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N-(6-methyl-2-pyridine)-amino-methylene-diethyl malonate was produced by condensation reaction of 2-amino-6-methyl pyridine with ethoxymethylene diethyl malonate under optimal conditions that n(2-amino-6-methyl pyridine)∶n(ethoxymethylene diethyl malonate) is 1∶1.3, reacting time 45 min and temperature 130 ℃,the yield of this reaction was 96%,which was 6% higher than that of literature.

在250℃的反应温度下,分别以二苯、石蜡油和邻苯二甲酸二乙酯为热载体进行成环反应,得到4-氧-7-甲基-1,8-萘啶-3-羧酸乙酯的收率分别为88.6%、56.3%和61.2%,确定二苯为最佳热载体,并发现反应温度对产率的影响最大,原料配比次之,反应时间基本无影响。

The free fatty acids were extracted with petroleum ether and were separated on silicon gel column chromatography. The ethyl acetate-soluble lipid fraction and water-soluble lipid fraction were subjected to hydrochloric acid-catalyzed methanolysis, then were extracted with petroleum ether, respectively.

用石油提取低极性组分,经硅胶柱层析分离得到游离脂肪酸;用乙酸乙酯提取酯溶性神经酰胺及其衍生脂类,提取物和残余的水溶性脂类分别经盐酸甲醇解,水解产物再用石油提取。

MC and HPMC are both non-ionic,and etherified products of cellulose.They have functions such as thickening,emulsionizing,filming,water-maintaining,colloid-protecting,bonding,antienzyming,metabotic indifference and so on.They are applied widely in the fields of building,milkness paint,medcine,PVC,chemical articles,ceramics and agriculture.

甲基纤维素和羟丙基甲基纤维素均属非离子纤维素,是纤维素的化产品,具有优良的增稠、乳化、成膜、保护胶体、保持水份、粘合、抗酶以及代谢惰性等性能,广泛应用于建筑、乳胶涂料、医药、PVC、日用化学品、陶瓷以及农业生产中。

In this article, high DS and low viscosity carboxymethyl starch was prepared in aqueous media through the reaction between corn starch with acid treatment and etherifying agent, the effect of acid treatment time, liquor/material ratio, the amount of sodium hydroxide, the amount of monochloroacetic acid, etherification time, and reaction tempera.

以玉米淀粉为原料,采用酸化-化复合变性的方法在水相中制备高取代度低黏度羧甲基淀粉,探讨了酸化时间、液固比、NaOH用量、ClCH2COOH用量、化反应时间、反应温度对羧甲基化过程的影响,研究发现,对原淀粉进行酸化,可以在不增加其它反应试剂用量的基础上提高产物的取代度,但是酸化时间不应过长。

Among the open-chain crown ethers and cryptands with a same structure, the compounds disubstituted at the amide nitrogen atoms show the larger extractability for Am and Eu than the monosubstituted ones. The compounds disubstituted at the amide nitrogen atoms by two phenyl groups show the larger extractability for Am and Eu than those by two alkyl groups.

3在结构相同的开链冠和开链穴中,酰胺氮原子上二取代化合物对Am和Eu的萃取能力大于一取代化合物;酰胺氮原子上两个取代基都是苯基的化合物对Am和Eu的萃取能力大于两个取代基都是烷基的化合物。

Alkylphenol ethoxylates are nonionic surfactants and extensively used in industry. Manufacturers in Taiwan used to import nonene to produce nonylphenol and nonylphenol ethoxylates. They used to import octylphenol directly because it isn't easy to get octenes.

烷基酚聚乙基醇是工业上用途非常广泛的非离子性界面活性剂,国内目前有进口壬烯生产壬基酚及壬基酚聚乙基醇,而由於受限於辛烯原料取得不易,辛基酚都是直接进口。

A process for preparing clean gasoline features that under existance of epoxidizing catalyst and alkoxylating catalyst, the olefine in gasoline and the oxygen and alcohol take part in epoxidizing and alkoxylating reactions to generate diolmonoether or dioldiether compounds which has higher octane number, so being excellent gasoline component.

本发明公开了一种清洁汽油的生产方法,在一个具有环氧化的催化剂以及同时具有烷氧化催化组分或者催化剂的存在下,汽油中的烯烃与氧、醇、发生环氧化、烷氧基化反应而生成二醇单或二醇双类化合物,这类化合物具有较高的辛烷值,是优良的汽油组分。

Fourteen unreported N-substituted piperidin-4-one oxime ethers derivatives were synthesized withsubstituted benzylamines or phenethylamine as raw materials via a series of Michael addition, Dieckmann condensation, hydrolysis decarboxylation reactions, oximation a...

以取代苄胺或苯乙胺为起始原料,依次经Michael加成,Dieckmann缩合,水解脱羧,肟化和化等多步反应合成了14个未见文献报道的N-取代哌啶酮肟衍生物。

The intermediate which obtained from oximation of 7a-e reacted withmethyl N-(2-bromomethylphenyl)-N-methoxycarbamate to synthesize oxime ether methyl carbamate 3a-e.

以邻位卤代苯甲醛和3-丁烯-2-醇为原料通过钯催化&一锅法&反应合成了2-乙酰基茚7a-e,7a-e 肟化之后和N-(2-溴甲基苯基)-N-甲氧基氨基甲酸甲酯反应合成了肟类氨基甲酸甲酯3a-e,进一步胺解之后得到了肟类氨基甲酰甲胺3f-j。

Another relevant oxygenate is ethyl-tertiary-butyl ether, which has increasingly replaced MTBE.

另一个相关的氧化是乙基叔丁基,这已日益取代甲基叔丁基

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

聚光:照片上是建在西班牙桑路卡拉马尤城的一座新型PS20塔式太阳能电站。被称为&日光反射装置&的镜子将太阳光反射到主塔,然后用聚集的热量产生蒸汽进而通过涡轮机转化为电力