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The p-tert-butyl calix arene (n=4,6,8) were synthesized by p-tert-butyl phenol, formaldehyde aqueous solution as raw materials. Six kinds of calixarene oligomeric surfactants were prepared by etherification of the calix arene with 1,3-propane sultone and 1,4-butane sultone.

以对叔丁基苯酚、甲醛为主要原料合成杯芳烃母体对叔丁基杯芳烃(n=4,6,8);以1,3-丙烷磺内酯、1,4-丁烷磺内酯为化试剂,经Williamson化反应,合成出6种杯芳烃基低聚表面活性剂。

The polyurethane hot-melt adhesive film was prepared by casting process and the effects of polyether diol trpe,chain exlender amount andpolyol molecular weight on tensile strength,tensibility and hardness were studied.

采用流延法制备聚氨酯热熔胶膜,对影响聚氨酯热熔胶膜的拉伸强度、断裂伸长率、硬度的几个因素:聚多元醇类型、扩链剂用量和聚多元醇的分子质量等进行了研究。

DPODPS with melting point within three degrees can be obtained,purified by recrystal.2, 4,4\'-diphenyoxy-diphenyl sulfone was synthesized by reaction of phenol with bis (4-chlorophenyl)sulfone in tetramethylene sulfone in the presence of NaOH.

将其在亲电反应条件下和对苯二甲酰氯或间苯二甲酰氯共缩聚制得了二种聚芳酮酮树脂,用IR、DSC、TG、WAXD等对其结构和性能进行了表征,同时研究了聚合物在300±10℃空气中的氧化热稳定性。

Five species of solvents, namely, acetone, ethyl acetate, ether, trichloromethane and petroleum ether were selected to obtain extracts from Portulaca oleracea L. with microwave assistance and the biological activities of each extract was tested against Plutella xylostella L.

在微波加热条件下,以丙酮、乙酸乙酯、乙、三氯甲烷和石油为溶剂对马齿苋干粉进行提取,试验了各溶剂提取物对小菜蛾幼虫的触杀、胃毒及拒食活性,确定了石油提取物触杀作用的LD50。

Poly(aryl ether sulfone ether ketone ketone) with side carboxyl attached to the main chain was synthesized by Friedel-Crafts polycondensation of 4,4′-diphenyoxyl diphenyl sulfone with trimellitic anhydride chloride.

以4,4′-二苯氧基二苯砜,偏苯三酸酐酰氯为单体通过Friedel-Crafts亲电反应合成了主链芳环上带有羧基侧基的聚芳酮酮树脂。

The results indicated that: Tripyrazolone, tripodal and crptands ligand L〓, L〓 and L〓 have good coordination ability with rare earth ions Rare earth ions were coordinated with their oxygen and nitrogen atoms.

结果表明,三脚架结构吡唑啉酮、三酸和穴配体与稀土离子有较好的配位作用,它是通过氮原子、氧原子与稀土离子配位的。而穴配体与稀土离子配位效果却不好。

In order to investigate the relation between the ligands and rare earth ions, in this dissertation, two new polyaza cryptands, two new tripyrazolone ligands, a macrobicyclic rare earth cryptates, a tripyrazolone and a tripodal ligands rare earth complexes have been synthesized.

为了进一步研究和探讨穴、吡唑啉酮、三脚架化合物配体对稀土元素的配位作用,论文首次报道了两个新氮杂穴配体、两个新三脚架吡唑啉酮结构配体、一个系列大二环新型的稀土配合物、一个系列三脚架吡唑啉酮结构配合物、一个系列三脚架结构三酸配合物的合成。

The allelopathic bioactivities on mycelial growth and the dose-activity relationships of two different Eucalyptus globulus leaves extracts,petroleum ether extract and chloroform extract,against five phytopathogens,Pyricularia oryzae,Rhizoctonia solani,Fusarium solani,Venturia pyrina,and Alternaria solani,were determined by mycelial growth rate method in PDA petri dish.

采用菌丝生长速率法,在PDA培养基上测定了蓝桉叶片的石油和氯仿提取物对水稻稻瘟病、小麦纹枯病、蚕豆根腐病、梨黑星病、番茄早疫病5种植物病原菌的化感作用,研究了蓝桉叶片的石油和氯仿提取物与病原菌的剂-效关系和提取物对病原菌菌丝生长速率的影响。

The improved method of konjac glucomannan carboxy methylation was proposed in this paper according to the effects of deacetylation. Carboxymethyl KGM were synthesized by blending KGM with etherification agent first and then basifying and catalyzing in ethanol. Basifying first and then etherifying prepared traditional carboxymethyl KGM.

针对脱乙酰基的这种影响进行羧甲基化方法的改进,在乙醇介质中先混合化剂,再进行碱化催化反应制备羧甲基魔芋葡甘聚糖,并通过与传统的先碱化再化的KGM羧甲基改性方法比较,达到乙酰基脱出顺序上的不同。

Flame retardant properties and mechanical properties of ABS which was incorporated into different molecular weight bromated epoxy resins flame retardant agent were evaluated.

与十溴二苯对比试验研究表明,添加高分子量溴化环氧树脂阻燃剂的ABS材料溴含量为7.9%时与添加十溴二苯阻燃剂的ABS材料溴含量为10.1%的阻燃性能相当。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

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