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重氮化

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Use nitrite and the Sulfanilic acid diazotization in acidic conditions,with dinitroaniline coupling formation color reaction,established the method of using the color reaction Determination Chinese cabbage s Nitrite content.

在酸性条件下亚硝酸盐与对氨基苯磺酸重氮化后,再与盐酸萘乙二胺偶合形成颜色反应,建立了用比色法测定大白菜中亚硝酸盐的方法。

This specific preparation methods including: parathion of the initial reaction in acid and zinc metal in the common under redox reaction, a product of the reduction of parathion - parathion, with the sodium nitrite in the cold under diazotization reaction, and bovine serum protein tyrosine on the o-hydroxy combination of the adult immune original and immune rabbit polyclonal antibody preparation.

本发明制备方法具体包括:以对硫磷为反应初始物,在酸和金属锌的共同参与下进行氧化还原反应,得对硫磷还原产物对氨基对硫磷,再与亚硝酸钠在低温下进行重氮化反应后,与牛血清蛋白酪氨酸上羟基的邻位结合,制备成人工免疫原,并免疫新西兰大白兔制备多克隆抗体。

The method is based on the diazo-reaction between nitrite ion and fuchsin acid in a hydrochloric acid medium.

研究了在酸性介质中,NO2-与酸性品红发生重氮化反应,致使酸性品红的荧光强度随NO2-加入量增加而明显降低的现象,建立了荧光熄灭法测定痕量NO2-新方法。

A rapid and sensitive flow-injection spectrophotometric method was proposed for the determination of metoclopramide. This method was based on the diazotisation of metoclopramide with sodium nitrite in acidic medium and coupling with α-naphthylamine.

基于在盐酸介质中,利用甲氧氯普胺一亚硝酸钠-α-萘胺的重氮化-偶合反应,建立了流动注射光度法测定甲氧氯普胺的新方法。

A new spectrophotometric method for the determination of chromium has been developed. In HCl medium, the chromium oxidizes hydroxylammonium chloride to form nitrite, which produces a pink azo dye when reacting with p-aminobenzene sulfonic acid and α-naphthylamine.

基于铬在稀盐酸介质中氧化盐酸羟胺产生亚硝酸根,而亚硝酸根与对氨基苯磺酸重氮化后可与α-萘胺偶联产生粉红色偶氮染料,提出了分光光度法测定铬的新方法。

In HCl medium, iodate oxidizes hydroxylammonium chloride to form nitrite, which can produce a red azo dye with the reaction of p nitroaniline and α naphthylamine.

基于碘酸根在稀盐酸介质中氧化盐酸羟胺产生亚硝酸根,而亚硝酸根和对硝基苯胺重氮化后可以与α-萘胺偶联产生红色偶氮染料,提出了分光光度法测定碘的新方法。

The nitric oxide released process of nitrosyl metalloporphyrins in vitro was detected with diazotization assay at room temperature, the four nitrosyl metalloporphyrinsbCo-NO、bFe-NO、a_(Co-NO、a_were good nitric oxide donors, the nitric oxide released efficiency is attained about seventy percent.

在室温下采用重氮化反应研究了这些金属卟啉-NO 配合物在水溶液中释放NO的过程,其中四种金属卟啉(bCo-NO、bFe-NO、aCo-NO、aFe-NO)有较好的释放效果,释放率达到近70%。

To prepare antibodies against MG, Pararosaniline was bound to BSA or OVA using nitrous acid as the coupling reagent, and using UV spectrophotometer scanning identified the conjugates.

为了制备针对MG及其代谢产物的抗体,将MG代谢相似物之一副品红用重氮化法偶联到牛血清白蛋白,获得免疫原BSA-PA。

A new fluotescence quenching method has been developed to determine nitrite in water samples. The method is based on the diazo-reaction between nitrite ion and thionine in dilute suifuric acid medium.

文章研究了在稀硫酸介质中亚硝酸根与硫堇发生的重氮化反应,基于硫堇的荧光强度随亚硝酸根的加入量增加而明显降低的现象,建立了荧光猝灭法测定痕量亚硝酸根的新方法。

Methoxystilbene and 2-methoxy-4'-nitrostilbene were synthesized from benzyl chloride and nitrobenzyl chloride by the Wittig reaction, and used as intermediates for the synthesis of the final product fluorescent whitener FP4,4'-bis(2-methoxystyrylbiphenyl via reduction and diazotisation of the latter followed by reaction with the former in the presence of NaOH.

以氯化苄和对硝基氯苄为原料,经Wittig反应合成中间体:2-甲氧基-二苯乙烯和2-甲氧基-4'-硝基-二苯乙烯。后者经还原反应、重氮化反应后,在氢氧化钠存在下与前者反应生成最终产品荧光增白剂FP4,4'-双-2-(甲氧基苯乙烯基联苯。为该类荧光增白剂的合成开辟了一条新路线

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