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By following the "self-assisted molecular editing" protocol first established in our labs,a number of Aphos ligands were efficiently prepared from a single starting material and they were screened for catalytic efficacy, leading to the discovery of the best-performing Aphos appended with a 3-nitrophenyl group at the C4 position.Combination of this Aphos with Pd_2 offers a precatalyst for successful cross-coupling of unactivated aryl chlorides with aryl boronic acids at room temperature.The reactions took place under mild basic conditions to produce the products in high yields.

通过我们首次提出的&自助分子剪裁&的概念从单一起始物快速合成和筛选了一系列膦配体,并发现C4位含3-硝基苯基的的膦配体和醋酸钯联用可以在室温下顺利地催化不活泼氯代芳烃和芳基硼酸的偶联反应,反应条件温和且产物收率很高。

Can mix undisturbedly slow the skin, restore the softness with its youth particular skin and vitality, cellulose of vitaminic E acetic acid conduces to antioxidant the loss that avoids free radical cell, and with other each component is mixed attainments cooperation, in order to retain cutaneous health and vigor.

可以镇静和舒缓皮肤,恢复其青春肌肤独有的柔软和活力,抗氧化剂维他命E醋酸纤维素有助于防止游离基细胞的损伤,并且与其它各成份和诣协作,以保持皮肤的健康和活力。

All the cases were compared locally biopsy under vaginoscope. We observed the reaction of the blood vessel of cervical epithelium with acetic acid on the green filter disc under vaginoscope.

用阴道镜绿色滤光片仔细观察涂醋酸后宫颈上皮血管的反应及整个宫颈醋白上皮变化并定位活检,全部病例匀在阴道镜下定位活检进行对照。

After consented and investigated using questionnaire (including risk factors of cervical cancer, knowledge of cancers), eligible women were examined by VIA and VILI and women who had ab...

对符合条件的妇女进行危险因素、癌症及子宫颈癌认知情况的问卷调查,用醋酸染色后肉眼观察和碘染色后肉眼观察进行宫颈检查,结果异常者进行阴道镜下活组织检查并得到最终的病理学诊断。

Gastric acidity and the concertration of pepsin were decreased.In addition, WYPE could promote gastrointestinal peristalsis,reduce the body torsion induced by acetic acid in mice.

结果胃疡平浸膏能抑制大鼠幽门结扎型胃溃疡、小鼠利血平型胃溃疡的形成;促进醋酸烧灼型胃溃疡的愈台;抑制胃液的分泌,降低胃液的酸度和胃蛋白酶含量。

The rats in control group were given distilled water, and the rats in experimental groups were given different doses of capsule(4.0、2.0、1.0g/kg), then enhance the capillary permeability of abdominal skin of rats by using xylic acid,and the OD numerical value was detected.

(1)抗炎实验:将40只小鼠随机分为补肾利浊胶囊高、中、低剂量组及对照组各10只,补肾利浊胶囊高、中、低剂量组分别给予相应剂量的补肾利浊胶囊(分别为4.0、2.0、1.0 g/kg),对照组给予蒸馏水,采用二甲苯酸致小鼠腹部皮肤毛细血管通透性增高,测定光密度值;(2)镇痛实验:40只小鼠分组及给药同抗炎实验,采用腹腔注射醋酸致小鼠出现扭体反应,纪录扭体次数并计算镇痛百分率;(3)抗前列腺炎实验:将雄性大鼠50只随机分为补肾利浊胶囊高、中、低剂量组及模型对照组及正常对照组,各10只。

Methods ①anti-inflammatory trial: 40 rats were randomly divided into control group, high-dose bushenlizhuo capsule group, middle-dose bushenlizhuo capsule group and low-dose bushenlizhuo capsule group(10 rats in each group).the rats in control group were given distilled water, and the rats in experimental groups were given different doses of capsule(4.0、2.0、1.0g/kg), then enhance the capillary permeability of abdominal skin of rats by using xylic acid,and the od numerical value was detected.

(1)抗炎实验:将40只小鼠随机分为补肾利浊胶囊高、中、低剂量组及对照组各10只,补肾利浊胶囊高、中、低剂量组分别给予相应剂量的补肾利浊胶囊(分别为4.0、2.0、1.0 g/kg),对照组给予蒸馏水,采用二甲苯酸致小鼠腹部皮肤毛细血管通透性增高,测定光密度值;(2)镇痛实验:40只小鼠分组及给药同抗炎实验,采用腹腔注射醋酸致小鼠出现扭体反应,纪录扭体次数并计算镇痛百分率;(3)抗前列腺炎实验:将雄性大鼠50只随机分为补肾利浊胶囊高、中、低剂量组及模型对照组及正常对照组,各10只。

Mesoporous zincum sulfide is synthesized by gentle wet chemosynthesis method, with DDA as templates and Zinc acetate and TAA as precursors. The effect to the synthesis of the ratio of reactive components, the volume of pH, reactive time and reactive temperature has been dicussed systematically, and structures of the as-synthesized samples have been characterized by X-ray diffraction, N2 adsorption-desorption, scanning electron microscopy, Fourier transform-infrared spectra, UV-vis diffuse reflectance spectroscopy, transmission electron microscopy.

以十二胺为模板,醋酸锌及硫代乙酰胺为前驱体,温和湿化学法合成了硫化锌无序介孔结构,系统研究了反应物配比、pH值、反应温度、反应时间对材料合成的影响,运用X射线衍射、N2吸附-脱附、扫描电镜、红外光谱、紫外-可见吸收光谱、透射电镜等分析手段对介孔材料的结构进行了详细的表征。

On sand packs consisting of 100 cm~3 quartz of particle size 0.3—0.6 mm, 2 mL kerosene, 1 mL produced water and several drops of isopropyl alcohol, the formulation of LFAR sand consolidation fluid is studied on the basis of the experimental data of compression strength and permeability of the consolidated sand packs and established as follows: 5.0 g LFAR; 0.5 g paratoluene sulfonic acid as curing agent; 5.0 g butyl acet...

在由100cm3粒径0.3~0.6mm的石英砂、2mL煤油、1mL油田污水、几滴异丙醇组成的固砂模型上,根据固结砂的抗压强度和渗透率筛选出了糠醇聚合物固砂剂各组分的用量:糠醇聚合物5g,固化剂对甲苯磺酸0.5g,稀释剂醋酸丁酯5g,后固化剂NaCl+HCl溶液100mL,预冲洗液80mL,后冲洗液80mL。

The toughening effect of chlorinated polye thylene and nano-mete r fumed silica (SiO 2) on polyvinyl chlorid e was investigated by means of to ughness contribution rate, the mechanical properties of the composite were also studied.

传统增韧硬PVC的技术是在树脂中加入弹性体,如CPE、乙烯-醋酸乙烯酯共聚物、丁腈胶 [1] ;但增韧后PVC的性能往往出现一种或多种缺陷,如拉伸、弯曲强度下降和模量损失等,使增韧和增强成为一种矛盾体。

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But we don't care about Battlegrounds.

但我们并不在乎沙场中的显露。

Ah! don't mention it, the butcher's shop is a horror.

啊!不用提了。提到肉,真是糟透了。

Tristan, I have nowhere to send this letter and no reason to believe you wish to receive it.

Tristan ,我不知道把这信寄到哪里,也不知道你是否想收到它。