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Critical temperatures of lyotropic liquid crystalline formed in cellulose diacetate/trifluoroacetic acid and CDA/dichloroacetic acid solutions of different concentration were determined respectively using DSC technique.

用DSC技术分别测定了二醋酸纤维素在不同浓度的三氟醋酸和二氯醋酸溶液中形成的溶致液晶的临界温度,并绘制了相图。

The spectra of X-ray diffract revealed that its crystal is B type and the value is about 18%, far lower than that of ordinary maize starch. With the method of chemistry modification, we modified the amylose starch with acetates. The result showed that the best reaction condition was at the ratio of 1:5.3 (glucose: acerbity), with MSA 1.5% catalyzer, at 75℃ for 3 h.

利用化学改性法对高直链玉米淀粉进行醋酸酯化改性,最佳反应条件为,淀粉葡萄糖基与酸的质量比1:5.3、催化剂甲磺酸用量为体系的1.5%、反应温度75℃、反应时间3 h,在此条件下可制备取代度为2.84的醋酸酯淀粉,比普通玉米淀粉高0.78。

Our company is mainly engaged in chemical raw materials trading, the company mainly engaged in: toluene, xylene, mesitylene, durene, 6 # 120 # 200 # solvent, ethyl acetate, butyl acetate, acetone, butanone, cyclohexanone, isophorone, MIBK, isopropyl alcohol, isobutyl alcohol, butanol, mixed alcohols, methanol, ethanol, ethylene glycol, diethylene glycol, diacetone alcohol, Anti-White Water, CAC, n-hexane, dichloromethane, trichloro-B, DMF, 5 # 10 # 15 # white mineral oil, lubricating oil, sewing machine oil, as well as high-pressure polyethylene, linear polyethylene, low-pressure polyethylene, polypropylene, rubber and other chemical raw materials.

我公司主要从事化工原料贸易,公司主要经营:甲苯、二甲苯、三甲苯、四甲苯、6# 120# 200#溶剂、醋酸乙酯、醋酸丁酯、丙酮、丁酮、环已酮、异佛尔酮、MIBK、异丙醇、异丁醇、正丁醇、混丙醇、甲醇、乙醇、乙二醇、二甘醇、二丙酮醇、防白水、CAC、正已烷、二氯甲烷、三氯乙、DMF、5# 10# 15#白矿油、润滑油、针车油以及高压聚乙烯、线性聚乙烯、低压聚乙烯、聚丙烯、橡胶等各种化工原料。

With addition of benzene and under certain current density and temperature, the indirect organic electrosynthesis using lead tetraacetate as media could be carried out in one compartment and no lead metal was deposited on the counter electrode.

在该醋酸电解液中加入一定量的苯,控制一定的电流密度、温度等条件可以阻化铅在对电极上的析出,实现了无隔膜电解槽中四醋酸铅的电解生成,并应用于间接有机电合成。

The results show that under the follow conditions: pyrolysis temperature 270癈,active carbon and: ethyne black=9:l, carbon pretreated with HNOs, 7.18% Mn(NO3)2(vs. carbon support) catalyst can exhibit the best performance. In order to improve the electrocatalystic performance of MnO2, Pb(CH3COO)2 , La(NO3)3-6H2O and Ce(NO3)3-6H2O are chosen as additives of MnCVC air electrode . Electrochemical performance of the electrodes is studied by current-potential polarization curves.

为了提高催化剂的性能,选择了醋酸铅、稀土作为添加剂,采用稳态极化和交流阻抗测试方法,结果表明:铅的氧化物、稀土La和Ce可作为MnO_2催化剂的助剂来促进氧气还原反应的进行,醋酸铅添加7.5%时极化最小,在一般金属-空气电池的工作电流密度20~50mA/cm~(-2)下,电位比单独MnO_2催化剂可提升30~50mV。

The optimum process starting from 1,3-dihydroxyacetone and formamidine acetate was: 22.54g(0.25mol) 1,3-dihydroxyacetone, 29.12g(0.28mol) formamidine acetate and 120ml isopropanol in liquid ammonia was heated to 40℃ for 8h.

以1,3-二羟基丙酮和醋酸甲脒为原料的较佳工艺:1,3-二羟基丙酮22.54g (0.25mol),醋酸甲脒29.12g (0.28mol),异丙醇120ml,通入液氨,40℃反应8h,减压蒸馏除去反应液中的氨气后过滤,滤液加至热的苦味酸饱和溶液,自然冷却至室温,制得4(5)-羟甲基咪唑苦味酸盐69.5g,收率85.0%。

Amount of 2 furaldehyde were increased with the increase of acetic acid aqueous solution concentration from 0 to 3%,and almost constant from 3% to 30%.

醋酸浓度从0至3%时,糠醛的收量随着增加,但是当醋酸浓度从3%增至30%时,其收量却几乎不变。

The monoesters of furoin were synthesized by esterification of corresponding the acyl chloride with the furoin.

糠偶姻单酯在醋酸铵和醋酸作用下合成了新化合物2-取代-4,5-双恶唑。

Isoamyl acetate and vanillin were chosen as pure olfactory nerve stimulator. There were 2 types of tasks in the experiment.

两种任务,一个是单一醋酸异戊酯刺激,另一个在醋酸异戊酯前给予香草醛,以防止可能的嗅觉注意减低。

A random copolymer of poly(vinyl acetate-co-isopropenyl acetate) with number-average molecular weight of 9600 and relatively narrow molecular weight distribution (MWD, M w/ M n=2.03)was prepared by free radical copolymerization of vinyl acetate with isopropenyl acetate using AIBN as initiator.

通过自由基共聚合方法,以AIBN为引发剂引发醋酸乙烯酯和醋酸异丙烯酯共聚,得到两者的无规共聚物聚。

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