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Using the procedure described in Example 1, boron trifluoride diethyl etherate (1.49 liters, 12.1 moles) was added followed by 1.21 liters (12.1 moles) of borane-dimethyl sulfide at reflux.

用所述的程序例子1 ,硼乙( 1.49升, 12.1痣),然后又说是1.21升( 12.1痣)的硼-二甲基硫在回流。

Nitratomethyl-3-ethyloxetane was synthesized by the process of cyclization, nitation from trimethlolpropane and diethyl carbonate, and the homopolymer of 3-nitratomethyl-3-ethyloxetane was synthesized with 1,4-butanediol as initator and boron trifluoride etherate as an catalyst by cationic ring-opening polymerization.

以三羟-甲基丙烷和碳酸二乙酯为原料经环化、硝化两步反应合成了化合物3-硝酸酯甲基-3-乙基氧丁环;采用1,4-丁二醇为引发剂,三氟化硼乙(BF3Et2O)为催化剂,NIMEO发生阳离子开环聚合得到一种端羟硝酸酯均聚PNIMEO。

In the sevoflurane group, hepaticadenosine triphosphate and energy charge were significantlyhigh at all measurement times.

在七氟组,肝的三磷酸腺苷和能荷在所有测量时间点都明显较高。

The method comprises steps as follows:(1) Chinese herbal medicines are taken and added with purified water for soaking, with the material-to-water ratio of 1:10;(2) the Chinese herbal medicines with the purified water are placed in a microwave heating system; the power of the microwave and the radiation extraction time are controlled;(3) leaching liquor is poured out and put into a centrifuge for centrifugation to obtain the Chinese herbal medicine water extract;(4) polyethersulfone ultrafiltration film is arranged in an ultrafilter; the Chinese herbal medicine water extract is poured into the ultrafilter and placed in a normal pressure type microwave heating system; and (5) the power of the microwave and the radiation extraction time are controlled and the pressure of nitrogen is regulated so as to obtain the purified Chinese herbal medicine water extract.

本发明公开了一种利用微波辐射改善中草药水提液膜超滤过程的方法,该方法由以下步骤完成:(1)取中草药材以1∶10的料液比加入纯净水,浸泡;(2)置于微波加热系统,控制微波功率和辐射提取时间;(3)倾出浸提液;然后用离心机离心得中草药水提液;(4)超滤器内置有聚砜超滤膜,将中草药水提液倒入超滤器并置于常压式微波加热系统;(5)控制微波功率和辐射提取时间,调节氮气压力,得到纯化的中草药水提液。

The study of fluorescence spectrum proved that the excited phenylenerings of amorphous PES copolymer with high density phenylenerings in its main chain could form an excimer with the surrounding unexcited phenylenerings, and the emission peak intensity of excimer was strengthened with the increase of aging time.

荧光光谱的研究证明,非晶态聚砜共聚物由于主链苯环密度较高,苯环受激处于激发态时易与周围激态苯环相互作用形成激基缔合物,缔合物发射峰的强度随老化时间增加而增强。

The study of fluorescence spectrum proved that the excited phenylene-rings of amorphous PES copolymer with high density phenylene-rings in its main chain could form an excimer with the surrounding unexcited phenylene-rings, and the emission peak intensity of excimer was strengthened with the increase of aging time.

荧光光谱的研究证明,非晶态聚砜共聚物由于主链苯环密度较高,苯环受激处于激发态时易与周围激态苯环相互作用形成激基缔合物,缔合物发射峰的强度随老化时间增加而增强。

The S-PEU as well as H-PEU had a soft segment-rich surface as shown by ESCA study. The recalcification times for S-PEU and H-PEU increased 20% and 100%, respectively,as compared with that of ungrafted PEU.

ESCA及抗凝血性研究结果表明,不同位置接枝的PEU,其表面都有明显的聚链段富集。S-PEU抗凝血复钙时间只比未接枝者增长约20%,而H-PEU则增约一倍,比S-PEU增约60%。

The problems in production of low unsaturation polyether with DMC catalyst were introduced.

介绍了使用DMC催化剂生产低不饱和度聚时存在的问题。

These combinations of physical properties in the moisture cured polymer are superior to those obtained from prepolymers of the so called 'low unsaturation' polyether polyols.

这些在湿固化聚合物中的综合物理性质优于从所谓的"低不饱和"聚多元醇的预聚物得到的物理性质。

We recently caught up with him to talk FIFA versus PES, revolutionising dribbling games, unsporting behaviour and the merits of annual updates to the franchise.

最近,我们赶上了他说话国际足联和聚砜、改革盘带游戏、非体育道德行为而与之优点,每年更新的免赔额。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

聚光:照片上是建在西班牙桑路卡拉马尤城的一座新型PS20塔式太阳能电站。被称为&日光反射装置&的镜子将太阳光反射到主塔,然后用聚集的热量产生蒸汽进而通过涡轮机转化为电力