衍射和差示扫描量热法对制得的有机/无机纳米复合相变储能材料进行了表征。

The temperature for crystallization obtained by differential scanning calorimetry is 193.92 ℃. The undeposited AgInSbTe is amorphous by the measurement of X-ray diffraction, while the phase change film is heated at 200 ℃, the peak could be observed by XRD, which indicated that the amorphous state had become a crystalline state.

示差扫描量热实验测定的结晶峰温度为193.92 ℃。X射线衍射表明未经热处理的沉积态薄膜是非晶态，而经过200 ℃热处理，X射线衍射图出现衍射峰，薄膜从非晶态转变到晶态。

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。