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The oily substances and the acidic components were characterized using elementary analysis, IR spectral analyses and acidimetry.

采用石油和三氯甲烷分级萃取孤岛油田含聚污水中的油分,得到两个不同极性的组分F1和F2;用碱抽提法从酸值较高的F2组分中分离酸性物质并将其甲酯化,通过柱层析法将甲酯化物分成Ⅰ、Ⅱ和Ⅲ三个甲酯组分。

The experimental results showed that it was feasible to use vinyl ether as reactive monomer in the epoxy acrylate system.

实验结果表明,乙烯基作为活性单体用在环氧丙烯酸酯光固化体系中是可行的。

RESULTS: All combinations produced a result within 10% of that which would be predicted by additivity except for the combination of isoflurane with nitrous oxide where infraadditivity was found.

结果:除了有次相加性的笑气和异氟间的组合之外,其他所有的配对都得到了一个根据可加性得出的其预计值10%以内的结果。

It be easy to solve in alcohol ,aether and warm water.

本品为白色或浅白色粉末,熔点:260~264℃,易溶于醇、和热水。

Objective] GC analytical method for butyl ether in the workplace air using sampling by charcoal tube was studied.

目的] 研究炭管采集空气中丁的气相色谱分析方法。

In according with the reaction mechanism of alchohol and aldehyde, the reactional condition of 414 was originally explored.

根据醛对的加成反应机理,对414的合成条件进行了初步探索,确定了反应的最初反应条件。

The curing procedure of bisphenol A cyanate ester resin modified by copolymerization with epoxy E-51 and alicyclic epoxy resin R-122 was studied by differential scanning calorimetry.

采用示差扫描量热法对缩水甘油类环氧树脂(E-51)与脂环族环氧树脂(R-122)共同改性的双酚A型氰酸酯树脂的固化反应历程进行了研究。

The actinic radiation-curable and cationically polymerizable organic substance is at least one glycidylether of a polyhydric aliphatic, alicyclic or aromatic alcohol having at least three epoxy groups with epoxy equivalent weight between 90 and 800 grams per equivalent, at least one solid or liquid alicyclic epoxide with an epoxy equivalent weight between 90 and 330 grams per equivalent having at least two epoxy groups and monomer purity greater than about 90 % by weight, or at least a solid or liquid epoxycresol novolac or epoxyphenol novolac having epoxy equivalent weight between 130 and 350, or mixtures thereof.

可光化辐射固化并可阳离子聚合的有机物质为至少一种带有至少3个环氧基团环氧当量为90―800克每当量的脂族、脂环族或芳族多元醇的缩水甘油,至少一种环氧当量为80―330克每当量带有至少两个环氧基团且单体纯度大于约90wt%的固态或液态脂环环氧化物,或至少一种环氧当量为130―350的固态或液态环氧甲酚线性酚醛清漆或环氧苯酚线性酚醛清漆,或其混合物。

Recent progresses in thermodynamic study on the coordination of calixcrowns to alkali metal ions are introduced in the paper.

概要介绍了杯芳冠与碱金属离子配合的热力学研究方面的最新进展,较为系统地分析了选择性与热力学参数之间的相关性,得出了一般规律。

Methods: from prepation of crude drug as start, study the technology of extract and defat with L9 (3~4) orthogonal test. With EtOH extraction and water sed, alkali washing, EtOAC extraction as main methods of eliminate dopant. Finally with alky AlzO3 chromatographic column, rich and gain anticancer active site. The maximum response was achieved at a 40 min extracting time with 10 times volume 90% EtOH added to the sample for the first time and 30 min for the second time. Adding 10 times water will produce precipitation; Place the precipitation into 6 times petroleum benzin to de-fat at 60℃.

云南红豆杉中抗癌活性物制备工艺研究方法:利用正交设计试验L9(3~4)确定原料药提取工艺为:10倍量90%乙醇提取两次,第一次40分钟,第二次30分钟;醇提液用10倍量水沉;沉淀加6倍量石油40℃脱脂;用1mol/L的NaOH溶液碱洗,除去酸性杂质;以碱性氧化铝柱,以环己烷/丙酮为洗脱溶剂,在环己烷-丙酮(6:4)段富集到所需活性部位,洗脱剂用量为3VB。

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