重氮化反应

In the dyestuff production process, such as AZO pigments of diazotization, it controls temperature technical by adding ice, which can be effective to control the diazonium salt decomposition in coupling reaction.

在颜料生产过程中，例如偶氮颜料的重氮化反应，偶合反应中，采用加冰控温工艺，可有效控制重氮盐的分解。

A series of azobenzenes with different electron effect substituents were prepared from diazonium salts and benzoguanamine.

将含有不同取代基的芳胺在盐酸介质中进行重氮化反应，制得相应的重氮盐，再与苯代三聚氰胺发生偶合反应，最终得到一系列含有不同取代基的偶氮化合物。

The paper discloses a process for diazotization fluorination of aromatic primary amines utilizing sodium nitrite and anhydrous hydrofluoride to produce the corresponding diazonium fluoride which is decomposed, usually by heat, to make the desired fluoroaromatics .

本文通过重氮化工艺路线的改进，在液态氟化氢中进行重氮化和重氮盐的热分解，提高了芳香族氟化物的收率，并且使重氮化反应工艺能应用于工业化生产。

The diazotization and hydrolysis process was used to synthesize high-purity m-cresol using m-toluidine as the main material.

间甲酚是一种重要的精细化工中间体，以间甲苯胺为原料，采用重氮化-水解法制备高纯度间甲酚，通过正交实验和单因素实验对重氮化反应工艺条件进行了优化。

Diazido-1,2,4,5-tetrazine has been synthesized from 3,6-bis(3,5-dimethylpyrazol-1-yl)-1,2,4,5-tetrazine by hydrazinolysis and diazotization.

以3，6-双（3，5-二甲基吡唑基）－1，2，4，5-四嗪为原料，经过肼解反应和重氮化反应，制得了3，6-二迭氮基－1，2，4，5-四嗪。

3,6-Diazido-1,2,4,5-tetrazine has been synthesized from 3,6-bis(3,5-dimethylpyrazol-l- yl)-1,2,4,5-tetrazine by hydrazinolysis and diazotization.

以3，6-双(3，5-二甲基吡唑基)-1，2，4，5-四嗪为原料，经过肼解反应和重氮化反应，制得了3，6-二叠氮基-1，2，4，5-四嗪。

The diazotization condition of 4-methyl-1-ethyl-3-cyano-5amino-6-hydroxy-2-pyridone and coupling condition of its diazo salt were researched, and the structure of its diazo salt was confirmed.

研究了4-甲基-1-乙基-3-氰基-5-氨基-6-羟基-2-吡啶酮的重氮化反应及其重氮盐发生偶合反应的条件，确定了重氮盐的结构。

The appropriate temperature of diazotization was-10～-5℃,and the diazotizating fluoborate was decomposed in petroleum ether to get 2-chloro-3-fluoropyridine with 64% yield.

以2-氯-3-氨基吡啶为原料，在40%的氟硼酸溶液中，采用饱和的亚硝酸钠为重氮化剂，在-10~-5℃下进行重氮化反应制得重氮盐，在石油醚中热分解得到2-氯-3-氟吡啶，收率为64%。

Syntheses of Curing Agent Modified Dicyandiamide by m-Toluidine;2. The diazotization and hydrolysis process was used to synthesize high-purity m-cresol using m-toluidine as the main material.

间甲酚是一种重要的精细化工中间体，以间甲苯胺为原料，采用重氮化-水解法制备高纯度间甲酚，通过正交实验和单因素实验对重氮化反应工艺条件进行了优化。

Methoxystilbene and 2-methoxy-4'-nitrostilbene were synthesized from benzyl chloride and nitrobenzyl chloride by the Wittig reaction, and used as intermediates for the synthesis of the final product fluorescent whitener FP4,4'-bis(2-methoxystyrylbiphenyl via reduction and diazotisation of the latter followed by reaction with the former in the presence of NaOH.

以氯化苄和对硝基氯苄为原料，经Wittig反应合成中间体：2-甲氧基-二苯乙烯和2-甲氧基-4'-硝基-二苯乙烯。后者经还原反应、重氮化反应后，在氢氧化钠存在下与前者反应生成最终产品荧光增白剂FP4，4'-双-2-(甲氧基苯乙烯基联苯。为该类荧光增白剂的合成开辟了一条新路线

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。