量滴

Transfer 50 ml of this solution to 200-ml Erlenmeyer flask, or, if smaller aliquot is taken, dilute to about 50 ml with water. Add 10 ml 4 N H2SO4, 1 ml KI,1 drop ammonium molybdate solution, and 50 ml water. With continuous agitation, add excess of 0.00359 N Na2S2O3 (5 10 ml).

移取50毫升上述溶液于200毫升于锥形瓶中，如果取样量较少，用水稀释到50 毫升，加入10 ml 4 N H2SO4，1 ml KI， 1滴钼酸胺溶液和50毫升水，边搅拌边加入过量的0.00359 N Na2S2O3溶液(5 10 ml)。

CALORIMETRIC TITRATION FOR COORDINATION REACTION OF 2, 3-BENZO-8, 11, 15-TRIMETHYL-18-CROWN-6 WITH ALKALI AND ALKALINE EARTH METAL IONS

若干碱金属及碱土金属离子与2，3-苯并-8，11，15-三甲基-18-冠-6配位反应的量热滴定研究

The works in the project just done can be summarized as five respects.(1) A device was designed to fabricate the asymmetrical resonant cavities by a pendant drop. A series ARCs with variable parameters provides a valuable experimental method for investigating the characteristics of ARCs.(2) The relationship between the number of active modes and the shape parameters in an ARC was investigated. The experimental lasing threshold was compared with theoretical result, the good agreement between two shown that it was the decrease of the number of active modes in an ARC that decreased lasing threshold.(3) Dye lasing gain was used to enhance the signals of stimulated Raman scattering of the weak gain Raman modes in a circular cavity made by a pendant drop, the instantaneous SRS spectra of weak gain Raman modes in ethanol was obtained by this new method.(4) The SRS signals of minority compound in a binary chemical complex was obtained by using dye lasing gain method. The detection concentration of minority compound was reduced to an order compared with normal SRS method.(5) A cylindrical circular cavity was formed by a liquid jet, which was used to reduce the pump intensity required for laser induced plasma spectroscopy. The limit of detection of trace element in aqueous sample was greatly decreased by this new method.

我们设计并成功制作了使悬垂液滴连续变形的装置，用此装置可以方便地改变非圆对称谐振腔的几何参数，为ARCs的研究提供了一种有效的实验方法；研究了ARCs中活性模式数和变形参数间的变化规律，激光阈值的数值计算结果和激光辐射的实验结果作了比较，二者吻合的曲线说明ARCs中活性模式数量的减少是受激辐射放大阈值降低的原因；在由单元化合物构成的微型圆对称谐振腔中，首次尝试用"激光增益"增强弱增益拉曼模式的受激拉曼散射信号，获得了乙醇分子中弱增益拉曼模式的瞬态SRS光谱；在由二元混合物构成的微型圆对称谐振腔中，用染料的激光增益增强了少量化合物的SRS信号，把少量化合物的SRS信号探测浓度降低了近一个数量级，在SRS应用于瞬态过程的组份分析方面做了卓有成效的探索；用石英毛细管形成的稳定液拄构成拄形谐振腔，降低了激光诱导等离子体光谱需要的激励能量，有效地降低了水相样品的痕量元素分析极限，为LIPS应用于微量元素的化学分析开拓了一条新的技术路线。

This paper studies the main geometrical parameter such as angle, height, width, stagger and the upper width in dentation and trapezoid flow path, firstly, uses the single-phase numerical simulation of the computational fluid dynamics technique to analyse the influence of different geometrical parameter on discharge coefficient and flow state exponent of drip emitter. Secondly, uses the two-phases numerical simulation of CFD (1% sand content ) to analyse the influence of the above mentioned geometrical parameter on the contribution regulation of sand and anti-clogging performance. Thirdly, uses the PIV （ particle Tracking Velocimetry ） technique which can see the small-scale flow path to observe and test the trajectories and velocities of solid particles in labyrinth flow path, and analyses the basic factors which can influence the movement characteristic of solid particles and the flow state in flow path.

本文以齿形流道、梯形流道为主要研究对象，以流道转角、流道高，流道宽、偏差量及梯形流道上底宽为主要结构参数，首先应用 CFD 单相流数值模拟技术对不同结构参数灌水器流道水力性能进行模拟，分析了不同结构参数对流态指数和流量系数的影响，其次，应用 CFD 两相流（含沙量为1%）数值模拟技术分析了结构参数对含沙量分布规律和抗堵塞性能的影响，然后，应用 PIV 可视化测试方法测试了固体颗粒在流道内运行轨迹及速度，分析了影响固体颗粒运动特性及流道内流体流态的基本因素，最后，对上述流道结构形式通过模具加工及滴灌带试制，进行了标准化测试（ GB/T 17187-1997 农业灌溉设备滴头技术规范和试验方法与 ISO 标准 ISO /TC23 /SC18 /WG5N4短周期堵塞测试程序），测试结果验证了 CFD 模拟结果，并提出了迷宫结构流道灌水器的抗堵塞设计方法。

The total iron in iron ore was titrated by potassium permanganate standard solution with sodium diphenylamine sulfonate as indicator.

用HNO3-HF处理，硫-磷混酸溶解试样，在盐酸介质中，用二氯化锡－三氯化钛将Fe(上标 3+)还原为Fe(上标 2+)，以二苯胺磺酸钠为指示剂，以高锰酸钾标准溶液滴定铁矿石中的全铁量。

In the presence of the combination of sulphuric and phosphoric acid, with sodium diphenylamine sulfonate as the indicator, standard solution of potassium dichromate was used to titrate total iron value.

试样以盐酸溶解后，在酸性介质中，先以氯化亚锡将三价铁大部分还原为二价，然后在钨酸钠指示下，再以三氯化钛将剩余的三价铁还原为二价，过量的三氯化钛以重铬酸钾氧化消除干扰，在硫磷混合酸存在下，以二苯胺磺酸钠为指示剂，用重铬酸钾标准溶液滴定全铁量。

Absorption spectrum of this complex is measured in 420nm wavelength,so titanium content in ferrotitanium will be determined.

将经典的铝还原—硫酸高铁滴定法，改为在硫酸—盐酸介质中，二安替比林甲烷与钛生成黄色可溶性络合物，在波长420nm处测量吸光度，借此进行测定钛铁中钛量。

A great deal of their difficulty is, of course, the difficulty of the subject and the inapplicability of the scientific method to the subject.

举个例子，密立根做了个油滴实验，量出了电子的带电量，得到一个今天我们知道是不大对的答案。

Place a loopful of the inoculum into the drop of stain and mix with the loop.

加入一菌环量的接种原至一滴染剂中，并用接菌环将之混合。

The table data measures the number of detected oil droplets per frame and converts to parts per million.

该表的数据检测了每个集中监测到的油滴的说量，然后换算成 PPM 。

In the United States, chronic alcoholism and hepatitis C are the most common ones.

在美国，慢性酒精中毒，肝炎是最常见的。

If you have any questions, you can contact me anytime.

如果有任何问题，你可以随时联系我。