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Secondly,the synthesis of SIPE and the reaction conditions such as catalyst,anti-ether agent,temperature and water are researched to control the generation of diethylene glycol and the self-polymerization of SIPM by controlling the total quantum of distillate and the temperature of distillation column and reaction and the reliable synthetic conditions of SIPE are obtained.

其次,在此基础上,研究了三单体的中间体SIPE的合成工艺,研究了催化剂、抑剂、反应温度及水分等对合成反应的影响,同时提出了控制馏出物总量、控制分馏柱温度和控制反应温度等措施来控制二甘醇生成反应和SIPM自聚等副反应,得到了可靠的SIPE合成工艺。

RESULTS β-sitosterol(1),2,6-dihydroxyhumlan-9-3(12),7(13),9-triene(2),quercetin-7-methyl ester(3),protocatecheuic acid(4),shikimic acid(5),shikimic acid methyl ester(6) and daucosterol(7) were isolated from Ill...

结果从厚皮香八角果皮中分离得到了7个化合物,分别是β-谷甾醇(1)2、,6-dihydroxyhumulan-9-3(12),7(13),9-triene(2)、槲皮素-7-甲基(3)、原儿茶酸(4)、莽草酸(5)、莽草酸甲酯(6)和胡萝卜苷(7)。

In this review, basically classified by the chemical construction of dendritic skeleton, mainly focusing on the polyamidoamine, polypropylene imine, polycarbosilane, polyether and polyester systems, the recent advances in the rationally designed syntheses and their self-organized superstructure of side-chain LC dendrimers have been summarized and commented.

本文按树枝状大分子骨架的化学结构分类,对侧链型树枝状大分子液晶的设计合成、液晶相行为及其自组织超结构的最新研究进展进行总结和评述,重点介绍了聚酰胺-胺、聚丙烯亚胺、聚碳硅烷、聚以及聚酯树枝状大分子液晶体系。

The environmentally friendly scouring agent KX-301 is synt he sized based on fatty acid amide polyoxyethylene sodium succinate sulfonate and alkyl polyglucoside as main raw materials.

以脂肪酰胺琥珀酸单酯磺酸钠和烷基糖苷为主要原料,合成了环保型高效精练剂KX 30 1,该产品高效、耐强碱、绿色环保,可用于短流程染整前处理工艺。

Objective To investigate the chemical constituents of the root of Solanum torvum Swartz.

目的 研究金钮扣根石油部位和醋酸乙酯部位的化学成分。

Properties: colorless needle-like crystals, melting point 105 ~ 106 ℃, optical rotation +51 °(c = 0.978, chloroform), other reports shows that by ethanol recrystallization the melting point 104 ~ 105 ℃, methanol re - the formation of solvate crystal melting point 84 ℃.it is Soluble in acetone, chloroform, insoluble in ether, petroleum ether, insoluble in water.

性质:无色针状结晶,熔点105~106℃,旋光度+51°( c=0.978,氯仿),还有报道经乙醇重结晶熔点104~105℃,经甲醇重结晶形成的溶剂化物熔点84℃。易溶于丙酮、氯仿,难溶于乙、石油,不溶于水。

In recent years, the rapid development of domestic industries spandex polyurethane, polyether, the rapid growth of demand.

由于近年来国内氨纶的聚氨酯行业的高速发展,对聚的需求量快速增长。

Microcapsule is very small, hollow spherule is about 50/um fluoroaracil, the cyst from VDC and acryionitrile (about 2: 1) copolymer body composition, and in the presence of nangqian condrctor hydrocarbos as the petroleum ether that organic solvents.

微囊是很小的空腹小球,粒径约为50/um,囊壁由不正氯乙烯与丙烯腈(约2:1)共合体构成,而在囊芯洋含有矮冰点的如火油那样的无机溶剂。

The spherulite growth rates of PPS were measured in the range of crystallization temperature from 235 ℃ to 265 ℃ as a function of crystallization time.

采用热台偏光显微镜技术观察了聚苯硫及其玻璃纤维、炭纤维及芳纶纤维增强复合材料等温结晶过程中球晶结构形态的变化。

36 cases severe cardiac valve replacement whose cardio/thorax were 0.68~0.90 measured by sternite, heart function were Ⅲ~Ⅳ grade, average of left ventricle diastole diameterwas 67±9.2mm. All the patients heart function were improved by strict therapy before operate. Selecting best opportunity for operation, by general anesthesia, moderate hypothermia extracorporeal circulation, perfusing heart by cold stop-beating fluid including hypokalium and blood ,and refusing dopamine to maintain haemodynamics after cardiac resuscitation.

36例重症心脏瓣膜置换术病人,X线胸片心胸比0.68~0.90,心功能Ⅲ~Ⅳ级,左室舒张末径平均67±9.2mm,术前均经过严格改善心功能治疗,选择有利的手术时机,采用以芬太尼为主,咪唑安定、异丙酚、异氟等为辅助药的全身麻醉,中度低温体外循环,以高钾含血冷停跳液灌注心脏,心脏复苏后静脉输注多巴胺等维持血流动力学稳定。

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