量出

The results of toxicity experiments showed that R32 would not cause acute, chronic, cumulative and genetical toxicity effect on algae, Allium cepa, Zebra, fish and mice before it absorbed Cr. The recovery and sterilization measurement in routine water treatment could reduce most of the R32 in effluent. This may ensure that the effluent would not cause any ill effect on all kinds of biology in the environment after it was discharged into the river.

毒性实验结果表明：在吸附Cr~(6+)以前R_(32)对微生物无致突变性，对藻类、洋葱、斑马鱼和小鼠无急性毒性、慢性毒性和蓄积毒性；吸附Cr~(6+)后，常规水处理中的各种回收和杀菌措施可以降低出水中R_(32)的量，使出水排入江河后不会对环境中的各种生物产生不良的影响。

Given the current complexity of industrial recovery of 3'-methyl-2'-butenyl 3, 3-dimethyl-pentenoate and the decomposition problems with 2-methyl-1-butene, research was conducted on a process for direct recycling of MBDP involving an ester exchange reaction of MBDP with either methanol, trimethyl orthoacetate, or solutions of methanol and trimethyl orthoacetate.

针对目前工业上回收3，3-二甲基－4-戊烯酸－3'-甲基－2'-丁烯酯工艺复杂、异戊烯大量分解问题，研究了MBDP直接返回循环使用工艺，MBDP与甲醇、原乙酸三甲酯或与甲醇原乙酸三甲酯混合溶液进行酯交换反应的回收新工艺，比较了四异丙基钛酸酯、甲醇钠、氢氧化钾用作酯交换催化剂的效果，筛选出回收MBDP&一锅煮&最佳工艺：按照n：n：n：n＝1.0：9.8：9.2：0.05物质的量比投料，74℃~78℃反应21h，MBDP转化为贲亭酸甲酯和异戊烯醇，单程转化率87.7%，用85%的磷酸中和甲醇钠，蒸出甲醇，直接用于合成贲亭酸甲酯。

Five water sampling collected from Miyun Reservoir were observed quantitatively. Thirty-six species of zooplankton including 11 protozoan, 15 rotifers,6 cladocero and 4 copepoda were found. The results showed the eutrophicational feature, such as lower biodiversity ,miniaturization and more amount.

浮游动物共检出4门，30属，36种；浮游动物群落具有原生动物数量多，轮虫次之，枝角类与桡足类量少的特点，呈现出浮游动物数量大、小型化、多样性低等伴随水体富营养化出现的特征。

The micro actuator's static state characteristic by static electric force is analyzed in detail. The steady balance position's existing condition is educed while the moving pole move with linear displacement, and the relationship between driving voltage and the moving pole's line displacement is presented. The adsorption voltage by which the moving pole is adsorbed to fixed pole is exported. The resolution method of the pole cornual displacement's static state characteristic is opened out.

以应用RP技术制作三自由度电容式微型激励器为例，阐明了这种制造工艺的主要特点，探索了复杂微机械结构制作的新方法；详细分析了所设计微驱动器在静电力作用下的静态特性，推导出了可动极板线位移运动时存在稳定平衡位置的条件及驱动电压与可动极板线位移量之间的关系曲线；给出了可动极板吸合到固定电极上的吸合电压，指出了分析可动极板角位移静态特性的解析方法。

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area;2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support;3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier;4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling;5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene PolymerizationIn this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that:1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS;2.co-mlling time had no obvious effect on the texture of support after 12 hours;3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明，MAO不仅仅只和乙醇作用，MAO还与MgCl_2本身有一定的作用，这是一个极为重要的发现；3、通过ICP和EDX表征，发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布；4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能，特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化，并且催化剂寿命长，表现出稳定的动力学行为，最终获得了高堆密度(大于0.35g／ml)的球形聚乙烯颗粒；5、本文选择MSPC-5为研究对象，考察了聚合反应参数对催化剂的活性及其聚合物的影响，研究发现：不同的烷基铝对催化剂具有非常重要的影响，特别足TIBA对MSPC-5的助催化活性最高，烷基铝的加入量有一个较佳值，聚合温度为80度时活性最高，H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小；、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨，制备出了一种的新型的氯化镁载体，并将该载体用于多种单活性中心催化剂的负载化研究，研究表明：1、通过BET、XRD的表征，再次证实了MAO与MgCl_2之间具有直接作用，与XPS的研究结果相一致；2、当研磨时间高于12小时时，延长研磨时间对载体的结构没有显著的影响；3、将配合物3负载于共研磨时间不同的一系列载体上，乙烯聚合结果表明，尽管共研磨时间对负载催化剂的活性具有明显的影响，但是它对聚合物的性能以及催化剂的影响不明显。

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area; 2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support; 3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier; 4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling; 5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene Polymerization In this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that: 1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS; 2.co-mlling time had no obvious effect on the texture of support after 12 hours; 3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明，MAO不仅仅只和乙醇作用，MAO还与MgCl_2本身有一定的作用，这是一个极为重要的发现； 3、通过ICP和EDX表征，发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布； 4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能，特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化，并且催化剂寿命长，表现出稳定的动力学行为，最终获得了高堆密度(大于0.35g／ml)的球形聚乙烯颗粒； 5、本文选择MSPC-5为研究对象，考察了聚合反应参数对催化剂的活性及其聚合物的影响，研究发现：不同的烷基铝对催化剂具有非常重要的影响，特别足TIBA对MSPC-5的助催化活性最高，烷基铝的加入量有一个较佳值，聚合温度为80度时活性最高，H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小；、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨，制备出了一种的新型的氯化镁载体，并将该载体用于多种单活性中心催化剂的负载化研究，研究表明： 1、通过BET、XRD的表征，再次证实了MAO与MgCl_2之间具有直接作用，与XPS的研究结果相一致； 2、当研磨时间高于12小时时，延长研磨时间对载体的结构没有显著的影响； 3、将配合物3负载于共研磨时间不同的一系列载体上，乙烯聚合结果表明，尽管共研磨时间对负载催化剂的活性具有明显的影响，但是它对聚合物的性能以及催化剂的影响不明显。

During the process of the fore mentioned analyses, some tentative works as follows were done.(1)On the basis of the fundamental of spatial analytic geometry, the basic method for displaceable block searching was put forward and the relevant program was written. With this program one can easily search out all the displaceable blocks and omitting of blocks, which is very common in searching blocks manually, can be avoided.(2)The coefficient of stability of blocks with failure mode II-2(that is, sliding on a single sliding surface, but confined by near intersecting line )was deduced.(3)The multi-cavern effect of Laxiwa underground caverns was studied on the assumption that all of the caverns were full face tunneled at the same time.(4)The stability classification scheme of rock mass surrounding large scale underground caverns was established. In addition to inherit the merits of the method of engineering geological

在完成上述工作的过程中，本论文主要在以下几个方面进行了一些探索：①基于空间解析几何原理，提出了块体搜索的基本思路并编制出相应的程序，基本实现了块体搜索的自动化，既大大缩短了块体搜索时间，又能防止因人工搜索引起的遗漏；②推导出Ⅱ-2型(单滑面滑动，但受侧限面约束)块体的稳定性系数计算公式；③以数值模拟方法论证了拉西瓦地下厂房洞室群全断面一次开挖时群洞效应的具体特点；④以岩体质量、开挖效应、群洞效应和次生灾害效应为评价指标，建立了&大型地下洞室群围岩稳定性分类&方案；该方案既继承了水电行业规范&围岩工程地质分类&法的优点，又综合考虑了大型地下洞室群的工程特点。

The results show that by providing wastewaters pH of about 3 and reaction time of 2 hours, the quantity of H2O2 of 40 mL/L, the concentration of ferrous iron is 0.4 g/L, the effluent of microelectrolysis goes into Biological contact oxidation process, in which DO, HRT and volume load are 4.5 mg/L, 10 hours and 1.0 kg CODCr/(m3·d) respectively, satisfying the first grade of the national standard.

结果表明，在废水pH值为3左右、反应时间2 h的前提下，双氧水投加量40 mL/L，二价铁离子质量浓度为0.4 g/L，再经过微电解处理后的出水进入接触氧化阶段。在溶解氧为4.5 mg/L左右，水力停留时间为10 h、容积负荷1.0 kg CODCr/（m3·d）左右的条件下，出水CODCr小于100 mg/L，可达到国家对丙烯腈废水处理要求的一级标准。

In order to select optimal grid and good computation efficiency to recover the entire signal, aiming at the Ricker wavelet commonly used in forward modeling, we analyzed the alias and signal restoration problem in finite-difference method based on spatial sampling theorem and seismic wave traveling regulation in media with different velocity, to derive quantitative relationship among the modeling grid size, minimum velocity of model layer, and recovered main frequency of wavelet.

为了选择最佳的网格尺寸以及以最小的计算量完整地恢复出信号，针对地震波场正演模拟中经常使用的Ricker子波，根据空间采样定理和地震波在不同速度介质中的传播规律，分析了有限差分算法中的假频和信号恢复问题，推导出模拟网格尺寸、模型地层的最小速度和能够恢复的子波主频之间的近似定量关系，并用数值算例验证了这一关系。

Results: There were 56 cases with bilateral effusion ( 80.00%), 12 cases with right side effusion, and 2 cases with left side effusion;30 cases have small quantity of effusion , 32 cases have middle quantity of effusion, and 8 cases have large quantity of effusion; the pleural effusion of 41 cases is exuding, and that of 6 cases is transudate; the colour of the pleural effusion of 49 cases is yellow, that of 3 cases is sanguinolent.

结果：双侧积液为80.00%，右侧为17.14%，左侧为2.86%；胸腔积液少量30例(42.86%)，中量32例(45.71%)，大量8例(11.43%)；胸水性质漏出液41例，渗出液6例，介于渗漏出液之间5例；抽出黄色液体49例，血性液体3例。

In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

。但是，在否定句或疑问句里，这种带有"do"的方法表达的效果却没有什么强调的意思。

Go down on one's knees;kneel down

屈膝跪下。。。下跪祈祷